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1. 发明授权

US07657332B2 Process and systems for the epoxidation of an olefin 失效
标题翻译：用于烯烃环氧化的方法和系统
公开(公告)号：US07657332B2
公开(公告)日：2010-02-02
申请号：US11670338
申请日：2007-02-01
申请人： Peter Ingraham Chipman , Jeffrey Michael Kobe , Arjan Jan Te Raa , Leonid Isaakovich Rubinstein , Brian Scott Vanderwilp , Thijs Wermink
发明人： Peter Ingraham Chipman , Jeffrey Michael Kobe , Arjan Jan Te Raa , Leonid Isaakovich Rubinstein , Brian Scott Vanderwilp , Thijs Wermink
IPC分类号： G05B13/00
CPC分类号： C07D301/10
摘要： A process for the epoxidation of an olefin, which process comprises reacting a feed comprising the olefin, oxygen and a reaction modifier in the presence of a highly selective silver-based catalyst at a reaction temperature T, and with the reaction modifier being present in a relative quantity Q which is the ratio of an effective molar quantity of active species of the reaction modifier present in the feed to an effective molar quantity of hydrocarbons present in the feed, and which process comprises the steps of: operating at a first operating phase wherein the value of T is T1 and the value of Q is Q1, and subsequently operating at a second operating phase at a reaction temperature which is different from the reaction temperature employed in the first operating phase, such that the value of T is T2 and the value of Q is substantially Q2, whereby Q2 is determined by calculation and Q2 is defined by the formula Q2=Q1+B(T2−T1), wherein B denotes a constant factor which is greater than 0; a reaction system suitable for performing the process for the epoxidation of an olefin; a computer program product which comprises a computer readable program recorded on a computer readable medium, suitable for instructing a data processing system of a computer system to execute calculations for the process for the epoxidation of an olefin; and a computer system which comprises the computer program product and a data processing system.
摘要翻译：一种烯烃环氧化方法，该方法包括在高反应温度T下，在高度选择性的银基催化剂存在下使包含烯烃，氧和反应调节剂的进料反应，并且反应改性剂存在于相对量Q是进料中存在的反应改性剂的活性物质的有效摩尔量与进料中存在的有效摩尔量的烃的比例，该方法包括以下步骤：在第一操作阶段 T的值为T1，Q值为Q1，随后在与第一运行阶段中使用的反应温度不同的反应温度下在第二运行阶段运行，使得T的值为T2， Q值基本上为Q2，由此通过计算确定Q2，Q2由公式Q2 = Q1 + B（T2-T1）定义，其中B表示大于0的常数因子 ; 适于进行烯烃环氧化方法的反应体系; 计算机程序产品，其包括记录在计算机可读介质上的计算机可读程序，适于指示计算机系统的数据处理系统执行烯烃的环氧化方法的计算; 以及包括计算机程序产品和数据处理系统的计算机系统。

2. 发明授权

US07528270B2 Process for the production of an olefin oxide, a 1, 2-diol, a 1,2-diol ether, or an alkanolamine 有权
标题翻译：制备烯烃氧化物，1,2-二醇，1,2-二醇醚或链烷醇胺的方法
公开(公告)号：US07528270B2
公开(公告)日：2009-05-05
申请号：US11154184
申请日：2005-06-16
申请人： Randall Clayton Yeates , Leonid Isaakovich Rubinstein
发明人： Randall Clayton Yeates , Leonid Isaakovich Rubinstein
IPC分类号： C07D301/10
CPC分类号： C07D301/10 , Y02P20/142
摘要： A process is provided for the epoxidation of an olefin comprising the steps of: contacting a feed comprising an olefin and oxygen with a catalyst comprising a silver component and a high-selectivity dopant deposited on a fluoride-mineralized carrier; and producing a product mix comprising an olefin oxide, wherein the concentration of carbon dioxide in the feed is less than about 2 mole-%, relative to the total feed.
摘要翻译：提供了一种用于烯烃的环氧化的方法，包括以下步骤：使包含烯烃和氧的进料与包含沉积在氟化物矿化载体上的银组分和高选择性掺杂剂的催化剂接触; 以及生产包含烯烃氧化物的产物混合物，其中进料中二氧化碳的浓度相对于总进料小于约2摩尔％。

