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1. 发明授权

US5017606A Fluorobenzyl esters 失效
标题翻译：氟苄酯
公开(公告)号：US5017606A
公开(公告)日：1991-05-21
申请号：US536078
申请日：1990-06-11
申请人： Michael J. Robson
发明人： Michael J. Robson
IPC分类号： C07C69/747 , A01N37/10 , A01N53/00 , A01N53/06 , C07B61/00 , C07C33/48 , C07C67/03 , C07C67/08 , C07C67/11 , C07C67/14 , C07C69/743
CPC分类号： A01N53/00 , C07C33/483
摘要： Fluorobenzyl esters of the formula: ##STR1## wherein X represents the residue of any carboxylic acid of formula X-COOH which forms an insecticidally active ester with a 3-phenoxybenzyl alcohol, and R, R.sup.6 and R.sup.7 are each selected from hydrogen, halogen and alkyl of up to four carbon atoms, provided that at least one of R, R.sup.6 and R.sup.7 represents halogen, and further provided that R and R.sup.6 are not both bromine when R.sup.7 is hydrogen. The compounds are useful for combatting insect and acarine pests.
摘要翻译：式（I）的氟苄基酯，其中X表示与3-苯氧基苄醇形成杀虫活性酯的式X-COOH的任何羧酸的残基，R，R6和R7各自选自氢卤素和至多四个碳原子的烷基，条件是R，R 6和R 7中的至少一个表示卤素，并且进一步规定当R 7为氢时R和R 6不同时为溴。这些化合物可用于防治昆虫和螨类害虫。

2. 发明授权

US4853414A Halogenated esters 失效
标题翻译：卤代酯
公开(公告)号：US4853414A
公开(公告)日：1989-08-01
申请号：US114732
申请日：1987-10-30
申请人： Michael J. Robson , John Williams
发明人： Michael J. Robson , John Williams
IPC分类号： C07C69/747 , A01N53/00 , A01N53/06 , C07C43/23 , C07C53/00 , C07C69/743
CPC分类号： C07C43/23 , A01N53/00
摘要： Compounds of formula (I), useful as insecticides and knockdown agents: ##STR1## where Y is C.sub.1-6 alkoxy, Z is halo or C.sub.1-6 alkoxy; R is --(CH.sub.2).sub.p --(O).sub.m --R.sup.3 where m and p may be 0 or 1; R.sup.3 is C.sub.1-6 alkyl, phenyl or benzyl, or when m is 0, R.sup.3 is C.sub.1-6 alkenyl, haloalkenyl, alkynyl or haloalkynyl, and either (a) A and B are both C.sub.1-4 alkyl or (b) A is hydrogen and B is (R.sup.1)(R.sup.2)C.dbd.CH-- where R.sup.1 and R.sup.2 are selected from methyl, chloro, bromo, fluoro and trifluoromethyl.
摘要翻译：用作杀虫剂和敲低剂的式（I）化合物：其中Y是C 1-6烷氧基，Z是卤素或C 1-6烷氧基; R是 - （CH 2）p - （O）m -R 3，其中m和p可以是0或1; R3是C1-6烷基，苯基或苄基，或当m是0时，R3是C1-6链烯基，卤代烯基，炔基或卤代炔基，（a）A和B都是C1-4烷基或（b）A是氢和B是（R 1）（R 2）C = CH-，其中R 1和R 2选自甲基，氯，溴，氟和三氟甲基。

