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1. 发明授权

US08182574B2 Metal fine particles, composition containing the same, and production method for producing metal fine particles 有权
标题翻译：金属微粒，含有它们的组合物和金属微粒的制造方法
公开(公告)号：US08182574B2
公开(公告)日：2012-05-22
申请号：US12730776
申请日：2010-03-24
申请人： Yoshiaki Takata , Hiroki Hirata , Jun-etsu Satoh , Yasuro Niidome , Sunao Yamada , Koji Nishioka , Hideya Kawasaki , Daigou Mizoguchi , Masanori Nagai , Masato Murouchi , Masaoki Ishihara
发明人： Yoshiaki Takata , Hiroki Hirata , Jun-etsu Satoh , Yasuro Niidome , Sunao Yamada , Koji Nishioka , Hideya Kawasaki , Daigou Mizoguchi , Masanori Nagai , Masato Murouchi , Masaoki Ishihara
IPC分类号： B22F9/24
CPC分类号： B22F9/24 , B22F1/0025 , B22F2999/00 , B82Y30/00 , C22C5/02 , C23C24/00 , C23C24/08 , Y10S977/899 , B22F1/0088 , B22F1/0085
摘要： The present invention provides metal fine particles which have selective wavelength absorption characteristics in a wavelength region from visible light to near infrared light, and have sharp absorption characteristics, and influences little the surrounding wavelength, and therefore, they yield tones having high chroma. The present invention provides metal fine particles wherein an aspect ratio is in a range from 1.1 to 8.0, a maximum absorption wavelength in plasmon absorption is in a range from 400 nm to 1,200 nm, and an absorption coefficient at a peak position of the maximum absorption wavelength is in a range from 6,000 to 20,000 L/mol·cm (measurement concentration: 1.6×10−4 mol/L, and solvent: water).
摘要翻译：本发明提供在从可见光到近红外光的波长区域中具有选择性波长吸收特性的金属微粒，并且具有尖锐的吸收特性，并且影响周围波长很小，因此它们产生色度高的色调。本发明提供金属细颗粒，其中纵横比在1.1至8.0的范围内，等离子体激元吸收中的最大吸收波长在400nm至1200nm的范围内，并且在最大吸收峰峰位置处的吸收系数波长在6000〜20,000L / mol·cm（测定浓度：1.6×10 -4 mol / L，溶剂：水）的范围内。

2. 发明授权

US07976609B2 Method for manufacturing metal nanorods and use thereof 有权
标题翻译：金属纳米棒的制造方法及其用途
公开(公告)号：US07976609B2
公开(公告)日：2011-07-12
申请号：US12704364
申请日：2010-02-11
申请人： Yasuro Niidome , Sunao Yamada , Koji Nishioka , Hideya Kawasaki , Hiroki Hirata , Daigou Mizoguchi , Yoshiaki Takata , Jun-etsu Satoh , Masaoki Ishihara , Masanori Nagai , Masato Murouchi
发明人： Yasuro Niidome , Sunao Yamada , Koji Nishioka , Hideya Kawasaki , Hiroki Hirata , Daigou Mizoguchi , Yoshiaki Takata , Jun-etsu Satoh , Masaoki Ishihara , Masanori Nagai , Masato Murouchi
IPC分类号： B22F9/24 , B82B3/00
CPC分类号： B22F1/0025 , B22F9/24 , B22F2999/00 , B82Y30/00 , C30B7/00 , C30B7/14 , C30B29/605 , Y10S977/762 , Y10S977/896 , B22F2202/11
摘要： A method for manufacturing metal nanorods includes: a step of adding a reducing agent to a metallic salt solution; a step of radiating light into the metallic salt solution containing the reducing agent; and a step of leaving the light-radiated metallic salt solution containing the reducing agent stationary in a dark place so as to grow metal nanorods. Metal nanorods can be also grown by forming a mixed solution by fractionating the above light-radiated metallic salt solution and mixing the fractionated metallic salt solution into a non-radiated metallic salt solution containing the reducing agent, or mixing a non-radiated metallic salt solution and the reducing agent into the above light-radiated metallic salt solution; and leaving the mixed solution stationary in a dark place so as to grow metal nanorods.
摘要翻译：金属纳米棒的制造方法包括：向金属盐溶液中添加还原剂的工序; 将光照射到含有还原剂的金属盐溶液中的步骤; 以及将含有还原剂的光照射的金属盐溶液静置在黑暗处，以便生长金属纳米棒的步骤。金属纳米棒也可以通过将上述光照的金属盐溶液分级分离并将分级的金属盐溶液混合到含有还原剂的非辐射金属盐溶液中，或混合未辐射的金属盐溶液并将还原剂加入上述光照金属盐溶液中; 并将混合溶液静置在黑暗的地方，以便生长金属纳米棒。

