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1. 发明申请

WO2009115318A1 A METHOD FOR PRODUCING A MULTILAYER STRUCTURE 审中-公开
标题翻译：一种生产多层结构的方法
公开(公告)号：WO2009115318A1
公开(公告)日：2009-09-24
申请号：PCT/EP2009/002009
申请日：2009-03-18
申请人： TECHNICAL UNIVERSITY OF DENMARK , LARSEN, Peter, Halvor , MENON, Mohan
发明人： LARSEN, Peter, Halvor , MENON, Mohan
IPC分类号： C04B35/622 , C04B35/64 , B01D53/00 , B01D53/32 , B32B18/00
CPC分类号： B32B18/00 , B01D53/32 , B01D67/0041 , B01D67/0046 , B01D69/12 , B01D71/024 , B01D2257/404 , B01D2257/702 , B01D2323/46 , B01D2325/04 , C04B35/632 , C04B35/63404 , C04B35/6342 , C04B38/0022 , C04B2111/0081 , C04B2235/6025 , C04B2235/656 , C04B2235/6567 , C04B2237/34 , C04B2237/52 , C04B2237/525 , C04B2237/704 , C04B2237/84 , C04B35/50 , C04B38/0074 , C04B38/068
摘要： Provided is method for producing a multilayer structure, one method comprising the steps of: - providing a laminate of a first electrode or electrode precursor layer, an electrolyte layer, and a second electrode or electrode precursor layer; - folding the laminate at least once; and - sintering the stack; - wherein the number of layers in the multilayer structure is at least 5. Also provided is a method for producing a multilayer structure, comprising the steps of: - providing an electrolyte layer; - applying a blocking layer on one edge of the electrolyte layer; - providing an electrode or electrode precursor layer directly on the electrolyte layer on the side of the electrolyte layer where the blocking layer has been applied so as to obtain a laminate; - stacking at least two laminates such that the electrolyte layer of each laminate being stacked is applied on the electrode or electrode precursor layer of the stack on which it is stacked; and such that the blocking layer of each laminate being stacked is on the horizontally opposite side of the blocking layer of the laminate on which it is stacked; and - sintering the stack; - wherein the number of layers in the multilayer structure is at least 5. The present invention moreover provides a multilayer structure, obtainable by the above methods.
摘要翻译：提供一种制造多层结构体的方法，一种方法包括以下步骤： - 提供第一电极或电极前体层，电解质层和第二电极或电极前体层的叠层; - 将层压板折叠至少一次; 和 - 烧结堆垛; - 其中多层结构中的层数至少为5.还提供了一种制备多层结构的方法，包括以下步骤： - 提供电解质层; - 在电解质层的一个边缘上施加阻挡层; - 在已经施加阻挡层的电解质层侧面的电解质层上直接提供电极或电极前体层，以获得层压体; - 堆叠至少两个层压板，使得堆叠的每个层叠体的电解质层被施加在其堆叠的堆叠的电极或电极前体层上; 并且使得层叠的每个层压体的阻挡层位于层叠体的堆叠的阻挡层的水平相对侧上; 和 - 烧结堆垛; - 其中所述多层结构中的层数为至少5.本发明还提供了可通过上述方法获得的多层结构。

