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1. 发明授权

US5876686A Process for making inorganic oxide gels in fluorocarbon solvents 失效
标题翻译：在氟碳溶剂中制备无机氧化物凝胶的方法
公开(公告)号：US5876686A
公开(公告)日：1999-03-02
申请号：US663833
申请日：1996-06-14
申请人： Michael Joseph Michalczyk , Kenneth George Sharp
发明人： Michael Joseph Michalczyk , Kenneth George Sharp
IPC分类号： C01B13/32 , C03C1/00 , C03C17/42 , C04B41/45 , C04B41/52 , C04B41/81 , C04B41/89 , C09D5/00 , C23C26/00 , C01B13/14 , B32B27/00 , C01B33/12 , C01B35/10
CPC分类号： C04B41/009 , C01B13/32 , C03C1/008 , C03C17/42 , C04B41/4554 , C04B41/52 , C04B41/81 , C04B41/89 , C09D5/002 , C23C26/00 , Y10T428/3154 , Y10T428/31645 , Y10T428/31649 , Y10T428/31826 , Y10T428/31928 , Y10T428/31989
摘要： This invention relates to a process for the preparation of an inorganic oxide gel comprising contacting at least one fluorinated inorganic oxide precursor with a fluorinated gelling agent in the presence of at least one fluorinated solvent to form a solution; allowing sufficient time for gelation to occur; and isolating the inorganic oxide gel. Gels made by this process are useful as coatings and as components in inorganic/organic hybrid materials.
摘要翻译：本发明涉及一种制备无机氧化物凝胶的方法，包括在至少一种氟化溶剂存在下使至少一种氟化无机氧化物前体与氟化胶凝剂接触以形成溶液; 允许有足够的时间发生凝胶化; 并分离无机氧化物凝胶。通过该方法制成的凝胶可用作无机/有机杂化材料中的涂料和组分。

2. 发明授权

US08921300B2 Fluorinated surfactants 有权
标题翻译：氟化表面活性剂
公开(公告)号：US08921300B2
公开(公告)日：2014-12-30
申请号：US12465311
申请日：2009-05-13
申请人： Alexander Borisovich Shtarov , Michael Joseph Michalczyk , Charles Kenneth Taylor
发明人： Alexander Borisovich Shtarov , Michael Joseph Michalczyk , Charles Kenneth Taylor
IPC分类号： D06L1/02 , C07F9/09 , C07C67/287 , C07C309/10 , C07C309/17
CPC分类号： C07C309/10 , C07C67/287 , C07C309/17 , C07F9/091 , Y10T428/31855
摘要： A composition of formula I [Rf(CH2)m(O)n]x-A wherein Rf is a straight or branched perfluoroalkyl group having from about 2 to about 20 carbon atoms, or a mixture thereof, m is a positive integer equal to or greater than 3, n is 0 or 1, x is 1 to about 3, and A is −SO2B, B is N(R2)2 or N(CH2CH3)(CH2CH2OH), R2 is C1 to C4 alkyl.
摘要翻译：式I [Rf（CH 2）m（O）n] x A的组合物，其中Rf是具有约2至约20个碳原子的直链或支链全氟烷基，或其混合物，m是等于或大于 3以上，n为0或1，x为1〜3，A为-SO2B，B为N（R2）2或N（CH2CH3）（CH2CH2OH），R2为C1〜C4烷基。

3. 发明申请

US20090221466A1 FLUORINATED SURFACTANTS 有权
标题翻译：氟化表面活性剂
公开(公告)号：US20090221466A1
公开(公告)日：2009-09-03
申请号：US12465311
申请日：2009-05-13
申请人： Alexander Borisovich Shtarov , Michael Joseph Michalczyk , Charles Kenneth Taylor
发明人： Alexander Borisovich Shtarov , Michael Joseph Michalczyk , Charles Kenneth Taylor
IPC分类号： C07F9/09 , C07C69/54 , D06L1/00 , C11D3/24 , C11D17/08
CPC分类号： C07C309/10 , C07C67/287 , C07C309/17 , C07F9/091 , Y10T428/31855
摘要： A composition of formula I [Rf(CH2)m(O)n]x-A wherein Rf is a straight or branched perfluoroalkyl group having from about 2 to about 20 carbon atoms, or a mixture thereof, m is a positive integer equal to or greater than 3, n is 0 or 1, x is 1 to about 3, and A is —P(O)(OR1)y(OM+)3−y−x, —C(O)CH(SO3−M+)CH2C(O)−, −(CH2CH2O)d(CH2CHR2O)eR3, or −SO2B, M+ is an alkali metal ion, NH4+, or NH2(CH2CH2OH)2, B is N(R)2 or N(CH2CH3)(CH2CH2OH), R1 is C1 to C3 alkyl, and R2 is C1 to C4 alkyl, R3 is H or CH3, y is 0 to about 1, d is 0 to about 16, e is 0 to about 16, provided that (d+e) is from about 3 to about 16 is disclosed.
摘要翻译：式I的组合<？in-line-formula description =“In-line Formulas”end =“lead”？> [Rf（CH2）m（O）n] xA <？in-line-formula description =“In 其中R f为具有约2-约20个碳原子的直链或支链全氟烷基，或其混合物，m为等于或大于3的正整数，n为0 或（1），x为1至约3，A为-P（O）（OR 1）y（OM +）3-yx，-C（O）CH（SO 3 -M +）CH 2 C（O） - ， - （CH 2 CH 2 O） d（CH2CHR2O）eR3或-SO2B，M +是碱金属离子，NH4 +或NH2（CH2CH2OH）2，B是N（R）2或N（CH2CH3）（CH2CH2OH），R1是C1至C3烷基， R 2为C 1至C 4烷基，R 3为H或CH 3，y为0至约1，d为0至约16，e为0至约16，条件是（d + e）为约3至约16 。

