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1. 发明授权

US4071347A Novel composition for use in agriculture as soil improvers and fertilizers and process for their production 失效
标题翻译：用于农业的新型组合物，作为土壤改良剂和肥料及其生产过程
公开(公告)号：US4071347A
公开(公告)日：1978-01-31
申请号：US631275
申请日：1975-11-12
申请人： Luigi Piccolo , Benedetto Calcagno , Marcello Ghirga , Antonio Paolinelli
发明人： Luigi Piccolo , Benedetto Calcagno , Marcello Ghirga , Antonio Paolinelli
IPC分类号： C09K17/00 , C05C3/00 , C05D9/02 , C05G1/00 , C05G3/00 , C09K17/02 , C09K101/00
CPC分类号： C05C3/00 , C09K17/04
摘要： Novel compositions for use in agriculture as soil improvers and fertilizers comprising as essential components ammonium sulfate and ferric oxide hydrate. By-products obtained in the production of titanium dioxide from ilmenite or ilmenite slag in the sulfate process and substantially consisting of ferrous sulfate heptahydrate are reacted with ammonia and that the reaction product obtained, consisting substantially of ammonium sulfate and ferrous hydrate, is subsequently oxidized until a composition is obtained which substantially consists of ammonium sulfate and ferric oxide hydrate.
摘要翻译：用于农业的新型组合物作为土壤改良剂和肥料，其包含作为必需组分的硫酸铵和氧化铁水合物。在硫酸盐工艺中由钛铁矿或钛铁矿矿渣生产二氧化钛，并且基本上由七水硫酸亚铁组成的副产物与氨反应，并且基本上由硫酸铵和水合铁形成的反应产物随后被氧化直到获得了基本上由硫酸铵和氧化铁水合物组成的组合物。

2. 发明授权

US4021533A Manufacture of titanium dioxide by the sulphate process using nuclei formed by steam hydrolysis of TiCl.sub.4 失效
标题翻译：通过硫酸盐工艺制造二氧化钛，使用通过TiCl的蒸汽水解形成的核（hd 4
公开(公告)号：US4021533A
公开(公告)日：1977-05-03
申请号：US617954
申请日：1975-09-29
申请人： Luigi Piccolo , Marcello Ghirga , Antonio Paolinelli
发明人： Luigi Piccolo , Marcello Ghirga , Antonio Paolinelli
IPC分类号： C01G23/04 , C01G23/047 , C01G23/053 , C01G23/07
CPC分类号： C01G23/047 , C01G23/0534 , C01P2004/32 , C01P2004/50 , C01P2004/62 , C01P2006/22 , C01P2006/60
摘要： A solution of active nuclei for the hydrolysis of titanium sulphate and for the rutilisation of titanium dioxide in the manufacture of titanium dioxide in tutile form in the method via sulphate is prepared by transforming titanium tetrachloride into a compound of the formula Ti(OH).sub.x Cl.sub.y, wherein x ranges from 1 to 3, y from 3 to 1 and x + y is equal to 4 by contact with steam in the vapor phase, and contacting the reaction products with an aqueous solution of sodium hydroxide to form an aqueous suspension of titanium hydroxide having a TiO.sub.2 content of from 10 to 30 grams/liter and a pH value of from 3 to 4.
摘要翻译：通过将四氯化钛转化为式Ti（OH）xCly的化合物，制备硫酸钛水解的活性核和二氧化钛在通过硫酸盐的方法中制备二氧化钛在金属络合物中的金红石化的溶液，其中x为1至3，y为3至1，x + y等于4，通过与气相中的蒸汽接触，并使反应产物与氢氧化钠水溶液接触以形成氢氧化钛的水悬浮液 TiO 2含量为10至30克/升，pH值为3至4。