2. 发明申请

WO2006082057A2 A METHOD FOR PRODUCING A REVERSIBLE SOLID OXID FUEL CELL 审中-公开
标题翻译：一种生产可再生固体氧化物燃料电池的方法
公开(公告)号：WO2006082057A2
公开(公告)日：2006-08-10
申请号：PCT/EP2006/000920
申请日：2006-02-02
申请人： RISOE NATIONAL LABORATORY , LARSEN, Peter, Halvor
发明人： LARSEN, Peter, Halvor
IPC分类号： H01M8/12 , H01M4/88 , H01M4/90 , H01M4/86 , H01M8/02
CPC分类号： H01M8/0243 , H01M4/8885 , H01M4/9025 , H01M4/905 , H01M8/023 , H01M8/0232 , H01M8/1253 , H01M8/126 , H01M8/184 , H01M2008/1293 , Y02E60/525 , Y02E60/528 , Y02P70/56 , Y10T29/49115
摘要： The present invention provides a method for producing a reversible solid oxide fuel cell, comprising the steps of: - providing a metallic support layer; - forming a cathode precursor layer on the metallic support layer; - forming an electrolyte layer on the cathode precursor layer; - sintering the obtained multilayer structure; - impregnating the cathode precursor layer so as to form a cathode layer; and - forming an anode layer on top of the electrolyte layer. Furthermore, a reversible SOFC is provided which is obtainable by said method. The method advantageously allows for a greater choice of anode materials, resulting in more freedom in cell design, depending on the desired application.
摘要翻译：本发明提供一种生产可逆固体氧化物燃料电池的方法，包括以下步骤： - 提供金属支撑层; - 在所述金属支撑层上形成阴极前体层; - 在所述阴极前体层上形成电解质层; - 烧结得到的多层结构; - 浸渍阴极前体层以形成阴极层; 以及 - 在所述电解质层的顶部上形成阳极层。此外，提供了可通过所述方法获得的可逆SOFC。该方法有利地允许阳极材料的更多选择，导致电池设计的更多自由度，这取决于所需的应用。

3. 发明申请

WO2009115319A1 AN ALL CERAMICS SOLID OXIDE FUEL CELL 审中-公开
标题翻译：所有陶瓷固体氧化物燃料电池
公开(公告)号：WO2009115319A1
公开(公告)日：2009-09-24
申请号：PCT/EP2009/002010
申请日：2009-03-18
申请人： TECHNICAL UNIVERSITY OF DENMARK , LARSEN, Peter, Halvor
发明人： LARSEN, Peter, Halvor
IPC分类号： H01M4/88 , H01M4/86 , H01M4/90 , H01M8/12
CPC分类号： H01M4/8885 , H01M4/8621 , H01M4/8657 , H01M4/8892 , H01M4/9025 , H01M4/905 , H01M8/1226 , H01M8/1286 , Y02P70/56 , Y10T29/49108 , Y10T29/49115 , Y10T428/24942
摘要： The present invention provides an all ceramics solid oxide cell, comprising an anode layer, a cathode layer, and an electrolyte layer sandwiched between the anode layer and the cathode layer, wherein the electrolyte layer comprises doped zirconia and has a thickness of from 40 to 300 μm; wherein the anode layer and the cathode layer both comprise doped ceria or both comprise doped zirconia; and wherein the multilayer structure formed of the anode layer, the electrolyte layer and the cathode layer is a symmetrical structure. The present invention further provides a method of producing said solid oxide cell.
摘要翻译：本发明提供一种全部陶瓷固体氧化物电池，其包括阳极层，阴极层和夹在阳极层和阴极层之间的电解质层，其中电解质层包含掺杂的氧化锆，其厚度为40至300 微米; 其中所述阳极层和所述阴极层都包含掺杂的二氧化铈或二者均包括掺杂的氧化锆; 并且其中由阳极层，电解质层和阴极层形成的多层结构是对称结构。本发明还提供一种制备所述固体氧化物电池的方法。

