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1. 发明授权

US5594065A Two component waterborne crosslinkable polyurethane/acrylate-hybrid systems 失效
标题翻译：双组分水性交联聚氨酯/丙烯酸酯 - 混合体系
公开(公告)号：US5594065A
公开(公告)日：1997-01-14
申请号：US436534
申请日：1995-05-09
申请人： Chao-Fong Tien , Charles R. Hegedus , Thomas M. Santosusso , Jeanine M. Snyder , Lisa A. Mercando
发明人： Chao-Fong Tien , Charles R. Hegedus , Thomas M. Santosusso , Jeanine M. Snyder , Lisa A. Mercando
IPC分类号： C08G18/00 , C08G18/08 , C08G18/10 , C08G18/12 , C08G18/32 , C08G18/67 , C09D175/00 , C09D175/04 , C09D175/16 , C08L75/04 , C08F8/32
CPC分类号： C09D175/16 , C08G18/0823 , C08G18/10 , C08G18/12 , C08G18/672
摘要： An improved two component coating system based upon crosslinkable hydroxy containing polymers and a polyisocyanate crosslinker. The improvement resides in the utilization of a water-borne hydroxy-terminated polyurethane prepolymer/acrylate hybrid, preferably a hydroxy acrylate hybrid, in combination with a water-dispersible polyisocyanate. The two component coating composition can be prepared by:a) forming a carboxy-containing, water-dispersible, isocyanate-terminated polyurethane prepolymer,b) adding at least one acrylic monomer which contains a hydroxy-group to the carboxy-containing, water-dispersible, isocyanate-terminated polyurethane prepolymer to form a prepolymer/monomer mixture,c) adding an alkanolamine to the prepolymer/monomer mixture to introduce hydroxy functionality into the polyurethane prepolymer,d) dispersing the prepolymer/monomer mixture in water,e) adding an oil-soluble free radical initiator and a hydroxy-containing chain extender to the aqueous dispersion,f) polymerizing the acrylic monomers and completing the chain extension of the prepolymer by heating the aqueous dispersion, andg) mixing the resulting hybrid dispersion with a water-dispersible polyisocyanate.
摘要翻译：基于可交联羟基聚合物和多异氰酸酯交联剂的改进的双组分涂料体系。改进在于水性羟基封端的聚氨酯预聚物/丙烯酸酯杂化物，优选羟丙基酯杂化物与水分散性多异氰酸酯的组合的利用。双组分涂料组合物可以通过以下方法制备：a）形成含羧基的水分散性异氰酸酯封端的聚氨酯预聚物，b）将至少一种含有羟基的丙烯酸单体加入含羧基的水溶性聚氨酯预聚物中，可分散的异氰酸酯封端的聚氨酯预聚物以形成预聚物/单体混合物，c）将烷醇胺加入到预聚物/单体混合物中以将羟基官能团引入聚氨酯预聚物中，d）将预聚物/单体混合物分散在水中，e）油溶性自由基引发剂和含羟基的扩链剂，f）聚合丙烯酸单体并通过加热水分散体完成预聚物的链延伸，和g）将得到的混合分散体与水溶性自由基引发剂可分散多异氰酸酯。