3. 发明授权

US3946068A Process for the production of vinyl acetate from ethylene 失效
标题翻译：从乙烯生产乙酸乙烯酯的方法
公开(公告)号：US3946068A
公开(公告)日：1976-03-23
申请号：US862955
申请日：1969-10-01
申请人： Benedetto Calcagno , Claudio Divo , Marcello Ghirga
发明人： Benedetto Calcagno , Claudio Divo , Marcello Ghirga
IPC分类号： B01J27/06 , C07C67/055 , C07C69/15 , C07C67/04
CPC分类号： B01J27/06 , C07C67/055 , Y02P20/584
摘要： The palladium and copper ethylene-oxidation catalysts used in vinyl acetate production are regenerated by a process including a galvanic displacement of the metals from solution and their reconversion to halides.
摘要翻译：用于乙酸乙烯酯生产中的钯和铜乙烯 - 氧化催化剂通过包括从溶液中电离位移金属及其再转化成卤化物的方法再生。

4. 发明授权

US4388223A Catalyst for the conversion of unsaturated hydrocarbons into diolefins or unsaturated aldehydes and nitriles, and process for preparing the same 失效
标题翻译：用于将不饱和烃转化为二烯烃或不饱和醛和腈的催化剂及其制备方法
公开(公告)号：US4388223A
公开(公告)日：1983-06-14
申请号：US251434
申请日：1981-04-06
申请人： Natale Ferlazzo , Natale Bertolini , Marcello Ghirga
发明人： Natale Ferlazzo , Natale Bertolini , Marcello Ghirga
IPC分类号： C07C57/05 , B01J23/28 , B01J23/34 , B01J23/88 , B01J27/057 , B01J27/19 , B01J27/195 , B01J27/198 , B01J27/199 , C07B35/04 , C07B61/00 , C07C1/00 , C07C5/333 , C07C5/48 , C07C11/00 , C07C11/12 , C07C45/00 , C07C45/34 , C07C45/35 , C07C47/21 , C07C47/22 , C07C51/00 , C07C57/07 , C07C67/00 , C07C253/00 , C07C255/08 , C07C255/51 , B01J23/10 , B01J23/86
CPC分类号： B01J23/8872 , B01J23/28 , B01J23/887 , B01J23/8871 , B01J23/8876 , B01J23/8878 , C07C253/26 , C07C253/28 , Y02P20/52
摘要： The catalyst comprises one or more molybdates of trivalent metals chosen from Fe, Al, Ce and Cr and/or molybdates of bivalent metals chosen from alpha manganese molybdate, beta cobalt molybdate, beta nickel molybdate and the molybdates of Zn, Mg and Ca, and one or more promoter elements chosen from Se, Te, As, Sb, V, Nb, Sn, Pb and Tl homogeneously distributed within the crystalline structure of said molybdates with distortion thereof without creating new crystalline phases.
摘要翻译：催化剂包含一种或多种选自Fe，Al，Ce和Cr的三价金属钼酸盐和/或选自钼酸锰钼，钼酸钼钴，β钼酸镍和Zn，Mg和Ca的钼酸盐的二价金属钼酸盐，和选自Se，Te，As，Sb，V，Nb，Sn，Pb和Tl的一种或多种助催化剂元素均匀地分布在所述钼酸盐的晶体结构中，同时具有变形，而不产生新的结晶相。

5. 发明授权

US4343957A Process for the production of cumene 失效
标题翻译：异丙苯生产工艺
公开(公告)号：US4343957A
公开(公告)日：1982-08-10
申请号：US218333
申请日：1980-12-19
申请人： Emanuele Sartorio , Benedetto Calcagno , Fulvio Trombetti , Marcello Ghirga
发明人： Emanuele Sartorio , Benedetto Calcagno , Fulvio Trombetti , Marcello Ghirga
IPC分类号： C07C2/70 , C07C2/68
CPC分类号： C07C2/70 , C07C2527/173
摘要： Production of cumene by alkylation of benzene with propylene on a solid phosphoric acid catalyst, using in a first step a plurality of catalyst beds in series and in a second step a single catalyst bed, using an overall benzene/propylene molar ratio of at least 5:1, continuously delivering the benzene to the first bed, continuously delivering a series of streams of liquid propylene respectively to the first bed and, in the form of a cold stream, between each pair of contiguous beds, and carrying out a partial recycle of reaction products of the second step as a cold stream between the first and the second step, and using a benzene/propylene molar ratio higher than 13:1 at the inlet of each bed of the first step, and higher than 25:1 at the inlet of the bed of the second step.
摘要翻译：通过在固体磷酸催化剂上用丙烷烷基化苯来生产枯烯，在第一步中使用多个催化剂床串联，在第二步中使用单一催化剂床，使用总苯/丙烯摩尔比为至少5 ：1，连续地将苯输送到第一床，连续地将一系列液态丙烯流分别连续地输送到第一床，并以冷流的形式在每对连续的床之间进行，并进行部分循环在第一步骤和第二步骤之间的第二步骤的反应产物作为冷流，并且在第一步骤的每个床的入口处使用高于13:1的苯/丙烯摩尔比，并且在第第二步床的入口。