3. 发明授权

US4681969A Process for the preparation of an enantiomeric pair of isomers of cyfluthrin 失效
标题翻译：制备氟氯氰菊酯异构体对映异构体的方法
公开(公告)号：US4681969A
公开(公告)日：1987-07-21
申请号：US769493
申请日：1985-08-26
申请人： John Williams , Michael J. Robson
发明人： John Williams , Michael J. Robson
IPC分类号： C07C253/34 , A01N53/00 , A01N53/08 , C07B31/00 , C07B55/00 , C07C67/00 , C07C253/00 , C07C255/39 , C07C121/75
CPC分类号： A01N53/00
摘要： A process is described by which the pair of isomers represented by (R)-.alpha.-cyano-4-fluoro-3-phenoxybenzyl (1R,cis)-3-(2,2-dichlorovinyl)-2,2-dimethylcyclopropane carboxylate and its enantiomer is converted by base catalyzed epimerization in solution into the insecticidally more useful isomer pair represented by (S)-.alpha.-cyano-4-fluoro-3-phenoxybenzyl (1R,cis)-3-(2,2-dichlorovinyl)-2,2-dimethylcyclopropane carboxylate and its enantiomer, which may then be caused to crystallize out from the solution.
摘要翻译：描述由（R）-α-氰基-4-氟-3-苯氧基苄基（1R，顺式）-3-（2,2-二氯乙烯基）-2,2-二甲基环丙烷羧酸酯代表的一对异构体对和（S）-α-氰基-4-氟-3-苯氧基苄基（1R，顺式）-3-（2,2-二氯乙烯基）-3-甲氧基苯甲酸酯代替的杀虫剂更有用的异构体对，将其对映异构体转化为碱溶液中的碱催化差向异构体， 2,2-二甲基环丙烷羧酸酯及其对映异构体，然后可以从溶液中结晶出来。

4. 发明授权

US5132469A Fluorobenzyl esters 失效
标题翻译：氟菊酯
公开(公告)号：US5132469A
公开(公告)日：1992-07-21
申请号：US667804
申请日：1991-03-11
申请人： Michael J. Robson
发明人： Michael J. Robson
IPC分类号： C07C69/747 , A01N37/10 , A01N53/00 , A01N53/06 , C07B61/00 , C07C33/48 , C07C67/03 , C07C67/08 , C07C67/11 , C07C67/14 , C07C69/743
CPC分类号： A01N53/00 , C07C33/483
摘要： 4-Haloalkenyl-2,3,5,6-tetrafluorobenzyl alcohols of formula (III): ##STR1## are intermediates to insecticidally active fluorobenzyl esters of formula (I): ##STR2## wherein X represents the residue of any carboxylic acid of formula X-COOH which forms an insecticidally active ester with a 3-phenoxybenzyl alcohol, and R, R.sup.6 and R.sup.7 are each selected from hydrogen, halogen and alkyl of up to four carbon atoms, provided that at least one of R, R.sup.6 and R.sup.7 represents halogen, and further provided that R and R.sup.6 are not both bromine when R.sup.7 is hydrogen.

5. 发明授权

US4778822A Insecticidally active ester 失效
标题翻译：杀虫活性酯
公开(公告)号：US4778822A
公开(公告)日：1988-10-18
申请号：US481948
申请日：1983-04-04
申请人： Michael J. Robson
发明人： Michael J. Robson
IPC分类号： A01N53/00 , C07C17/093 , C07C17/14 , C07C25/13 , C07C69/743
CPC分类号： C07C25/13 , A01N53/00 , C07C17/093 , C07C17/14
摘要： The invention relates to a method of combating soil-dwelling root worms of the genus Diabrotica which comprises treating the soil in which said root worms dwell with the compound 2-chloro-3, 6-difluorobenzyl (.+-.)-cis-3-(Z-2-chloro-3,3,3-trifluoroprop-1-en-1-yl)- 2,2-dimethylcyclopropane carboxylate.
摘要翻译：本发明涉及一种防治黑腹病属的土壤 - 居住根蠕虫的方法，该方法包括用所述化合物2-氯-3,6-二氟苄基（+/-） - 顺式-3- （Z-2-氯-3,3,3-三氟丙-1-烯-1-基）-2,2-二甲基环丙烷羧酸酯。