3. 发明申请

US20100229684A1 METAL FINE PARTICLES, COMPOSITION CONTAINING THE SAME, AND PRODUCTION METHOD FOR PRODUCING METAL FINE PARTICLES 有权
标题翻译：金属微粒，含有它们的组合物，以及生产金属微粒的生产方法
公开(公告)号：US20100229684A1
公开(公告)日：2010-09-16
申请号：US12730776
申请日：2010-03-24
申请人： Yoshiaki Takata , Hiroki Hirata , Jun-etsu Satoh , Yasuro Niidome , Sunao Yamada , Koji Nishioka , Hideya Kawasaki , Daigou Mizoguchi , Masanori Nagai , Masato Murouchi , Masaoki Ishihara
发明人： Yoshiaki Takata , Hiroki Hirata , Jun-etsu Satoh , Yasuro Niidome , Sunao Yamada , Koji Nishioka , Hideya Kawasaki , Daigou Mizoguchi , Masanori Nagai , Masato Murouchi , Masaoki Ishihara
IPC分类号： B22F9/18 , C25D1/00
CPC分类号： B22F9/24 , B22F1/0025 , B22F2999/00 , B82Y30/00 , C22C5/02 , C23C24/00 , C23C24/08 , Y10S977/899 , B22F1/0088 , B22F1/0085
摘要： The present invention provides metal fine particles which have selective wavelength absorption characteristics in a wavelength region from visible light to near infrared light, and have sharp absorption characteristics, and influences little the surrounding wavelength, and therefore, they yield tones having high chroma. The present invention provides metal fine particles wherein an aspect ratio is in a range from 1.1 to 8.0, a maximum absorption wavelength in plasmon absorption is in a range from 400 nm to 1,200 nm, and an absorption coefficient at a peak position of the maximum absorption wavelength is in a range from 6,000 to 20,000 L/mol·cm (measurement concentration: 1.6×10−4 mol/L, and solvent: water).
摘要翻译：本发明提供在从可见光到近红外光的波长区域中具有选择性波长吸收特性的金属微粒，并且具有尖锐的吸收特性，并且影响周围波长很小，因此它们产生色度高的色调。本发明提供金属细颗粒，其中纵横比在1.1至8.0的范围内，等离子体激元吸收中的最大吸收波长在400nm至1200nm的范围内，并且在最大吸收峰峰位置处的吸收系数波长在6000〜20,000L / mol·cm（测定浓度：1.6×10 -4 mol / L，溶剂：水）的范围内。

4. 发明授权

US06329490B1 Polyhedral organosilicon compound and method for producing the same 有权
标题翻译：多面体有机硅化合物及其制备方法
公开(公告)号：US06329490B1
公开(公告)日：2001-12-11
申请号：US09540285
申请日：2000-03-31
申请人： Yukiya Yamashita , Kenji Hayashi , Masaoki Ishihara
发明人： Yukiya Yamashita , Kenji Hayashi , Masaoki Ishihara
IPC分类号： C08G7724
CPC分类号： C08G77/045 , C08G77/22 , C08G77/24
摘要： Disclosed are polyhedral organosilicon compounds which are possible to be polymerized and can form a film excellent in adhesiveness to a substrate, having a high hardness, a high transparency and having water and oil repellency, and comprise organofluoro groups or both of organofluoro groups and reactive functional groups, the compounds being soluble in an organic solvent and stable. Organosilicon compounds which have perfluoroalkyl groups or both perfluoroalkyl groups and reactive functional groups and which have a polyhedral structure have the following formulas of (I), (II) and (III): [Rf1—X1—(CH2)a—SiO1.5]m (I) [Rf1—X1—(CH2)a—SiO1.5]m[Rf2—(X2)c—(CH2)b—SiO1.5]n (II) [Rf1—X1—(CH2)a—SiO1.5]m[R—(X2)c—(CH2)b—SiO1.5]n (III) wherein each of Rf1 and Rf2 represents a perfluoroalkyl group, R represents a functional group, each of X1 and X2 represents a divalent bonding group, each of a and b represents 0 or an integer of up to 10, c represents 0 or 1, each of m and n represents an integer of 1 to 19 and m+n is an integer of 4 to 20.
摘要翻译：公开了可能聚合的多面体有机硅化合物，并且可以形成具有高硬度，高透明度和具有拒水拒油性的基材粘附性优异的膜，并且包含有机氟基团或有机氟基团和反应性官能团所述化合物可溶于有机溶剂并稳定。具有全氟烷基或全氟烷基和反应性官能团两者并具有多面体结构的有机硅化合物具有下式（I），（II）和（III）：其中，Rf1和Rf2各自表示全氟烷基，R表示官能团，X1和X2各自表示二价键合基，a和b各自表示0或10以下的整数，c表示0或1， m表示1〜19的整数，m + n表示4〜20的整数。