4. 发明授权

US07288282B2 Coating compositions containing a fluorinated organosilane polymer 失效
标题翻译：含氟化有机硅烷聚合物的涂料组合物
公开(公告)号：US07288282B2
公开(公告)日：2007-10-30
申请号：US10668991
申请日：2003-09-22
申请人： William F. Graham , Douglas Robert Anton , Jeffery W. Johnson , Michael Joseph Michalczyk , Sape Kwesi Quashie
发明人： William F. Graham , Douglas Robert Anton , Jeffery W. Johnson , Michael Joseph Michalczyk , Sape Kwesi Quashie
IPC分类号： B05D3/00 , B05D7/26
CPC分类号： C08G18/728 , C08G18/6295 , C08G18/792 , C09D175/04
摘要： A coating composition containing a film-forming organosilane polymer, optionally a non-aqueous dispersed polymer, and a crosslinking agent selected from one or both of an organic polyisocyanate and melamine crosslinker. Fluorine functionalities are incorporated in the organosilane polymer to enhance soil resistance and cleanability. The coating composition can be used as a clearcoat over a conventional pigmented basecoat. The coating composition provides improved soil resistance and cleanability.
摘要翻译：含有成膜有机硅烷聚合物，任选的非水分散聚合物和选自有机多异氰酸酯和三聚氰胺交联剂中的一种或两种的交联剂的涂料组合物。将氟功能引入有机硅烷聚合物中以增强土壤抗性和可清洁性。涂料组合物可以用作常规着色底漆的透明涂料。涂料组合物提供改善的耐污性和可清洁性。