3. 发明授权

US07153987B2 Process for making silver based epoxidation catalysts and process for preparing an olefin oxide 失效
标题翻译：制备银基环氧化催化剂的方法和制备烯烃氧化物的方法
公开(公告)号：US07153987B2
公开(公告)日：2006-12-26
申请号：US10677647
申请日：2003-09-30
申请人： Leonid Isaakovich Rubinstein , Candido Gutierrez
发明人： Leonid Isaakovich Rubinstein , Candido Gutierrez
IPC分类号： B01J27/232 , B01J23/50 , C07D301/10
CPC分类号： B01J37/0207 , B01J23/66 , B01J27/232 , B01J35/002 , B01J35/1009 , B01J35/1038 , B01J35/1066 , B01J35/1071 , B01J37/0203 , C07D301/10
摘要： The invention relates to a process for preparing a catalyst which involves (a) preparing a paste having a uniform mixture of at least one alkaline earth metal carbonate; a liquid medium; a silver bonding additive; and, at least one extrusion aid and/or optionally a burnout additive; (b) forming one or more shaped particles from the paste; (c) drying and calcining the particles; and, (e) impregnating the dried and calcined particles with a solution containing a silver compound. The invention also relates to a process for preparing an olefin oxide comprising reacting a gas composition containing an olefin having at least two carbon atoms with oxygen in the presence of the catalyst composition obtained by the process of this invention.
摘要翻译：本发明涉及一种制备催化剂的方法，其包括（a）制备具有至少一种碱土金属碳酸盐的均匀混合物的浆料; 液体介质; 银粘合剂; 和至少一种挤出助剂和/或任选的灼烧添加剂; （b）从糊状物形成一个或多个成形颗粒; （c）干燥和煅烧颗粒; 和（e）用含有银化合物的溶液浸渍干燥和煅烧的颗粒。本发明还涉及一种制备烯烃氧化物的方法，包括在通过本发明的方法获得的催化剂组合物的存在下使含有至少两个碳原子的烯烃的气体组合物与氧反应。

4. 发明授权

US07657331B2 Process and systems for the epoxidation of an olefin 失效
标题翻译：用于烯烃环氧化的方法和系统
公开(公告)号：US07657331B2
公开(公告)日：2010-02-02
申请号：US11670335
申请日：2007-02-01
申请人： Peter Ingraham Chipman , Jeffrey Michael Kobe , Arjan Jan Te Raa , Leonid Isaakovich Rubinstein , Brian Scott Vanderwilp , Thijs Wermink
发明人： Peter Ingraham Chipman , Jeffrey Michael Kobe , Arjan Jan Te Raa , Leonid Isaakovich Rubinstein , Brian Scott Vanderwilp , Thijs Wermink
IPC分类号： G05B13/00
CPC分类号： C07D301/10
摘要： A reaction system for epoxidation of olefins, with a feed control system configured to control the relative quantity of reaction modifier present in the feed, where the relative quantity of said reaction modifier is changed in response to changes in the reaction temperature.
摘要翻译：用于烯烃环氧化的反应体系，其中进料控制系统被配置为控制进料中存在的反应改性剂的相对量，其中反应改性剂的相对量响应于反应温度的变化而改变。