5. 发明授权

US5504133A Composition for forming conductive films 失效
标题翻译：用于形成导电膜的组合物
公开(公告)号：US5504133A
公开(公告)日：1996-04-02
申请号：US317363
申请日：1994-10-04
申请人： Masato Murouchi , Toshiharu Hayashi , Akira Nishihara , Masaoki Ishihara
发明人： Masato Murouchi , Toshiharu Hayashi , Akira Nishihara , Masaoki Ishihara
IPC分类号： C08K3/22 , C09D5/24 , G03G5/10 , H01B1/20 , H01L31/18 , C08K3/20 , H01B1/02
CPC分类号： H01L31/1884 , C08K3/22 , C09D5/24 , G03G5/104 , H01B1/20 , Y02E10/50 , Y10T428/256 , Y10T428/31797 , Y10T428/31902
摘要： A composition for forming transparent conductive films comprises a tin-containing indium oxide (ITO) powder dispersed in a binder solution. The binder solution comprises a mixed organic solvent consisting of at least one polar solvent and at least one non-polar solvent, in which a polymer having a weight-average molecular weight of from 8,000 to 150,000 is dissolved. The polymer contains (a) an acidic functional group in such a proportion that the polymer has an acid number of from 0.5 to 15 mg-KOH/g, or (b) a polyalkylene glycol chain in a proportion of from 0.5% to 40% by weight, or both of (a) and (b) in the molecule. Alternatively, the binder solution comprises an actinic radiation-curable binder, which comprises an acrylate or methacrylate compound containing an acid phosphate group in the molecule. The composition can form, by coating, a transparent conductive film having improved electrical and optical properties.
摘要翻译：用于形成透明导电膜的组合物包括分散在粘合剂溶液中的含锡氧化铟（ITO）粉末。粘合剂溶液包含由至少一种极性溶剂和至少一种非极性溶剂组成的混合有机溶剂，其中溶解了重均分子量为8,000至150,000的聚合物。聚合物包含（a）酸性官能团，其比例为聚合物的酸值为0.5-15mg-KOH / g，或（b）聚亚烷基二醇链的比例为0.5％至40％，或分子中的（a）和（b）两者。或者，粘合剂溶液包含光化学辐射固化粘合剂，其包含在分子中含有酸式磷酸酯基团的丙烯酸酯或甲基丙烯酸酯化合物。该组合物可以通过涂覆形成具有改善的电学和光学性质的透明导电膜。