4. 发明申请

WO2009115317A1 A METHOD FOR PRODUCING A MULTILAYER STRUCTURE 审中-公开
标题翻译：一种生产多层结构的方法
公开(公告)号：WO2009115317A1
公开(公告)日：2009-09-24
申请号：PCT/EP2009/002008
申请日：2009-03-18
申请人： TECHNICAL UNIVERSITY OF DENMARK , MENON, Mohan , LARSEN, Peter, Halvor
发明人： MENON, Mohan , LARSEN, Peter, Halvor
IPC分类号： C25D13/02 , C25D13/18 , C25D13/22 , C25D15/00 , C23C24/08 , B22F7/00
CPC分类号： C25D15/00 , B01D53/326 , B01D2257/404 , B01D2257/702 , C23C24/08 , C23C26/00 , C25D13/02 , C25D13/18 , C25D13/22 , H01L41/273
摘要： Provided is method for producing a multilayer structure, one method comprising the steps of: providing a suspension comprising first particles and second particles, wherein the first and second particles have opposite charges; introducing an electrode and a counterelectrode into the suspension; applying a current to said electrode and counterelectrode, whereby at least one layer comprising said first particles is deposited on said electrode and at least one layer comprising said second particles is deposited on the counterelectrode; and changing the direction of the current applied to said electrode and said counterelectrode, whereby at least one layer comprising said second particles is deposited on the electrode and at least one layer comprising said first particles is deposited on the counterelectrode. In another embodiment, there is provided a method for producing a multilayer structure, comprising the steps of: providing a suspension comprising first particles and particles having magnetic properties, wherein the first particles are charged; introducing an electrode having electromagnetic properties and a counterelectrode into the suspension; applying current to said electromagnetic electrode and counterelectrode, whereby at least one layer comprising said first particles is deposited on said electrode; and applying an electromagnetic field to said electrode, whereby at least one layer comprising said particles having magnetic properties is deposited on said electrode. The present invention also provides multilayer structures obtainable by said processes.
摘要翻译：提供了一种制备多层结构的方法，一种方法包括以下步骤：提供包含第一颗粒和第二颗粒的悬浮液，其中第一和第二颗粒具有相反的电荷; 将电极和反电极引入悬浮液中; 向所述电极和反电极施加电流，由此在所述电极上沉积包含所述第一颗粒的至少一层，并且包含所述第二颗粒的至少一层沉积在所述反电极上; 并且改变施加到所述电极和所述反电极的电流的方向，由此将包含所述第二颗粒的至少一个层沉积在所述电极上，并且包含所述第一颗粒的至少一个层沉积在所述反电极上。在另一个实施方案中，提供了一种制备多层结构的方法，包括以下步骤：提供包含第一颗粒和具有磁性的颗粒的悬浮液，其中第一颗粒被加料; 将具有电磁特性的电极和反电极引入所述悬浮液中; 向所述电磁电极和对电极施加电流，由此在所述电极上沉积包含所述第一颗粒的至少一层; 以及向所述电极施加电磁场，由此至少一层包含具有磁特性的颗粒沉积在所述电极上。本发明还提供可通过所述方法获得的多层结构。

5. 发明申请

WO2009027100A1 REMOVAL OF IMPURITY PHASES FROM ELECTROCHEMICAL DEVICES 审中-公开
标题翻译：从电化学设备中去除污染物相
公开(公告)号：WO2009027100A1
公开(公告)日：2009-03-05
申请号：PCT/EP2008/007097
申请日：2008-08-29
申请人： TECHNICAL UNIVERSITY OF DENMARK , LARSEN, Peter, Halvor , MOGENSEN, Mogens , HENDRIKSEN, Peter, Vang , LINDEROTH, Søren , CHEN, Ming
发明人： LARSEN, Peter, Halvor , MOGENSEN, Mogens , HENDRIKSEN, Peter, Vang , LINDEROTH, Søren , CHEN, Ming
IPC分类号： H01M4/86 , H01M4/88 , H01M8/12
CPC分类号： H01M8/1213 , H01M4/8663 , H01M4/8889 , H01M2008/1293 , Y02E60/521 , Y02E60/525
摘要： The present invention provides a solid oxide cell comprising a support layer, a first electrode layer, an electrolyte layer, and a second cathode layer, wherein at least one of the electrode layers comprises electrolyte material, a catalyst and agglomerated particles selected from the group consisting of alkali oxides, earth alkali oxides and transition metal oxides.
摘要翻译：本发明提供了一种固体氧化物电池，其包括支撑层，第一电极层，电解质层和第二阴极层，其中至少一个电极层包括电解质材料，催化剂和附聚粒子的碱金属氧化物，碱土金属氧化物和过渡金属氧化物。