5. 发明申请

US20090042996A1 Mixed fluoroalkyl-alkyl surfactants 有权
标题翻译：混合氟代烷基 - 烷基表面活性剂
公开(公告)号：US20090042996A1
公开(公告)日：2009-02-12
申请号：US11890395
申请日：2007-08-06
申请人： Charles Kenneth Taylor , Michael Joseph Michalczyk , Erick Jose Acosta
发明人： Charles Kenneth Taylor , Michael Joseph Michalczyk , Erick Jose Acosta
IPC分类号： A61K31/045 , A61K31/66 , C07C309/63 , C07C31/125 , C07C311/01 , C07C69/00 , C07F7/02 , C07F9/02 , C09G1/06 , C09K13/00 , C09K3/00 , C11D1/00 , C11D1/04 , C11D1/34 , C11D3/20
CPC分类号： C07C69/675 , C07C43/137 , C07C309/65 , C07F7/0838 , C07F7/1804 , C07F9/091 , C11D1/004
摘要： A surfactant of formula 1 (Rf-A)a-Q-([B]k—R)b Formula 1 wherein a and b are each independently 1 or 2; Rf is a linear or branched perfluoroalkyl radical having from 2 to about 20 carbon atoms, optionally interrupted with at least one oxygen; R is a C1 to C20 linear, branched or cyclic alkyl, or a C6 to C10 aryl; B is —(CH2CHR1O)x—, k is 0 or 1, x is 1 to about 20, A is —(CH2)m[(CHR1CH2O)]s—[(CH2)m(CH)tCHOH(CH2)m]e—, wherein each m is independently 0 to 3, s is 0 to about 30, t is 0 or 1, and e is 0 or 1, R1 is H or CH3, Q is: —OP(O)(O−M+)(O)—, —O—, —S—(CH2)m—C(O)—O—, —SO2—O— —CH2CH2O—C(O)CH2C(OH)(V)CH2C(O)O—; —(CH2CH2O)xCH2CH(OH)—(CH2CH2O)x—(CH2)m—Si[OSi(R2)3]2—, —SO2NR2—, —(CH2CH2O)zC(O)CH(SO3−M+)CH2C(O)(OCH2CH2)z— wherein z is 1 to about 15, or a bond when s is a positive integer, V is —C(O)OR3 and R3 is H, CH3 or Rf; R2 is C1 to C4 alkyl, and M+ is a Group 1 metal or an ammonium (NHxR2y)+ cation wherein x+y=4, and R2 is C1 to C4 alkyl, provided that when Q is —OP(O)(O−M+)(O)— or when Q is —(CH2CH2O)z—C(O)CH(SO3−M+)CH2C(O)(OCH2CH2)z—, then at least one of s or e is a positive integer.
摘要翻译：（Rf-A）aQ - （[B] kR）b式1 <？在线公式“=”在线公式“end =”lead“ description =“In-line Formulas”end =“tail”？>其中a和b各自独立地为1或2; Rf是具有2至约20个碳原子的直链或支链全氟烷基，任选被至少一个氧中断; R为C1至C20直链，支链或环状烷基或C6至C10芳基; B是 - （CH 2 CHR 1 O）x - ，k是0或1，x是1至约20，A是 - （CH 2）m [（CHR 1 CH 2 O）] s - [（CH 2）m（CH）t CHOH（CH 2）m] e-，其中每个m独立地为0至3，s为0至约30，t为0或1，e为0或1，R 1为H或CH 3，Q为：-OP（O）（O-M + ）（O） - ， - O - ， - S-（CH 2）m C（O）-O-，-SO 2 -O-CH 2 CH 2 O-C（O）CH 2 C（OH）（V）CH 2 C（O） - （CH2CH2O）xCH2CH（OH） - （CH2CH2O）x-（CH2）m-Si [OSi（R2）3] 2-，-SO2NR2-， - （CH2CH2O）zC（O）CH（SO3-M +）CH2C O）（OCH 2 CH 2）z - ，其中z为1至约15，或当s为正整数时为键，V为-C（O）OR 3且R 3为H，CH 3或R f; R2是C1-C4烷基，M +是1价金属或铵（NHxR2y）+阳离子，其中x + y = 4，R2是C1-C4烷基，条件是当Q是-OP（O） M +）（O） - 或Q为 - （CH 2 CH 2 O）z C（O）CH（SO 3 -M +）CH 2 C（O）（OCH 2 CH 2）z - 时，则s或e中的至少一个为正整数。

6. 发明申请

US20080131595A1 Method for achieving recoat adhesion over a fluorinated topcoat 有权
标题翻译：在氟化面漆上实现再涂覆粘合的方法
公开(公告)号：US20080131595A1
公开(公告)日：2008-06-05
申请号：US12012557
申请日：2008-02-04
申请人： William F. Graham , Douglas Robert Anton , Jeffery W. Johnson , Michael Joseph Michalczyk , Sape Kwesi Quashie
发明人： William F. Graham , Douglas Robert Anton , Jeffery W. Johnson , Michael Joseph Michalczyk , Sape Kwesi Quashie
IPC分类号： B05D3/10
CPC分类号： C09D143/04 , C09D133/16 , Y10T428/31551 , Y10T428/31598
摘要： A method for repairing a basecoat/clearcoat finish or coating comprised of a fluorinated organosilane topcoat. A fluorinated urethane additive is added to the fluorinated organosilane topcoat composition to improve recoat adhesion with the repair basecoat.
摘要翻译：一种用于修补由氟化有机硅烷面漆组成的底漆/透明涂层或涂层的方法。向氟化有机硅烷面漆组合物中加入氟化氨基甲酸酯添加剂以改善与修补底涂层的重涂性。

