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1. 发明专利

IL203608A Process for producing toluidine compound 未知
公开(公告)号：IL203608A
公开(公告)日：2014-04-30
申请号：IL20360810
申请日：2010-01-31
申请人： ISHIHARA SANGYO KAISHA , MURAI SHIGEO , YOSHIZAWA HIROSHI , OHSHIMA TAKESHI , MURAKAMI KATSUYOSHI , ANDO TAKAYOSHI , NAKAMURA TADASHI , ADACHI NORIO , ISOGAI AKIHIKO
发明人： MURAI SHIGEO , YOSHIZAWA HIROSHI , OHSHIMA TAKESHI , MURAKAMI KATSUYOSHI , ANDO TAKAYOSHI , NAKAMURA TADASHI , ADACHI NORIO , ISOGAI AKIHIKO
摘要： Because fluazinam is excellent as an active ingredient of pesticides and highly useful, it is desired to produce it efficiently in a proper form with simple operations at low cost in an environmentally friendly manner. The desired product is obtained in good yields with simple operations by using industrially advantageous reaction systems by a process comprising (1) a step of reacting ACTF and DCDNBTF in the presence of an alkali component, a solvent selected from the group consisting of ketones, nitriles, ethers and esters and a sufficient amount of water to substantially dissolve the alkali component, (2) a step of neutralizing or acidifying the reaction mixture with an acid and (3) a step of removing the solvent by distillation from the mixture containing fluazinam as the reaction product and the reaction solvent to precipitate crystals the product.

2. 发明申请

WO2009054210A1 PROCESS FOR PRODUCING TOLUIDINE COMPOUND 审中-公开
标题翻译：生产托洛芬化合物的方法
公开(公告)号：WO2009054210A1
公开(公告)日：2009-04-30
申请号：PCT/JP2008/066797
申请日：2008-09-10
申请人： ISHIHARA SANGYO KAISHA, LTD. , MURAI, Shigeo , YOSHIZAWA, Hiroshi , OHSHIMA, Takeshi , MURAKAMI, Katsuyoshi , ANDO, Takayoshi , NAKAMURA, Tadashi , ADACHI, Norio , ISOGAI, Akihiko
发明人： MURAI, Shigeo , YOSHIZAWA, Hiroshi , OHSHIMA, Takeshi , MURAKAMI, Katsuyoshi , ANDO, Takayoshi , NAKAMURA, Tadashi , ADACHI, Norio , ISOGAI, Akihiko
IPC分类号： C07D213/72
CPC分类号： C07D213/72
摘要： ABSTRACT Because fluazinam is excellent as an active ingredient of pesticides and highly useful, it is desired to produce it efficiently in a proper form with simple operations at low cost in an environmentally friendly manner. The desired product is obtained in good yields with simple operations by using industrially advantageous reaction systems by a process comprising (1) a step of reacting ACTF and DCDNBTF in the presence of an alkali component, a solvent selected from the group consisting of ethers, nitriles and esters, (2) a step of neutralizing or acidifying the reaction mixture with an acid and (3) a step of removing the solvent by distillation from the mixture containing fluazinam as the reaction product and the solvent to precipitate crystals of the product.
摘要翻译：摘要由于氟啶胺作为农药的有效成分非常有用，因而具有很高的用途，所以希望以低成本，环保的方式，以简单的操作，以合适的形式有效地生产。通过使用工业上有利的反应体系，通过以下方法获得所需产物，通过使用工业上有利的反应体系获得所需产物，该方法包括：（1）在碱组分，选自醚，腈的溶剂存在下使ACTF和DCDNBTF反应的步骤和酯，（2）用酸中和或酸化反应混合物的步骤和（3）通过蒸馏从包含氟啶胺作为反应产物和溶剂的混合物中除去溶剂以沉淀产物的晶体的步骤。