6. 发明申请

WO2009027099A1 MEMBRANE WITH A STABLE NANOSIZED MICROSTRUCTURE AND METHOD FOR PRODUCING SAME 审中-公开
标题翻译：具有稳定的纳米微结构的膜及其制造方法
公开(公告)号：WO2009027099A1
公开(公告)日：2009-03-05
申请号：PCT/EP2008/007096
申请日：2008-08-29
申请人： TECHNICAL UNIVERSITY OF DENMARK , LARSEN, Peter, Halvor , LINDEROTH, Søren
发明人： LARSEN, Peter, Halvor , LINDEROTH, Søren
IPC分类号： B01D71/02 , B01D53/22 , C01B13/02
CPC分类号： B01D67/0046 , B01D53/228 , B01D53/8668 , B01D69/10 , B01D69/145 , B01D71/024 , B01D2257/7022 , B01D2313/42 , B01D2325/10 , B01J23/002 , B01J23/83 , B01J23/86 , B01J23/8892 , B01J35/0033 , B01J35/023 , B01J35/065 , B01J37/0219 , B01J37/0244 , B01J2523/00 , C01B13/0255 , B01J2523/24 , B01J2523/3706 , B01J2523/842 , B01J2523/845 , B01J2523/3712 , B01J2523/375 , B01J2523/847 , B01J2523/47 , B01J2523/56 , B01J2523/36 , B01J2523/48 , B01J2523/72
摘要： The present invention provides a membrane, comprising in this order a first catalyst layer, an electronically and ionically conducting layer having a nanosized microstructure, and a second catalyst layer, characterized in that the electronically and ionically conducting layer is formed from an electrolyte material, a grain growth inhibitor and/or grain boundary modifier, and a method for producing same.
摘要翻译：本发明提供了一种膜，其依次包括第一催化剂层，具有纳米尺寸微结构的电子和离子导电层和第二催化剂层，其特征在于电子和离子导电层由电解质材料形成，晶粒生长抑制剂和/或晶界改性剂及其制造方法。

7. 发明申请

WO2009027098A1 ROBUST MIXED CONDUCTING MEMBRANE STRUCTURE 审中-公开
标题翻译：稳定的混合导电膜结构
公开(公告)号：WO2009027098A1
公开(公告)日：2009-03-05
申请号：PCT/EP2008/007095
申请日：2008-08-29
申请人： TECHNICAL UNIVERSITY OF DENMARK , LINDEROTH, Søren , LARSEN, Peter, Halvor
发明人： LINDEROTH, Søren , LARSEN, Peter, Halvor
IPC分类号： B01D53/22 , B01D69/14 , B01D71/02 , B01D67/00
CPC分类号： B01D53/228 , B01D67/0046 , B01D67/0088 , B01D69/141 , B01D71/025 , B01D2256/12 , B01D2256/16 , B01D2325/10 , C01B3/503 , C01B13/0255
摘要： The present invention provides a membrane structure, comprising in said order a first electronically conducting layer, an ionically conducting layer, and a second electronically conducting layer, characterized in that the first and second electronically conducting layers are internally short circuited. The present invention further provides a method of producing the above membrane structure, comprising the steps of : providing a ionically conducting layer; applying at least one layer of electronically conducting material on each side of said ionically conducting layer; sintering the multilayer structure; and impregnating the electronically conducting layers with a catalyst material or catalyst precursor material.
摘要翻译：本发明提供了一种膜结构，其以所述顺序包括第一电子导电层，离子传导层和第二电子导电层，其特征在于，第一和第二电子导电层内部短路。本发明还提供一种制备上述膜结构的方法，包括以下步骤：提供离子导电层; 在所述离子导电层的每一侧上施加至少一层电子导电材料; 烧结多层结构; 并用催化剂材料或催化剂前体材料浸渍电子导电层。

