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1. 发明授权

US06689218B2 Systems for the deposition and curing of coating compositions 失效
标题翻译：涂料组合物的沉积和固化系统
公开(公告)号：US06689218B2
公开(公告)日：2004-02-10
申请号：US09682831
申请日：2001-10-23
申请人： Radislav Alexandrovich Potyralio , Daniel Robert Olson , Michael Jarlath Brennan , Jay Raghunandan Akhave , Mark Anthony Licon , Ali Reza Mehrabi , Dennis Lee Saunders , Bret Ja Chisholm
发明人： Radislav Alexandrovich Potyralio , Daniel Robert Olson , Michael Jarlath Brennan , Jay Raghunandan Akhave , Mark Anthony Licon , Ali Reza Mehrabi , Dennis Lee Saunders , Bret Ja Chisholm
IPC分类号： B05C2100
CPC分类号： B82Y30/00 , B01J19/0046 , B01J2219/0036 , B01J2219/00378 , B01J2219/0043 , B01J2219/00518 , B01J2219/00527 , B01J2219/00585 , B01J2219/00596 , B01J2219/00605 , B01J2219/00612 , B01J2219/00621 , B01J2219/00637 , B01J2219/00659 , B01J2219/00689 , B01J2219/00704 , B01J2219/00711 , B01J2219/00716 , B01J2219/00756 , B05D1/00 , B05D3/00 , B05D3/0254 , B05D3/0263 , B05D3/06 , B05D3/067
摘要： Systems and methods for creating a combinatorial coating library including a coating system operatively coupled to at least one of a plurality of materials suitable for forming at least one coating layer on a surface of one or more substrates and a curing system operative to apply at least one of a plurality of curing environments to each of a plurality of regions associated with the at least one coating layer. The curing system including a scanning mirror system having a mirrored surface positionable relative to an incoming radiation beam, wherein the mirrored surface is positionable to direct the incoming radiation beam to a selected one of the plurality of regions associated with the coating layer. The combinatorial coating library comprising a predetermined combination of at least one of the plurality of materials and at least one of the plurality of curing environments associated with each of the plurality of regions.
摘要翻译：用于产生组合涂料库的系统和方法，其包括可操作地耦合到多种材料中的至少一种的涂层系统，所述涂层系统适用于在一个或多个基材的表面上形成至少一个涂层，以及固化系统，的多个固化环境中的至少一个涂层的多个区域中的每一个。该固化系统包括具有可相对于入射辐射束定位的镜面的扫描镜系统，其中镜面可定位成将入射辐射束引导到与涂层相关联的多个区域中的选定一个区域。组合涂料库包括多个材料中的至少一种材料和与多个区域中的每一个相关联的多个固化环境中的至少一个的预定组合。

2. 发明授权

US06538725B2 Method for determination of structural defects of coatings 有权
公开(公告)号：US06538725B2
公开(公告)日：2003-03-25
申请号：US09765757
申请日：2001-01-22
申请人： Radislav Alexandrovich Potyrailo , Daniel Robert Olson , Michael Jarlath Brennan , James Norman Cawse , Bret Ja Chisholm
发明人： Radislav Alexandrovich Potyrailo , Daniel Robert Olson , Michael Jarlath Brennan , James Norman Cawse , Bret Ja Chisholm
IPC分类号： G01B1116
CPC分类号： G01N21/6452 , C09K11/06 , G01N21/25 , G01N21/31 , G01N21/8422 , G01N21/88 , G01N2021/6417 , G01N2021/646
摘要： The present invention provides a method for quantifying structural defects of a coating composition on a given substrate, where certain structural defect-inducing tests are performed. In this method, a coating formulation is doped with a colorimetric or luminescent material. Concentration of the material depends on the quantum efficiency, excitation and emission wavelengths, and employed detection techniques, and can range from about 1 fM to about 1 mM. Before, during and/or after such tests, the coating is illuminated with a wavelength of radiation at which the reflected or transmitted color or emitted luminescence of the material in the coating is detectable with an optical detector or by visual inspection. In this fashion, the percentage of failure of the coating can be quantified as well as the level of interdiffusion of coating into substrate or substrate into coating. The method of the invention is thus particularly well-suited for the combinatorial analysis of an array of coating samples. Additionally, when the structural defect-inducing material test is being performed, the removed coating material can be analyzed in like fashion.