3. 发明申请

WO1997041106A1 PYRAZOLE COMPOUNDS, PROCESSES FOR THEIR PRODUCTION AND HERBICIDES CONTAINING THEM 审中-公开
标题翻译：吡咯化合物，含有它们的生产和除草剂的方法
公开(公告)号：WO1997041106A1
公开(公告)日：1997-11-06
申请号：PCT/JP1997001457
申请日：1997-04-25
申请人： ISHIHARA SANGYO KAISHA LTD. , MURAI, Shigeo , KIKUGAWA, Hiroshi , NAKAYAMA, Hitoshi , SANO, Makiko , ISOGAI, Akihiko
发明人： ISHIHARA SANGYO KAISHA LTD.
IPC分类号： C07D231/20
CPC分类号： C07D401/12 , A01N43/56 , C07D231/20
摘要： A pyrazole compound of formula (I) or its salt wherein R1 is an alkyl group, R2 is a hydrogen atom, a methyl group, -A-R3, a phenyl group which may be substituted, a pyridyl group which may be substituted, or an allyl group which is substituted by a phenyl group, A is -SO2-, -CO-, -CH(R6)- or -CH(R7)CO-, R3 is an alkyl group which may be substituted, an alkenyl group which may be substituted, an alkynyl group which may be substituted, an alkoxy group which may be substituted, a cyano group, a dialkylamino group or a phenyl group which may be substituted, each of R6 and R7 is a hydrogen atom or an alkyl group, X is a hydrogen atom, a halogen atom, an alkyl group, a haloalkyl group, an alkoxy group, an alkylthio group, an alkylsulfinyl group, an alkylsulfonyl group, a nitro group, an alkoxycarbonyl group, -SO2N(R8)R9, -N(R10)SO2R11, -CH2S(O)qR12 or -OSO2R13, each of R8, R9, R10, R11, R12 and R13 is an alkyl group, Z is an alkyl group, 1 is an integer of from 0 to 5, n is an integer of from 1 to 5, and q is an integer of from 0 to 2, provided that when 1 is at least 2, a plurality of Z may be the same or different, and when n is at least 2, a plurality of X may be the same or different.
摘要翻译：式（I）的吡唑化合物或其盐，其中R 1为烷基，R 2为氢原子，甲基，-A-R 3，可被取代的苯基，可被取代的吡啶基，或被苯基取代的烯丙基，A是-SO 2 - ， - CO - ， - CH（R 6） - 或-CH（R 7）CO-，R 3是可被取代的烷基，可以被取代，可以被取代的炔基，可以被取代的烷氧基，可以被取代的氰基，二烷基氨基或苯基，R6和R7各自是氢原子或烷基， X是氢原子，卤素原子，烷基，卤代烷基，烷氧基，烷硫基，烷基亚磺酰基，烷基磺酰基，硝基，烷氧基羰基，-SO 2 N（R 8）R 9， N（R 10）SO 2 R 11，-CH 2 S（O）q R 12或-OSO 2 R 13，R8，R9，R10，R11，R12和R13各自为烷基，Z为烷基，1为0〜5的整数， n是fr的整数 o为1〜5，q为0〜2的整数，条件是当1为至少2时，多个Z可以相同或不同，n为2以上时，多个X可以相同或不同