5. 发明授权

US07479565B2 Process for the production of an olefin oxide, a 1,2-diol, a 1,2-diol ether, or an alkanolamine 有权
标题翻译：制备烯烃氧化物，1,2-二醇，1,2-二醇醚或链烷醇胺的方法
公开(公告)号：US07479565B2
公开(公告)日：2009-01-20
申请号：US11154143
申请日：2005-06-16
申请人： Randall Clayton Yeates , Leonid Isaakovich Rubinstein
发明人： Randall Clayton Yeates , Leonid Isaakovich Rubinstein
IPC分类号： C07D301/10
CPC分类号： C07D301/10
摘要： A process is provided for the epoxidation of an olefin comprising the steps of: contacting a feed comprising an olefin and oxygen with a catalyst comprising a silver component deposited on a fluoride-mineralized carrier; and producing a product mix comprising an olefin oxide, wherein the partial pressure of olefin oxide in the product mix is greater than about 60 kPa. A process is provided for the epoxidation of an olefin comprising the steps of: contacting a feed comprising an olefin and oxygen with a catalyst comprising a silver component and a high-selectivity dopant deposited on a fluoride-mineralized carrier; and producing a product mix comprising an olefin oxide, wherein the partial pressure of olefin oxide in the product mix is greater than about 20 kPa.
摘要翻译：提供用于烯烃环氧化的方法，包括以下步骤：使包含烯烃和氧的进料与包含沉积在氟化物矿化载体上的银组分的催化剂接触; 以及生产包含烯烃氧化物的产物混合物，其中产物混合物中烯烃氧化物的分压大于约60kPa。提供了一种用于烯烃的环氧化的方法，包括以下步骤：使包含烯烃和氧的进料与包含沉积在氟化物矿化载体上的银组分和高选择性掺杂剂的催化剂接触; 以及生产包含烯烃氧化物的产物混合物，其中产物混合物中烯烃氧化物的分压大于约20kPa。

6. 发明授权

US07193094B2 Process and systems for the epoxidation of an olefin 有权
标题翻译：用于烯烃环氧化的方法和系统
公开(公告)号：US07193094B2
公开(公告)日：2007-03-20
申请号：US10404829
申请日：2003-04-01
申请人： Peter Ingraham Chipman , Jeffrey Michael Kobe , Arjan Jan Te Raa , Leonid Isaakovich Rubinstein , Brian Scott Vanderwilp , Thijs Wermink
发明人： Peter Ingraham Chipman , Jeffrey Michael Kobe , Arjan Jan Te Raa , Leonid Isaakovich Rubinstein , Brian Scott Vanderwilp , Thijs Wermink
IPC分类号： C07D301/10
CPC分类号： C07D301/10
摘要： A process for the epoxidation of an olefin, which process comprises reacting a feed comprising the olefin, oxygen and a reaction modifier in the presence of a highly selective silver-based catalyst at a reaction temperature T, and with the reaction modifier being present in a relative quantity Q which is the ratio of an effective molar quantity of active species of the reaction modifier present in the feed to an effective molar quantity of hydrocarbons present in the feed, and which process comprises the steps of: operating at a first operating phase wherein the value of T is T1 and the value of Q is Q1, and subsequently operating at a second operating phase at a reaction temperature which is different from the reaction temperature employed in the first operating phase, such that the value of T is T2 and the value of Q is substantially Q2, whereby Q2 is determined by calculation and Q2 is defined by the formula Q2=Q1+B(T2−T1), wherein B denotes a constant factor which is greater than 0; a reaction system suitable for performing the process for the epoxidation of an olefin; a computer program product which comprises a computer readable program recorded on a computer readable medium, suitable for instructing a data processing system of a computer system to execute calculations for the process for the epoxidation of an olefin; and a computer system which comprises the computer program product and a data processing system.
摘要翻译：一种烯烃环氧化方法，该方法包括在高反应温度T下在高度选择性的银基催化剂存在下使包含烯烃，氧和反应调节剂的进料反应，并且反应改性剂存在于相对量Q是进料中存在的反应改性剂的活性物质的有效摩尔量与进料中存在的有效摩尔量的烃的比例，该方法包括以下步骤：在第一操作阶段 T的值为T 1 N且Q的值为Q 1 N 1，随后在与所用反应温度不同的反应温度下在第二操作阶段在第一操作阶段中，使得T的值为T 2，并且Q的值基本上为Q 2，其中Q 2是通过计算确定，并且Q <2>由公式<β在线定义 -formulae description =“In-line Formulas”end =“lead”？> Q＆lt; 2＆gt; = Q 1＆lt; 1＆gt; + B（T 2＆lt; 2＆gt; <？in-line-formula description =“In-line formula”end =“tail”？>其中B表示大于0的常数因子; 适于进行烯烃环氧化方法的反应体系; 计算机程序产品，其包括记录在计算机可读介质上的计算机可读程序，适于指示计算机系统的数据处理系统执行烯烃的环氧化方法的计算; 以及包括计算机程序产品和数据处理系统的计算机系统。

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