6. 发明授权

US5093362A Insecticidal compounds 失效
标题翻译：杀虫剂化合物
公开(公告)号：US5093362A
公开(公告)日：1992-03-03
申请号：US472951
申请日：1990-01-31
申请人： David J. Milner , Mark A. Spinney , Michael J. Robson
发明人： David J. Milner , Mark A. Spinney , Michael J. Robson
IPC分类号： C07C67/08 , A01N53/00 , A01N53/06 , C07C67/10 , C07C67/14 , C07C69/747
CPC分类号： A01N53/00
摘要： The invention provides compounds of formula: ##STR1## wherein R.sup.1 represents hydrogen or halogen and R.sup.2 represents C.sub.1-8 alkyl or C.sub.1-8 haloalkyl, useful as insecticides and knockdown agents. The invention also provides compositions comprising them, methods of their use in controlling insects, and processes for their preparation.

7. 发明授权

US5049585A Certain 3,3-bis-(difluoro methyl)2,2-dimethyl-cyclopropane carboxylates having insecticidal activity 失效
标题翻译：某些具有杀虫活性的3,3-双（二氟甲基）2,2-二甲基 - 环丙烷羧酸盐
公开(公告)号：US5049585A
公开(公告)日：1991-09-17
申请号：US417921
申请日：1989-10-06
申请人： Michael J. Robson , Mark A. Spinney
发明人： Michael J. Robson , Mark A. Spinney
IPC分类号： A01N53/00 , A01N53/06 , C07B61/00 , C07C61/15 , C07C67/03 , C07C67/08 , C07C67/10 , C07C67/14 , C07C69/74 , C07D209/48 , C07D213/64 , C07D213/647 , C07D233/72 , C07D307/45 , C07D307/68
CPC分类号： C07D209/49 , A01N53/00 , C07C61/15 , C07D213/647 , C07D233/72 , C07D307/42
摘要： Insecticidal compounds with effective knockdown activity against public health pests and having the general formula: ##STR1## wherein Z is selected from 3-allyl-2-methyl-4-oxocyclopent-2-en-1-yl; 3-propargyl-2-methyl-4-oxocyclopent-2-en-1-yl; 1-ethynyl-2-methylpent-2-en-1-yl; 3,4,5,6-tetrahydrophthalimidomethyl; (6-phenoxypyrid-2-yl)methyl; 1-cyano-1-(6-phenoxypyrid-2-yl)methyl; 1-propargylimidazolin-2,4-dione-3-ylmethyl; 5-benzylfur-3-ylmethyl; and a group of formula: ##STR2## wherein X represents hydrogen, hydroxy, methoxy or ethynyl. The invention also provides processes for the preparation of, and insecticidal compositions comprising, the compounds of formula (I).

8. 发明授权

US4927852A Insecticidal compounds characterized by enhanced knockdown effect 失效
标题翻译：特征在于增强击倒效果的杀虫化合物
公开(公告)号：US4927852A
公开(公告)日：1990-05-22
申请号：US229532
申请日：1988-08-08
申请人： Michael J. Robson , Peter J. V. Cleare , Mark A. Spinney
发明人： Michael J. Robson , Peter J. V. Cleare , Mark A. Spinney
IPC分类号： C07B61/00 , A01N53/00 , A01N53/06 , A01P7/04 , C07C67/03 , C07C67/08 , C07C67/10 , C07C67/14 , C07C69/74 , C07C69/743
CPC分类号： A01N53/00
摘要： The invention provides insecticidal compositions exhibiting excellent knockdown activity against public health pests, in particular cockroach species, comprising compounds of formula (I): ##STR1## wherein X represents a group of formula: ##STR2## where (i) R.sup.1 and R.sup.2 are each selected from hydrogen, halo and C.sub.1-4 alkyl, or (ii) R.sup.1 is hydrogen and R.sup.2 represents either R.sup.3 (R.sup.4)C.dbd.CH-- or R.sup.3 (R.sup.4)(R.sup.5)C--CH(R.sup.5)--, where R.sup.3 and R.sup.4 are selected from hydrogen, methyl, halo and C.sub.1-2 haloalkyl and R.sup.5 is selected from chloro and bromo. The invention also provides methods of use of the compositions, novel compounds of formula (I) and processes for their preparation.