2. 发明授权

US5539007A Catalyst compositions for making polyurethane based on imidazoles and boron compounds 失效
标题翻译：用于制备基于咪唑和硼化合物的聚氨酯的催化剂组合物
公开(公告)号：US5539007A
公开(公告)日：1996-07-23
申请号：US474036
申请日：1995-06-07
申请人： Mark L. Listemann , Lisa A. Mercando , Ann C. L. Savoca
发明人： Mark L. Listemann , Lisa A. Mercando , Ann C. L. Savoca
IPC分类号： C08G18/16 , C08G18/20 , C08J9/00 , C08J9/08
CPC分类号： C08J9/0047 , C08G18/163 , C08G18/2027 , C08J9/0028 , C08J2375/04
摘要： A method for catalyzing the blowing reaction and making polyurethane foams employing a catalyst composition consisting essentially of a hydroxy-functional imidazole of the following formula I ##STR1## where R.sup.1 is a C.sub.1 -C.sub.10 alkyl; R.sup.2 is hydrogen, methyl or ethyl and R.sup.3 is hydrogen or a C.sub.1 -C.sub.20 organic group optionally having an ether functionality, provided that when R.sup.1 is methyl, R.sup.2 and R.sup.3 are not both hydrogen or a hydrogen and a methyl, in combination with a boron compound of the formulaR.sub.n B(OH).sub.3-nwhere n=0 or 1, and R=C.sub.1 -C.sub.8 alkyl, C.sub.5 -C.sub.8 cycloalkyl, or C.sub.6 -C.sub.10 aryl.
摘要翻译：一种用于催化发泡反应并制备聚氨酯泡沫的方法，该催化剂组合物主要由以下分子式I的羟基官能的咪唑组成，其中R1是C1-C10烷基; R2是氢，甲基或乙基，R3是氢或任选具有醚官能团的C1-C20有机基团，条件是当R 1是甲基时，R 2和R 3不同时是氢或氢和甲基，与硼的组合其中n = 0或1，R = C 1 -C 8烷基，C 5 -C 8环烷基或C 6 -C 10芳基的式R n B（OH）3-n的化合物。

3. 发明授权

US5512603A Hydroxy and amino functional pyrrolizidine catalyst compositions for the production of polyurethanes 失效
标题翻译：用于生产聚氨酯的羟基和氨基官能的吡咯烷啶催化剂组合物
公开(公告)号：US5512603A
公开(公告)日：1996-04-30
申请号：US199396
申请日：1994-02-22
申请人： Richard V. C. Carr , Kevin R. Lassila , Mark L. Listemann , Lisa A. Mercando , Kristen E. Minnich , Ann C. L. Savoca , Amy L. Wressell
发明人： Richard V. C. Carr , Kevin R. Lassila , Mark L. Listemann , Lisa A. Mercando , Kristen E. Minnich , Ann C. L. Savoca , Amy L. Wressell
IPC分类号： C08G18/18 , C08G18/20 , C08J9/04 , C07C269/02 , C07C273/02 , C07D251/34 , C08G18/30 , C08G18/32
CPC分类号： C08G18/1825 , C08G18/2054 , C08G2101/00 , C08G2105/02 , Y10S521/902
摘要： A method for preparing a polyurethane foam which comprises reacting an organic polyisocyanate and a polyol in the presence of a blowing agent, cell stabilizer and a catalyst composition consisting essentially of a pyrrolizidine of the formula: ##STR1## where R.sub.1 and R.sub.2 independently are --H, --OH, ##STR2## or --NR.sub.4 R.sub.5, R.sub.3 is hydrogen, a C.sub.1 -C.sub.12 alkyl, C.sub.5 -C.sub.6 cycloalkyl, C.sub.6 -C.sub.10 aryl, or C.sub.7 -C.sub.11 arylalkyl group, andR.sub.4 and R.sub.5 independently represent H, a C.sub.1 -C.sub.12 alkyl group, C.sub.5 -C.sub.10 cycloalkyl, C.sub.6 -C.sub.10 aryl, or C.sub.7 -C.sub.11 arylalkyl group, provided that at least R.sub.1 or R.sub.2 is not hydrogen.
摘要翻译：一种制备聚氨酯泡沫的方法，其包括在发泡剂，细胞稳定剂和基本上由下式组成的吡咯烷子基团的存在下使有机多异氰酸酯与多元醇反应：其中R1和R2独立地为-H ，-OH，kyl，C5-C6环烷基，C6-C10芳基或C7-C11芳烷基，R4和R5独立地表示H，C1-C12烷基，C5-C10环烷基，C6-C10芳基或C7 -C11芳烷基，条件是至少R1或R2不是氢。

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