6. 发明申请

US20100143184A1 METHOD FOR MANUFACTURING METAL NANORODS AND USE THEREOF 有权
标题翻译：制造金属纳米体的方法及其用途
公开(公告)号：US20100143184A1
公开(公告)日：2010-06-10
申请号：US12704364
申请日：2010-02-11
申请人： Yasuro Niidome , Sunao Yamada , Koji Nishioka , Hideya Kawasaki , Hiroki Hirata , Daigou Mizoguchi , Yoshiaki Takata , Jun-etsu Satoh , Masaoki Ishihara , Masanori Nagai , Masato Murouchi
发明人： Yasuro Niidome , Sunao Yamada , Koji Nishioka , Hideya Kawasaki , Hiroki Hirata , Daigou Mizoguchi , Yoshiaki Takata , Jun-etsu Satoh , Masaoki Ishihara , Masanori Nagai , Masato Murouchi
IPC分类号： B22F9/16 , C22C5/02
CPC分类号： B22F1/0025 , B22F9/24 , B22F2999/00 , B82Y30/00 , C30B7/00 , C30B7/14 , C30B29/605 , Y10S977/762 , Y10S977/896 , B22F2202/11
摘要： A method for manufacturing metal nanorods includes: a step of adding a reducing agent to a metallic salt solution; a step of radiating light into the metallic salt solution containing the reducing agent; and a step of leaving the light-radiated metallic salt solution containing the reducing agent stationary in a dark place so as to grow metal nanorods. Metal nanorods can be also grown by forming a mixed solution by fractionating the above light-radiated metallic salt solution and mixing the fractionated metallic salt solution into a non-radiated metallic salt solution containing the reducing agent, or mixing a non-radiated metallic salt solution and the reducing agent into the above light-radiated metallic salt solution; and leaving the mixed solution stationary in a dark place so as to grow metal nanorods.
摘要翻译：金属纳米棒的制造方法包括：向金属盐溶液中添加还原剂的工序; 将光照射到含有还原剂的金属盐溶液中的步骤; 以及将含有还原剂的光照射的金属盐溶液静置在黑暗处，以便生长金属纳米棒的步骤。金属纳米棒也可以通过将上述光照的金属盐溶液分级分离并将分级的金属盐溶液混合到含有还原剂的非辐射金属盐溶液中，或混合未辐射的金属盐溶液并将还原剂加入上述光照金属盐溶液中; 并将混合溶液静置在黑暗的地方，以便生长金属纳米棒。

7. 发明授权

US07691176B2 Method for manufacturing metal nanorods and uses thereof 有权
标题翻译：金属纳米棒的制造方法及其用途
公开(公告)号：US07691176B2
公开(公告)日：2010-04-06
申请号：US10556498
申请日：2004-05-13
申请人： Yasuro Niidome , Sunao Yamada , Koji Nishioka , Hideya Kawasaki , Hiroki Hirata , Yoshiaki Takata , Jun-etsu Satoh , Daigou Mizoguchi , Masaoki Ishihara , Masanori Nagai , Masato Murouchi
发明人： Yasuro Niidome , Sunao Yamada , Koji Nishioka , Hideya Kawasaki , Hiroki Hirata , Yoshiaki Takata , Jun-etsu Satoh , Daigou Mizoguchi , Masaoki Ishihara , Masanori Nagai , Masato Murouchi
IPC分类号： B22F9/22 , B01J13/00 , B82B3/00
CPC分类号： B22F1/0025 , B22F9/24 , B22F2999/00 , B82Y30/00 , C30B7/00 , C30B7/14 , C30B29/605 , Y10S977/762 , Y10S977/896 , B22F2202/11
摘要： A method for manufacturing metal nanorods includes: a step of adding a reducing agent to a metallic salt solution; a step of radiating light into the metallic salt solution containing the reducing agent; and a step of leaving the light-radiated metallic salt solution containing the reducing agent stationary in a dark place so as to grow metal nanorods. Metal nanorods can be also grown by forming a mixed solution by fractionating the above light-radiated metallic salt solution and mixing the fractionated metallic salt solution into a non-radiated metallic salt solution containing the reducing agent, or mixing a non-radiated metallic salt solution and the reducing agent into the above light-radiated metallic salt solution; and leaving the mixed solution stationary in a dark place so as to grow metal nanorods.
摘要翻译：金属纳米棒的制造方法包括：向金属盐溶液中添加还原剂的工序; 将光照射到含有还原剂的金属盐溶液中的步骤; 以及将含有还原剂的光照射的金属盐溶液静置在黑暗处，以便生长金属纳米棒的步骤。金属纳米棒也可以通过将上述光照的金属盐溶液分级分离并将分级的金属盐溶液混合到含有还原剂的非辐射金属盐溶液中，或混合未辐射的金属盐溶液并将还原剂加入上述光照金属盐溶液中; 并将混合溶液静置在黑暗的地方，以便生长金属纳米棒。