9. 发明授权

US4879423A 2-chloro-3,6-difluoro-benzyl halide 失效
标题翻译： 2-氯-3,6-二氟 - 苄基卤化物
公开(公告)号：US4879423A
公开(公告)日：1989-11-07
申请号：US230368
申请日：1988-08-10
申请人： Michael J. Robson
发明人： Michael J. Robson
IPC分类号： A01N53/00 , C07C17/093 , C07C17/14 , C07C25/13
CPC分类号： C07C25/13 , A01N53/00 , C07C17/093 , C07C17/14
摘要： The compound 2-chloro-3,6-difluorobenzyl 3-(2-chloro-3,3,3-trifluoroprop-1-en-1-yl)-2,2-dimethylcyclopropane carboxylate in any of its isomeric forms and mixture of these isomeric forms including racemates. Insecticidal compositions containing this compound and methods of using the compound against insect pests are also disclosed.
摘要翻译： 3-（2-氯-3,3,3-三氟丙-1-烯-1-基）-2,2-二甲基环丙烷甲酸酯的化合物2-氯-3,6-二氟苄基酯其任何异构体形式和这些异构形式包括外消旋体。还公开了含有该化合物的杀虫剂组合物和使用该化合物对昆虫害虫的方法。

10. 发明授权

US5208239A Fungicidal pyridinylpyrimidine compounds 失效
标题翻译：杀真菌素吡啶二吡啶化合物
公开(公告)号：US5208239A
公开(公告)日：1993-05-04
申请号：US785646
申请日：1991-10-31
申请人： Michael J. Robson , Paul A. Worthington
发明人： Michael J. Robson , Paul A. Worthington
IPC分类号： A01N43/54 , C07D401/04
CPC分类号： C07D401/04 , A01N43/54
摘要： Fungicidal compounds having the formula (I): ##STR1## wherein R.sup.1 is an optionally substituted phenyl group, C.sub.3-6 cycloalkyl optionally substituted by alkyl or alkyl; R.sup.2, R.sup.3, R.sup.4, R.sup.5, R.sup.6 and R.sup.7 are independently hydrogen, C.sub.1-4 alkyl, C.sub.1-4 haloalkyl, C.sub.1-4 alkoxy or N'R"; Z is a linking group and is --C.tbd.C--, --CR.sup.8 .dbd.CR.sup.10 -- or --CR.sup.8 R.sup.9 --CR.sup.10 R.sup.11 --; R.sup.8, R.sup.9, R.sup.10, R.sup.11, R' and R" are independently hydrogen or C.sub.1-4 alkyl; provided that when R is alkyl Z is not --CR.sup.8 R.sup.9 --CR.sup.10 R.sup.11 --; and acid addition salts or metal complexes thereof; and processes for preparing then, compositions comprising them and methods of using them to combat fungi.
摘要翻译：具有式（I）的杀真菌化合物：其中R 1是任选取代的苯基，任选被烷基或烷基取代的C 3-6环烷基; R2，R3，R4，R5，R6和R7独立地是氢，C1-4烷基，C1-4卤代烷基，C1-4烷氧基或N'R“; Z是连接基团，并且是-C 3 D C，-CR 8 = CR 10 - 或-CR 8 R 9 -CR 10 R 11 - ; R8，R9，R10，R11，R'和R“独立地为氢或C1-4烷基; 条件是当R是烷基时，不是-CR8R9-CR10R11-; 和酸加成盐或其金属络合物; 制备方法，包含它们的组合物和使用它们对抗真菌的方法。

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