6. 发明授权

US4167548A Process for the manufacture of a microfibrous pulp suitable for making synthetic paper 失效
标题翻译：用于制造适合制造合成纸的微纤维纸浆的方法
公开(公告)号：US4167548A
公开(公告)日：1979-09-11
申请号：US518117
申请日：1974-10-25
申请人： Guido Arduini , Marcello Ghirga , Gaspare Renda
发明人： Guido Arduini , Marcello Ghirga , Gaspare Renda
IPC分类号： D01F6/04 , D01D5/11 , D04H1/04 , D21H13/14 , B22D23/08
CPC分类号： D01D5/11
摘要： A microfibrous pulp suitable for use in the manufacture of synthetic paper is prepared by forming an aqueous emulsion of a solution in an organic solvent of olefinic homopolymers and copolymers and copolymers of at least one olefinic monomer with at least one further monomer copolymerizable therewith, heating the emulsion above the melting point of the polymers and spraying emulsion into a zone of expansion in which water and the organic solvent are evaporated. The hot emulsion is sprayed in the form of a tubular jet in the cavity of which a stream of inert gas is injected to spread the jet transversally in the zone of expansion.
摘要翻译：通过在烯烃均聚物和共聚物的有机溶剂中形成溶液的水性乳液和至少一种烯属单体与至少一种可与其共聚的其它单体的共聚物和共聚物来制备适用于制造合成纸的微纤维浆，加热乳液高于聚合物的熔点并将乳液喷射到其中水和有机溶剂蒸发的膨胀区域中。将热乳液以管状射流的形式喷射在空腔中，其中注入惰性气体流，以在扩张区域横向扩散射流。

7. 发明授权

US3956376A Process for the production of acrolein and acrylic acid 失效
标题翻译：制备丙烯醛和丙烯酸的方法
公开(公告)号：US3956376A
公开(公告)日：1976-05-11
申请号：US420344
申请日：1973-11-29
申请人： Natale Ferlazzo , Gian Fausto Buzzi , Marcello Ghirga
发明人： Natale Ferlazzo , Gian Fausto Buzzi , Marcello Ghirga
IPC分类号： C07C57/05 , B01J23/84 , B01J23/88 , B01J27/057 , C07C27/00 , C07C27/14 , C07C45/00 , C07C45/35 , C07C47/22 , C07C51/00 , C07C51/25 , C07C57/055 , C07C67/00 , C07C51/26
CPC分类号： C07C45/35 , B01J23/84 , B01J23/88 , B01J27/0576 , C07C51/252 , B01J2523/00
摘要： An improved process for the production of acrolein from propylene and of acrylic acid from propylene or acrolein or mixtures of propylene and acrolein which essentially comprises catalytic oxidation of propylene and/or acrolein with oxygen or a gas containing molecular oxygen in the presence of an oxidation catalyst and of methanol in a quantity of from 0.01 to 1% by volume with respect to the total gaseous mixture of the reactants. Acrolein and acrylic acid are formed in the process at high conversion rates and selectivities.
摘要翻译：用于由丙烯和丙烯酸从丙烯或丙烯醛或丙烯和丙烯醛的混合物制备丙烯醛的改进方法，其基本上包括丙烯和/或丙烯醛与氧或含有分子氧的气体在氧化催化剂存在下的催化氧化和相对于反应物的总气体混合物的体积的0.01至1体积％的甲醇。在高转化率和选择性的过程中形成丙烯醛和丙烯酸。