3. 发明授权

US06836362B2 Method for the rapid determination of the optical quality of combinatorial libraries 失效
标题翻译：快速确定组合库光学质量的方法
公开(公告)号：US06836362B2
公开(公告)日：2004-12-28
申请号：US09854718
申请日：2001-05-14
申请人： Radislav Alexandrovich Potyrailo , Michael Jarlath Brennan , Daniel Robert Olson
发明人： Radislav Alexandrovich Potyrailo , Michael Jarlath Brennan , Daniel Robert Olson
IPC分类号： G01N1104
CPC分类号： G01N21/47 , G01N2021/4735 , G01N2021/8427
摘要： This invention provides methodology for the measurement of both low and high levels of scattered radiation produced by decorative and barrier coatings and plastics. Measurements of low levels are especially important for coatings used in automotive applications. The method is based on the illumination of the sample with radiation and collection of only the portion of the radiation scattered from the coating before, during and after the testing step and relating the optical signal from the tested portion of the sample material to the untested portion of the material and/or a standard. Through the practice of the invention, a large number of coating samples, as in an array, may be analyzed for their optical quality, principally haze, either after coating and curing, and/or after subjection of such coatings samples to elongation stresses, and/or abrasion testing, solvent exposure, hydrolytic stability testing, and temperature exposure.
摘要翻译：本发明提供了用于测量装饰和阻隔涂层和塑料产生的低和高水平散射辐射的方法。低水平的测量对于汽车应用中使用的涂料尤为重要。该方法基于样品的照射，并且在测试步骤之前，之中和之后仅收集从涂层散射的辐射的部分，并将来自样品材料的测试部分的光学信号与未测试部分相关联的材料和/或标准。通过本发明的实践，如在阵列中，可以分析大量涂层样品的光学质量，主要是在涂层和固化之后和/或在将这样的涂层样品置于伸长应力之后的雾度，以及 /或磨损试验，溶剂暴露，水解稳定性试验和温度暴露。

4. 发明授权

US06684683B2 Method and apparatus for characterizing the barrier properties of members of combinatorial libraries 失效
标题翻译：表征组合库成员的屏障特性的方法和装置
公开(公告)号：US06684683B2
公开(公告)日：2004-02-03
申请号：US10083436
申请日：2002-02-27
申请人： Radislav Alexandrovich Potyrailo , Michael Jarlath Brennan
发明人： Radislav Alexandrovich Potyrailo , Michael Jarlath Brennan
IPC分类号： G01N2902
CPC分类号： G01H5/00 , G01N5/02 , G01N15/082 , G01N29/022 , G01N2015/086 , G01N2015/0873 , G01N2291/011 , G01N2291/015 , G01N2291/018 , G01N2291/0255 , G01N2291/0256 , G01N2291/02845 , G01N2291/02881 , G01N2291/0422 , G01N2291/0423 , G01N2291/0426 , G01N2291/0427 , G01N2291/106
摘要： A method and an apparatus for characterizing the barrier properties of an array of coatings. The method including providing a plurality of acoustic wave devices, wherein each of the plurality of acoustic wave devices comprises at least one surface, and providing a plurality of coating materials suitable for forming a plurality of coatings on the at least one surface of each of the plurality of acoustic wave devices. The method also including coating each of the plurality of acoustic wave devices with at least one of the plurality of coating materials to form a plurality of coated acoustic wave devices and measuring a predetermined output parameter of each of the plurality of coated acoustic wave devices. The method further including exposing the plurality of coated acoustic wave devices to an analyte vapor of a predetermined concentration, measuring the predetermined output parameter of each of the plurality of coated acoustic wave devices, and correlating a change in the predetermined output parameter of each of the plurality of coated acoustic wave devices to the barrier properties of each of the plurality of coatings.
摘要翻译：用于表征涂层阵列的阻挡性能的方法和装置。所述方法包括提供多个声波装置，其中所述多个声波装置中的每一个包括至少一个表面，并且提供适于在所述至少一个表面的至少一个表面上形成多个涂层的多个涂层材料多个声波装置。该方法还包括用多个涂覆材料中的至少一个涂覆多个声波装置中的每一个以形成多个涂覆的声波装置并测量多个涂覆的声波装置中的每一个的预定输出参数。该方法还包括将多个涂覆的声波装置暴露于预定浓度的分析物蒸气，测量多个涂覆的声波装置中的每一个的预定输出参数，并且将每个涂覆的声波装置的预定输出参数的变化相关联多个涂覆的声波装置到多个涂层中的每一个的阻挡性能。

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