4. 发明申请

WO2009017239A3 PROCESS FOR PRODUCING TOLUIDINE COMPOUND 审中-公开
标题翻译：生产托洛芬化合物的方法
公开(公告)号：WO2009017239A3
公开(公告)日：2009-06-25
申请号：PCT/JP2008063929
申请日：2008-07-29
申请人： ISHIHARA SANGYO KAISHA , MURAI SHIGEO , YOSHIZAWA HIROSHI , OHSHIMA TAKESHI , MURAKAMI KATSUYOSHI , ANDO TAKAYOSHI , NAKAMURA TADASHI
发明人： MURAI SHIGEO , YOSHIZAWA HIROSHI , OHSHIMA TAKESHI , MURAKAMI KATSUYOSHI , ANDO TAKAYOSHI , NAKAMURA TADASHI
IPC分类号： C07D213/74
CPC分类号： C07D213/74
摘要： Because fluazinam is excellent as an active ingredient of pesticides and highly useful, it is desired to produce it efficiently in a proper form with simple operations at low cost in an environmentally friendly manner. The desired product is obtained in good yields with simple operations by using industrially advantageous reaction systems by a process comprising (1) a step of reacting ACTF and DCDNBTF in the presence of an alkali component and a tertiary alcohol as a solvent and (2) a step of neutralizing or acidifying the reaction mixture with an acid.
摘要翻译：由于氟啶胺作为农药的有效成分是优异的，而且是非常有用的，因此希望能以低成本的环境友好的方式以简单的操作以适当的形式有效地生产。通过使用工业上有利的反应体系，通过使用（1）在碱组分和叔醇作为溶剂的存在下使ACTF和DCDNBTF反应的步骤，和（2）一种用酸中和或酸化反应混合物的步骤。

5. 发明申请

WO2009017241A3 PROCESS FOR PRODUCING TOLUIDINE COMPOUND 审中-公开
标题翻译：生产托洛芬化合物的方法
公开(公告)号：WO2009017241A3
公开(公告)日：2009-05-28
申请号：PCT/JP2008063933
申请日：2008-07-29
申请人： ISHIHARA SANGYO KAISHA , MURAI SHIGEO , YOSHIZAWA HIROSHI , OHSHIMA TAKESHI , MURAKAMI KATSUYOSHI , ANDO TAKAYOSHI , NAKAMURA TADASHI , ADACHI NORIO , ISOGAI AKIHIKO
发明人： MURAI SHIGEO , YOSHIZAWA HIROSHI , OHSHIMA TAKESHI , MURAKAMI KATSUYOSHI , ANDO TAKAYOSHI , NAKAMURA TADASHI , ADACHI NORIO , ISOGAI AKIHIKO
IPC分类号： C07D213/72
CPC分类号： C07D213/72
摘要： Because fluazinam is excellent as an active ingredient of pesticides and highly useful, it is desired to produce it efficiently in a proper form with simple operations at low cost in an environmentally friendly manner. The desired product is obtained in good yields with simple operations by using industrially advantageous reaction systems by a process comprising (1) a step of reacting ACTF and DCDNBTF in the presence of an alkali component, a solvent selected from the group consisting of ketones, nitriles, ethers and esters and a sufficient amount of water to substantially dissolve the alkali component, (2) a step of neutralizing or acidifying the reaction mixture with an acid and (3) a step of removing the solvent by distillation from the mixture containing fluazinam as the reaction product and the reaction solvent to precipitate crystals the product.
摘要翻译：由于氟啶胺作为农药的有效成分是优异的，而且是非常有用的，因此希望能以低成本的环境友好的方式以简单的操作以适当的形式有效地生产。通过使用工业上有利的反应体系，通过使用包括（1）在碱组分，选自酮，腈的溶剂存在下使ACTF和DCDNBTF反应的步骤，以简单的操作获得所需产物，醚和酯和足够量的水以基本上溶解碱组分，（2）用酸中和或酸化反应混合物的步骤和（3）通过蒸馏从包含氟啶胺的混合物中除去溶剂的步骤为反应产物和反应溶剂使产物析出晶体。