8. 发明授权

US4324941A Process for the production of cumene 失效
标题翻译：异丙苯生产工艺
公开(公告)号：US4324941A
公开(公告)日：1982-04-13
申请号：US225220
申请日：1981-01-15
申请人： Marcello Ghirga , Luigi Valtorta , Benedetto Calcagno
发明人： Marcello Ghirga , Luigi Valtorta , Benedetto Calcagno
IPC分类号： C07C2/70 , C07C2/68
CPC分类号： C07C2/70 , C07C2527/173
摘要： Cumene is prepared by alkylation of benzene with propylene in the presence of a solid phosphoric acid catalyst in a continuous process by delivering liquid benzene and liquid propylene in a molar ratio lower than 6:1, to a liquid reaction medium consisting essentially of benzene and cumene and containing the catalyst, while maintaining the temperature and composition of said medium substantially uniform in each point, operating at 170.degree.-280.degree. C. and in the liquid phase, and with a contact time higher than about 0.4 hours, expressed as the ratio between volume of catalyst and hourly volume of reagents fed in.
摘要翻译：通过在固体磷酸催化剂存在下，通过将液体苯和低于6:1的摩尔比的液体丙烯输送到基本上由苯和异丙基苯组成的液体反应介质，将苯与丙烯烷基化，并含有催化剂，同时保持所述介质的温度和组成在每个点上基本上均匀，在170℃-280℃和液相下操作，接触时间高于约0.4小时，以比例催化剂体积和加入的试剂的小时体积。

9. 发明授权

US4058389A Process for the preparation of fertilizers and soil modifiers 失效
标题翻译：化肥和土壤改良剂的制备过程
公开(公告)号：US4058389A
公开(公告)日：1977-11-15
申请号：US785706
申请日：1977-04-07
申请人： Luigi Piccolo , Marcello Ghirga , Antonio Paolinelli , Gian Pietro Paganessi
发明人： Luigi Piccolo , Marcello Ghirga , Antonio Paolinelli , Gian Pietro Paganessi
IPC分类号： C01C1/24 , C05D9/02 , C05D9/00 , C01C1/244 , C01G49/02
CPC分类号： C05D9/02 , C01C1/24 , Y10S71/903
摘要： A soil modifying composition and a concentrated solution of ammonium sulphate with a high purity degree are obtained from by-products consisting essentially of ferrous sulphate heptahydrate, obtained in the production of titanium dioxide from ilmenites by the sulphate process, by contacting solid particles of said by-products with gaseous ammonia, lixiviating the resulting product with water, thereby to recover said concentrated solution of ammonium sulphate, the dried residual solid yielding said soil modifying composition.
摘要翻译：通过硫酸盐法从钛铁矿生产二氧化钛得到的基本上由硫酸亚铁七水合物组成的副产物得到土壤改良组合物和浓度高的硫酸铵溶液， - 用气态氨产物，将所得产物与水混合，从而回收所述浓硫酸铵溶液，干燥的残余固体产生所述土壤改性组合物。

10. 发明授权

US3989742A Process for the production of vinyl acetate from ethylene 失效
标题翻译：从乙烯生产乙酸乙烯酯的方法
公开(公告)号：US3989742A
公开(公告)日：1976-11-02
申请号：US862913
申请日：1969-10-01
申请人： Benedetto Calcagno , Claudio Divo , Marcello Ghirga
发明人： Benedetto Calcagno , Claudio Divo , Marcello Ghirga
IPC分类号： B01J27/06 , C07C67/055 , C07C69/15 , C07C67/05
CPC分类号： B01J27/06 , C07C67/055
摘要： The copper and palladium ethylene-oxidation catalyst used in the preparation of vinyl acetate is regenerated in a process including deposition of the metals from solution in a Daniell-type galvanic cell and subsequent reconversion to the halides.
摘要翻译：用于制备乙酸乙烯酯的铜和钯乙烯 - 氧化催化剂在包括从Daniell型原电池中的溶液中沉积金属并随后再转化成卤化物的过程中再生。

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