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1. 发明申请

US20110065959A1 Removal of Silica from Water Soluble Compounds by Nanofiltration and Reverse Phase Chromatography 有权
标题翻译：通过纳滤和反相色谱从水溶性化合物中除去二氧化硅
公开(公告)号：US20110065959A1
公开(公告)日：2011-03-17
申请号：US12675130
申请日：2008-08-21
申请人： Allan R. Bailey , David H. White , Derick L. Kaspar , Robert E. Vandas , Michael J. Gentilcore , Hung V. Nguyen , Anna K. Fukunaga
发明人： Allan R. Bailey , David H. White , Derick L. Kaspar , Robert E. Vandas , Michael J. Gentilcore , Hung V. Nguyen , Anna K. Fukunaga
IPC分类号： C07C231/24
CPC分类号： B01D61/027 , A61K49/0433 , A61K49/103 , A61K49/106 , B01D15/325 , B01D2315/16
摘要： A process for separating soluble silica species such as monomeric silicic acid (or monosilicic acid) and low molecular weight soluble polymeric silica from impure water soluble compounds by membrane nanofiltration is provided. A process for separating soluble silica species and colloidal silica from impure water soluble compounds by reverse phase liquid chromatography is also provided.
摘要翻译：提供了通过膜纳滤法从不纯的水溶性化合物中分离可溶性二氧化硅物质例如单体硅酸（或单硅酸）和低分子量可溶性聚合二氧化硅的方法。还提供了通过反相液相色谱从可溶性水溶性化合物中分离可溶性二氧化硅物质和胶体二氧化硅的方法。

2. 发明授权

US06946060B2 Purification of N,N-dimethylacetamide 有权
标题翻译： N，N-二甲基乙酰胺的纯化
公开(公告)号：US06946060B2
公开(公告)日：2005-09-20
申请号：US10186764
申请日：2002-07-01
申请人： Michael J. Gentilcore
发明人： Michael J. Gentilcore
IPC分类号： B01D3/14 , B01D3/42 , C07C231/24 , C07C233/05
CPC分类号： C07C231/24 , B01D3/146 , Y10S203/09 , C07C233/05
摘要： A method to purify N,N-dimethylacetamide (DMAc) from an aqueous solution containing acetic acid as a contaminant. Two fractional distillation columns are arranged in a series. The solution containing the contaminant is provided to the first column with a temperature profile to result in acetic acid partitioning into the overhead water. The material remaining in the bottom portion of the first column is recycled to the first column and also provided into a second column, whereby DMAc free of acetic acid contamination is recovered, and remaining DMAc and acetic acid are returned to the first column for further separation. The method uses standard fractional distillation procedures and equipment, thus eliminating the need for more complex extractions and/or chromatographic separations.
摘要翻译：从含有乙酸作为污染物的水溶液中净化N，N-二甲基乙酰胺（DMAc）的方法。两个分馏塔排列成一系列。将含有污染物的溶液以温度分布提供给第一塔，导致乙酸分配到塔顶水中。残留在第一塔底部的材料被再循环到第一塔并且还提供到第二塔中，由此回收不含乙酸污染的DMAc，并且将剩余的DMAc和乙酸返回到第一塔进行进一步分离。该方法使用标准的分馏程序和设备，因此不需要更复杂的萃取和/或色谱分离。

3. 发明授权

US4724103A Process for preparing N,N-diacetic acid aminomethylenephosphonic acid 失效
公开(公告)号：US4724103A
公开(公告)日：1988-02-09
申请号：US676749
申请日：1984-12-05
申请人： Michael J. Gentilcore
发明人： Michael J. Gentilcore
IPC分类号： C07F9/06 , C07F9/38
CPC分类号： C07F9/3808
摘要： An energy saving process for preparing N,N-diacetic acid aminomethylenephosphonic acid by reacting an alkali metal salt of iminodiacetic acid in aqueous strong mineral acid solution with phosphorous acid and formaldehyde and then adding sufficient water to dissolve the alkali metal salt formed during the reaction. The desired product is recovered as a precipitate from the solution.

4. 发明授权

US4775498A Process for preparing N,N-diacetic acid aminomethylenephosphonic acid 失效
标题翻译：制备N，N-二乙酸氨基亚甲基膦酸的方法
公开(公告)号：US4775498A
公开(公告)日：1988-10-04
申请号：US823843
申请日：1986-01-29
申请人： Michael J. Gentilcore
发明人： Michael J. Gentilcore
IPC分类号： C07F9/38
CPC分类号： C07F9/3808
摘要： An energy saving process for preparing N,N-diacetic acid aminomethylenephosphonic acid by reacting an alkali metal salt of iminodiacetic acid in aqueous strong mineral acid solution with phosphorous acid and formaldehyde and then adding sufficient water to dissolve the alkali metal salt formed during the reaction. The desired product is recovered as a precipitate from the solution.
摘要翻译：通过将亚氨基二乙酸的碱金属盐在强酸性无机酸水溶液中与亚磷酸和甲醛反应制备N，N-二乙酸氨基亚甲基膦酸，然后加入足够的水来溶解反应中形成的碱金属盐。所需产物作为沉淀从溶液中回收。