8. 发明申请

US20060266157A1 Metal fine particles, composition containing the same, and production method for producing metal fine particles 审中-公开
标题翻译：金属微粒，含有它们的组合物和金属微粒的制造方法
公开(公告)号：US20060266157A1
公开(公告)日：2006-11-30
申请号：US10570523
申请日：2004-09-02
申请人： Yoshiaki Takata , Hiroki Hirata , Jun-etsu Satoh , Yasuro Niidome , Sunao Yamada , Koji Nishioka , Hideya Kawasaki , Daigou Mizoguchi , Masanori Nagai , Masato Murouchi , Masaoki Ishihara
发明人： Yoshiaki Takata , Hiroki Hirata , Jun-etsu Satoh , Yasuro Niidome , Sunao Yamada , Koji Nishioka , Hideya Kawasaki , Daigou Mizoguchi , Masanori Nagai , Masato Murouchi , Masaoki Ishihara
IPC分类号： B22F9/24 , C22C5/02
CPC分类号： B22F9/24 , B22F1/0025 , B22F2999/00 , B82Y30/00 , C22C5/02 , C23C24/00 , C23C24/08 , Y10S977/899 , B22F1/0088 , B22F1/0085
摘要： The present invention provides metal fine particles which have selective wavelength absorption characteristics in a wavelength region from visible light to near infrared light, and have sharp absorption characteristics, and influences little the surrounding wavelength, and therefore, they yield tones having high chroma. The present invention provides metal fine particles wherein an aspect ratio is in a range from 1.1 to 8.0, a maximum absorption wavelength in plasmon absorption is in a range from 400 nm to 1,200 nm, and an absorption coefficient at a peak position of the maximum absorption wavelength is in a range from 6,000 to 20,000 L/mol·cm (measurement concentration: 1.6×10−4 mol/L, and solvent:water).
摘要翻译：本发明提供在从可见光到近红外光的波长区域中具有选择性波长吸收特性的金属微粒，并且具有尖锐的吸收特性，并且影响周围波长很小，因此它们产生色度高的色调。本发明提供金属细颗粒，其中纵横比在1.1至8.0的范围内，等离子体激元吸收中的最大吸收波长在400nm至1200nm的范围内，并且在最大吸收峰峰位置处的吸收系数波长在6000至20,000L / mol.cm（测量浓度：1.6×10 -4 mol / L）和溶剂：水的范围内。

9. 发明申请

US20060196309A1 Method for manufacturing metal nanorods and use thereof 有权
标题翻译：金属纳米棒的制造方法及其用途
公开(公告)号：US20060196309A1
公开(公告)日：2006-09-07
申请号：US10556498
申请日：2004-05-13
申请人： Yasuro Niidome , Sunao Yamada , Koji Nishioka , Hideya Kawasaki , Hiroki Hirata , Yoshiaki Takata , Jun-etsu Satoh , Daigou Mizoguchi , Masaoki Ishihara , Masanori Nagai , Masato Murouchi
发明人： Yasuro Niidome , Sunao Yamada , Koji Nishioka , Hideya Kawasaki , Hiroki Hirata , Yoshiaki Takata , Jun-etsu Satoh , Daigou Mizoguchi , Masaoki Ishihara , Masanori Nagai , Masato Murouchi
IPC分类号： B22F9/24
CPC分类号： B22F1/0025 , B22F9/24 , B22F2999/00 , B82Y30/00 , C30B7/00 , C30B7/14 , C30B29/605 , Y10S977/762 , Y10S977/896 , B22F2202/11
摘要： A method for manufacturing metal nanorods includes: a step of adding a reducing agent to a metallic salt solution; a step of radiating light into the metallic salt solution containing the reducing agent; and a step of leaving the light-radiated metallic salt solution containing the reducing agent stationary in a dark place so as to grow metal nanorods. Metal nanorods can be also grown by forming a mixed solution by fractionating the above light-radiated metallic salt solution and mixing the fractionated metallic salt solution into a non-radiated metallic salt solution containing the reducing agent, or mixing a non-radiated metallic salt solution and the reducing agent into the above light-radiated metallic salt solution; and leaving the mixed solution stationary in a dark place so as to grow metal nanorods.
摘要翻译：金属纳米棒的制造方法包括：向金属盐溶液中添加还原剂的工序; 将光照射到含有还原剂的金属盐溶液中的步骤; 以及将含有还原剂的光照射的金属盐溶液静置在黑暗处，以便生长金属纳米棒的步骤。金属纳米棒也可以通过将上述光照的金属盐溶液分级分离并将分级的金属盐溶液混合到含有还原剂的非辐射金属盐溶液中，或混合未辐射的金属盐溶液并将还原剂加入上述光照金属盐溶液中; 并将混合溶液静置在黑暗的地方，以便生长金属纳米棒。

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