8. 发明申请

WO2008061782A3 THIN SOLID OXIDE CELL 审中-公开
标题翻译：固体氧化物细胞
公开(公告)号：WO2008061782A3
公开(公告)日：2008-12-24
申请号：PCT/EP2007010194
申请日：2007-11-23
申请人： UNIV DENMARK TECH DTU , LARSEN PETER HALVOR , LINDEROTH SOREN , HENDRIKSEN PETER VANG
发明人： LARSEN PETER HALVOR , LINDEROTH SOREN , HENDRIKSEN PETER VANG
IPC分类号： H01M8/12 , B01D71/02 , C01B3/50 , C01B13/02 , H01M4/86
CPC分类号： H01M8/1213 , B01D67/0041 , B01D67/0046 , B01D69/12 , B01D71/024 , B01D2323/46 , B01D2325/08 , B01D2325/10 , H01M4/8621 , H01M4/8652 , H01M4/8885 , H01M4/90 , H01M4/9016 , H01M4/9033 , H01M4/9066 , H01M8/122 , H01M2300/0094 , Y02E60/521 , Y02E60/525
摘要： The present invention relates to a thin and in principle unsupported solid oxide cell, comprising at least a porous anode layer, an electrolyte layer and a porous cathode layer, wherein the anode layer and the cathode layer comprise an electrolyte material, at least one metal and a catalyst material, and wherein the overall thickness of the thin reversible cell is about 150 µm or less, and to a method for producing same. The present invention also relates to a thin and in principle unsupported solid oxide cell, comprising at least a porous anode layer, an electrolyte layer and a porous cathode layer, wherein the anode layer and the cathode layer comprise an electrolyte material and a catalyst material, wherein the electrolyte material is doper zirconia, and wherein the overall thickness of the thin reversible cell is about 150 µm or less, and to a method for producing same. The present invention further provides a thin separation membrane, comprising at least a porous anode layer, a membrane layer comprising a mixed conducting material and a porous cathode layer, wherein the anode layer and the cathode layer comprise the mixed conducting material and a catalyst material, and wherein the overall thickness of the thin separation membrane is about 150 µm or less.
摘要翻译：本发明涉及一种薄而且原则上未支撑的固体氧化物电池，其至少包括多孔阳极层，电解质层和多孔阴极层，其中阳极层和阴极层包括电解质材料，至少一种金属和催化剂材料，并且其中薄可逆电池的总厚度为约150μm以下，以及其制造方法。本发明还涉及一种薄而且原则上未支撑的固体氧化物电池，其至少包括多孔阳极层，电解质层和多孔阴极层，其中阳极层和阴极层包括电解质材料和催化剂材料，其中所述电解质材料是多氧化锆，并且其中所述薄可逆电池的总厚度为约150μm以下，以及其制造方法。本发明还提供一种薄分离膜，其至少包括多孔阳极层，包含混合导电材料的膜层和多孔阴极层，其中阳极层和阴极层包含混合导电材料和催化剂材料，并且其中所述薄分离膜的总厚度为约150μm以下。

9. 发明申请

WO2006079558A1 REDOX-STABLE ANODE 审中-公开
标题翻译：防氧化阳极
公开(公告)号：WO2006079558A1
公开(公告)日：2006-08-03
申请号：PCT/EP2006/000813
申请日：2006-01-31
申请人： RISOE NATIONAL LABORATORY , LARSEN, Peter, Halvor , CHUNG, Charissa , MOGENSEN, Mogens
发明人： LARSEN, Peter, Halvor , CHUNG, Charissa , MOGENSEN, Mogens
IPC分类号： H01M4/86 , H01M4/88
CPC分类号： H01M4/8605 , H01M4/8652 , H01M4/8885 , H01M4/9033 , H01M8/1226 , H01M8/1253 , H01M2004/028 , Y02E60/525 , Y02P70/56
摘要： The present invention provides a method of producing a solid oxide fuel cell, comprising the steps of: forming an anode support layer; applying an anode layer on the anode support layer; applying an electrolyte layer on the anode layer; and sintering the obtained structure; wherein the anode support layer and/or the anode layer comprises a composition comprising doped zirconia, doped ceria and/or a metal oxide with an oxygen ion or proton conductivity, NiO and at least one oxide selected from the group consisting of AI 2 O 3 , TiO 2 , Cr 2 O 3 , Sc 2 O 3 , VO x , TaO x , MnO x , NbO x , CaO, Bi 2 O 3 , LnO x , MgCr 2 O 4 , MgTiO 3 , CaAI 2 O 4 , LaAIO 3 , YbCrO 3 , ErCrO 4 , NiTiO 3 , NiCr 2 O 4 , and mixtures thereof. According to the invention, a combination of nickel coarsening prevention due to specific Ni-particle growth inhibitors, and, at the same time, a strengthening of the ceramic structure of the anode support layer and/or the anode layer is achieved.
摘要翻译：本发明提供一种固体氧化物燃料电池的制造方法，其特征在于，包括：形成负极支撑层; 在阳极支撑层上施加阳极层; 在阳极层上施加电解质层; 烧结所得结构; 其中所述阳极支撑层和/或所述阳极层包括包含掺杂的氧化锆，掺杂的二氧化铈和/或具有氧离子或质子传导性的金属氧化物的组合物，NiO和选自以下的至少一种氧化物： 2个O 3，2个O 2，2个O 3，3个S 2， O 3，XO，XO，XO，XO，XO，XO， SUB，CaO，Bi 2 O 3，LnO x 2，MgCr 2 O 4，4 3，MgTiO 3，CaAl 2 O 4，LaAlO 3，YbCrO 3，/ 3 ，ErCrO 4，NiTiO 3，NiCr 2 O 4，以及它们的混合物。根据本发明，可以实现由于特定的Ni-颗粒生长抑制剂而导致的防止镍粗化，同时强化阳极支撑层和/或阳极层的陶瓷结构的组合。