7. 发明申请

US20080118741A1 Glass Articles with Adhesion and Stain Resistant Non-Stick Coatings 有权
标题翻译：玻璃制品具有粘附和耐污渍的不粘涂层
公开(公告)号：US20080118741A1
公开(公告)日：2008-05-22
申请号：US11927867
申请日：2007-10-30
申请人： Michael Joseph Michalczyk , Michael J. Witsch
发明人： Michael Joseph Michalczyk , Michael J. Witsch
IPC分类号： B32B5/16 , B32B17/06
CPC分类号： C03C17/009 , C03C17/007 , C03C17/3405 , C03C2217/475 , C03C2218/112 , C03C2218/113 , Y10T428/24364 , Y10T428/252 , Y10T428/259 , Y10T428/261 , Y10T428/265 , Y10T428/3154 , Y10T428/31663 , Y10T428/31721
摘要： The invention provides a non-stick coating for glass cookware that has good adhesion and stain resistance while maintaining the abrasion resistance of the non-stick coating. The non-stick coating comprises a base coat that contains fluoropolymer and colloidal silica and an overcoat comprising one or more polymer layers containing inorganic filler film hardener.
摘要翻译：本发明提供一种玻璃炊具的不粘涂层，其具有良好的粘附性和耐污染性，同时保持不粘涂层的耐磨性。不粘涂层包括含有含氟聚合物和胶态二氧化硅的底涂层和包含一个或多个包含无机填料膜固化剂的聚合物层的外涂层。

8. 发明授权

US06177196B1 Phosphorus-containing fluoromonomers and polymers thereof 有权
标题翻译：含磷含氟单体及其聚合物
公开(公告)号：US06177196B1
公开(公告)日：2001-01-23
申请号：US09255901
申请日：1999-02-23
申请人： Paul Douglas Brothers , Ming-Hong Hung , Michael Joseph Michalczyk , Tatsuhiro Takahashi
发明人： Paul Douglas Brothers , Ming-Hong Hung , Michael Joseph Michalczyk , Tatsuhiro Takahashi
IPC分类号： B32B2728
CPC分类号： C07F9/091 , C07F9/113 , C07F9/14 , C07F9/1403 , C08F30/02 , C08F214/184 , C08F214/262 , C08J7/047 , C08J2443/00 , C09D4/00 , Y10T428/3154 , Y10T428/31544 , Y10T428/31663 , Y10T428/31667 , Y10T428/31678 , Y10T428/31692 , Y10T428/31855 , C08F214/18
摘要： Fluorinated vinyl ethers having phosphorus-containing groups are useful as monomers in making fluoropolymers having functional sites.
摘要翻译：具有含磷基团的氟化乙烯醚可用作制备具有官能位点的含氟聚合物的单体。

9. 发明授权

US5684111A Silylated dioxolane polymers and monomeric compounds 失效
标题翻译：甲硅烷基二氧戊环聚合物和单体化合物
公开(公告)号：US5684111A
公开(公告)日：1997-11-04
申请号：US683514
申请日：1996-06-14
申请人： Michael Joseph Michalczyk , Ming-Hong Hung , Lech Wilczek
发明人： Michael Joseph Michalczyk , Ming-Hong Hung , Lech Wilczek
IPC分类号： C07F7/12 , C07F7/18 , C08G77/48 , C08G77/50 , C08G77/04
CPC分类号： C07F7/12 , C07F7/1836 , C08G77/48 , C08G77/50
摘要： This invention relates to novel polymeric and monomeric silane substituted fluorinated 1,3-dioxolane compounds and their preparation from 4,5-difluoro-1,3-dioxolane and difunctional or monofunctional silicon hydrides.
摘要翻译：本发明涉及新的聚合物和单体硅烷取代的氟化1,3-二氧戊环化合物及其由4,5-二氟-1,3-二氧戊环和双官能或单官能硅氢化物的制备。

10. 发明授权

US08071198B2 Glass articles with adhesion and stain resistant non-stick coatings 有权
标题翻译：玻璃制品具有粘附和耐污渍的不粘涂层
公开(公告)号：US08071198B2
公开(公告)日：2011-12-06
申请号：US11927867
申请日：2007-10-30
申请人： Michael Joseph Michalczyk , Michael J. Witsch
发明人： Michael Joseph Michalczyk , Michael J. Witsch
IPC分类号： B32B17/10 , B32B27/06 , B32B27/20 , B32B27/34
CPC分类号： C03C17/009 , C03C17/007 , C03C17/3405 , C03C2217/475 , C03C2218/112 , C03C2218/113 , Y10T428/24364 , Y10T428/252 , Y10T428/259 , Y10T428/261 , Y10T428/265 , Y10T428/3154 , Y10T428/31663 , Y10T428/31721
摘要： The invention provides a non-stick coating for glass cookware that has good adhesion and stain resistance while maintaining the abrasion resistance of the non-stick coating. The non-stick coating comprises a base coat that contains fluoropolymer and colloidal silica and an overcoat comprising one or more polymer layers containing inorganic filler film hardener.
摘要翻译：本发明提供一种玻璃炊具的不粘涂层，其具有良好的粘附性和耐污染性，同时保持不粘涂层的耐磨性。不粘涂层包括含有含氟聚合物和胶态二氧化硅的底涂层和包含一个或多个包含无机填料膜固化剂的聚合物层的外涂层。

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