6. 发明申请

WO2009017241A2 PROCESS FOR PRODUCING TOLUIDINE COMPOUND 审中-公开
标题翻译：生产甲苯胺化合物的方法
公开(公告)号：WO2009017241A2
公开(公告)日：2009-02-05
申请号：PCT/JP2008/063933
申请日：2008-07-29
申请人： ISHIHARA SANGYO KAISHA, LTD. , MURAI, Shigeo , YOSHIZAWA, Hiroshi , OHSHIMA, Takeshi , MURAKAMI, Katsuyoshi , ANDO, Takayoshi , NAKAMURA, Tadashi , ADACHI, Norio , ISOGAI, Akihiko
发明人： MURAI, Shigeo , YOSHIZAWA, Hiroshi , OHSHIMA, Takeshi , MURAKAMI, Katsuyoshi , ANDO, Takayoshi , NAKAMURA, Tadashi , ADACHI, Norio , ISOGAI, Akihiko
IPC分类号： C07D213/72
CPC分类号： C07D213/72
摘要： Because fluazinam is excellent as an active ingredient of pesticides and highly useful, it is desired to produce it efficiently in a proper form with simple operations at low cost in an environmentally friendly manner. The desired product is obtained in good yields with simple operations by using industrially advantageous reaction systems by a process comprising (1) a step of reacting ACTF and DCDNBTF in the presence of an alkali component, a solvent selected from the group consisting of ketones, nitriles, ethers and esters and a sufficient amount of water to substantially dissolve the alkali component, (2) a step of neutralizing or acidifying the reaction mixture with an acid and (3) a step of removing the solvent by distillation from the mixture containing fluazinam as the reaction product and the reaction solvent to precipitate crystals the product.
摘要翻译：由于氟啶胺作为杀虫剂的有效成分是优异的并且非常有用，所以希望以对环境友好的方式以低成本以简单的操作以适当的形式有效地生产它。通过使用工业上有利的反应体系，通过使用工业上有利的反应体系，通过包括（1）在碱性组分，选自酮，腈的溶剂（2）用酸中和或酸化反应混合物的步骤，和（3）从含有氟啶胺的混合物中蒸馏除去溶剂的步骤，反应产物和反应溶剂使产物沉淀结晶。

7. 发明申请

WO2009017239A2 PROCESS FOR PRODUCING TOLUIDINE COMPOUND 审中-公开
标题翻译：生产托洛芬化合物的方法
公开(公告)号：WO2009017239A2
公开(公告)日：2009-02-05
申请号：PCT/JP2008/063929
申请日：2008-07-29
申请人： ISHIHARA SANGYO KAISHA, LTD. , MURAI, Shigeo , YOSHIZAWA, Hiroshi , OHSHIMA, Takeshi , MURAKAMI, Katsuyoshi , ANDO, Takayoshi , NAKAMURA, Tadashi
发明人： MURAI, Shigeo , YOSHIZAWA, Hiroshi , OHSHIMA, Takeshi , MURAKAMI, Katsuyoshi , ANDO, Takayoshi , NAKAMURA, Tadashi
IPC分类号： C07D213/74
CPC分类号： C07D213/74
摘要： Because fluazinam is excellent as an active ingredient of pesticides and highly useful, it is desired to produce it efficiently in a proper form with simple operations at low cost in an environmentally friendly manner. The desired product is obtained in good yields with simple operations by using industrially advantageous reaction systems by a process comprising (1) a step of reacting ACTF and DCDNBTF in the presence of an alkali component a tertiary alcohol as a solvent and (2) a step of neutralizing or acidifying the reaction mixture with an acid.
摘要翻译：由于氟啶胺作为农药的有效成分是优异的，而且是非常有用的，因此希望能以低成本的环境友好的方式以简单的操作以适当的形式有效地生产。通过使用工业上有利的反应体系，通过使用工业上的方法（1）在碱成分（叔醇作为溶剂）存在下使ACTF和DCDNBTF反应的步骤，（2）步骤用酸中和或酸化反应混合物。

8. 发明专利

JPS6024901A SAW 失效
公开(公告)号：JPS6024901A
公开(公告)日：1985-02-07
申请号：JP13316883
申请日：1983-07-20
申请人： MURAI SHIGEO
发明人： MURAI SHIGEO
IPC分类号： B27B33/10

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