10. 发明申请

WO2005122300A3 SOLID OXIDE FUEL CELL 审中-公开
标题翻译：固体氧化物燃料电池
公开(公告)号：WO2005122300A3
公开(公告)日：2006-03-02
申请号：PCT/DK2005000379
申请日：2005-06-09
申请人： FORSKNINGSCT RISOE , LARSEN PETER HALVOR , MOGENSEN MOGENS BJERG , LINDEROTH SOEREN , HANSEN KENT KAMMER , WANG WEIGUO
发明人： LARSEN PETER HALVOR , MOGENSEN MOGENS BJERG , LINDEROTH SOEREN , HANSEN KENT KAMMER , WANG WEIGUO
IPC分类号： H01M8/12 , H01M4/86 , H01M4/88 , H01M4/90 , H01M8/00 , H01M8/02
CPC分类号： H01M8/0223 , H01M4/8621 , H01M4/8885 , H01M4/9016 , H01M4/9025 , H01M4/9033 , H01M4/9066 , H01M8/021 , H01M8/0217 , H01M8/0232 , H01M8/0236 , H01M8/0243 , H01M8/0247 , H01M8/1226 , H01M8/126 , Y02E60/525 , Y02P70/56 , Y10T29/49115
摘要： SOFC cell comprising a metallic support 1 ending in a substantially pure electron conducting oxide, an active anode layer 2 consisting of doped ceria, ScYSZ, Ni-Fe alloy, an electrolyte layer 3 consisting of co-doped zirconia based on oxygen ionic conductor, an active cathode layer 5 and a layer of a mixture of LSM and a ferrite as a transition layer 6 to a cathode current collector 7 of single phase LSM. The use of a metallic support instead of a Ni-YSZ anode support increases the mechanical strength of the support and secures redox stability of the support. The porous ferrite stainless steel ends in a pure electron conducting oxide so as to prevent reactivity between the metals in the active anode which tends to dissolve into the ferrite stainless steel causing a detrimental phase shift from ferrite to austenite structure.
摘要翻译： SOFC电池包括以基本上纯的电子传导氧化物为末端的金属载体1，由掺杂的二氧化铈，ScYSZ，Ni-Fe合金构成的活性阳极层2，由基于氧离子导体的共掺杂氧化锆组成的电解质层3，活性阴极层5和作为过渡层6的LSM和铁氧体的混合物层到单相LSM的阴极集电体7。使用金属载体代替Ni-YSZ阳极支撑件增加了载体的机械强度并确保了载体的氧化还原稳定性。多孔铁素体不锈钢以纯电子传导氧化物结束，以防止活性阳极中易于溶解到铁素体不锈钢中的金属之间的反应性，从而导致从铁素体到奥氏体结构的有害相移。

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