5. 发明授权

US5356520A Separation of high boiling point solvents from amyl acetate 失效
标题翻译：从乙酸戊酯中分离高沸点溶剂
公开(公告)号：US5356520A
公开(公告)日：1994-10-18
申请号：US23283
申请日：1993-02-26
申请人： William Z. McCarthy , Michael J. Gentilcore
发明人： William Z. McCarthy , Michael J. Gentilcore
IPC分类号： B01D3/32 , C07C67/54 , B01D3/14
CPC分类号： B01D3/32 , C07C67/54 , Y10S203/22
摘要： A process for the separation of amyl acetate, a high boiling point solvent from various high boiling point corrosive impurities, namely, bromoethyl acetate, in an industrial setting to allow for reuse through continuous recycling thereof.
摘要翻译：一种在工业环境中分离各种高沸点腐蚀性杂质（即乙酸溴乙酯）的高沸点溶剂的乙酸戊酯的方法，以允许通过其连续回收再利用。

6. 发明授权

US5052451A Dust control apparatus 失效
标题翻译：防尘设备
公开(公告)号：US5052451A
公开(公告)日：1991-10-01
申请号：US661509
申请日：1991-02-26
申请人： Michael J. Gentilcore , David G. Mock
发明人： Michael J. Gentilcore , David G. Mock
IPC分类号： B65B1/28
CPC分类号： B65B1/28
摘要： A dust control apparatus having a cover member lowerable into an opening of a container, the cover member having a radially expandable seal for sealing the opening, the cover member having a passage therethrough adapted to receive a conduit, the cover member being operable in telescoping relation to the conduit and the passage being sufficiently larger than the conduit for the passage of air between the cover member and conduit, the cover member being movable laterally relative to the conduit to enable the cover member to be lowered into a container which is not precisely aligned therewith, a filter sleeve having a lower end attached to the cover member and an upper end attached to the conduit, the filter sleeve being adapted to prevent the escape of dust from the space between the cover member and conduit, the filter sleeve being protected by the conduit from damage caused by materials flowing through the conduit, the apparatus including an optional fume collecting annulus locatable in surrounding relation to the filter sleeve for collecting and exhausting gases and fumes collected thereby, and an optional inlet port for introducing inert gases or pressurized air to the apparatus.
摘要翻译：一种防尘装置，具有能够容纳在容器的开口中的盖构件，所述盖构件具有用于密封所述开口的可径向扩张的密封件，所述盖构件具有适于容纳导管的通道，所述盖构件可伸缩地操作导管和通道足够大于用于使盖构件和导管之间的空气通过的管道，盖构件可相对于管道横向移动，以使覆盖构件能够降低到不精确对准的容器中其中，过滤套筒具有附接到盖构件的下端和附接到导管的上端，过滤套筒适于防止灰尘从盖构件和导管之间的空间逸出，过滤器套筒受到保护该管道由于材料流经导管而造成损坏，该设备包括可选的烟雾收集环，与过滤器套筒相关联，用于收集和排出由此收集的气体和烟雾，以及用于将惰性气体或加压空气引入到设备的可选入口。

7. 发明授权

US08420857B2 Removal of silica from water soluble compounds by nanofiltration and reverse phase chromatography 有权
标题翻译：通过纳滤和反相色谱从水溶性化合物中除去二氧化硅
公开(公告)号：US08420857B2
公开(公告)日：2013-04-16
申请号：US12675130
申请日：2008-08-21
申请人： Allan R. Bailey , David H. White , Derick L. Kaspar , Robert E. Vandas , Michael J. Gentilcore , Hung V. Nguyen , Anna K. Fukunaga
发明人： Allan R. Bailey , David H. White , Derick L. Kaspar , Robert E. Vandas , Michael J. Gentilcore , Hung V. Nguyen , Anna K. Fukunaga
IPC分类号： C07C231/24
CPC分类号： B01D61/027 , A61K49/0433 , A61K49/103 , A61K49/106 , B01D15/325 , B01D2315/16
摘要： A process for separating soluble silica species such as monomeric silicic acid (or monosilicic acid) and low molecular weight soluble polymeric silica from impure water soluble compounds by membrane nanofiltration is provided. A process for separating soluble silica species and colloidal silica from impure water soluble compounds by reverse phase liquid chromatography is also provided.
摘要翻译：提供了通过膜纳滤法从不纯的水溶性化合物中分离可溶性二氧化硅物质例如单体硅酸（或单硅酸）和低分子量可溶性聚合二氧化硅的方法。还提供了通过反相液相色谱从可溶性水溶性化合物中分离可溶性二氧化硅物质和胶体二氧化硅的方法。

8. 发明申请

US20080188680A1 Process Improvement Using Solubility Characteristics 审中-公开
标题翻译：使用溶解度特征的工艺改进
公开(公告)号：US20080188680A1
公开(公告)日：2008-08-07
申请号：US11817263
申请日：2006-02-21
申请人： Michael J. Gentilcore
发明人： Michael J. Gentilcore
IPC分类号： C07C205/04 , C07C63/04
CPC分类号： C07C201/12 , C07C205/57
摘要： The present invention is directed to a process of maximizing the solubility of a nonelectrolyte solute in a solvent by operating within an optimal temperature range at conditions wherein the nonelectrolyte solute is not a pure liquid. In particular, the process of the present invention is directed to conversion of a carboxylic acid compound to an ester under conditions wherein the solubility of the ester in an alcoholic solvent approaches ideal solubility behavior.
摘要翻译：本发明涉及通过在非电解质溶质不是纯液体的条件下在最佳温度范围内操作使非电解质溶质在溶剂中的溶解度最大化的方法。特别地，本发明的方法涉及在酯在醇类溶剂中的溶解度达到理想的溶解行为的条件下将羧酸化合物转化为酯。

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