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1. 发明授权

US06549714B1 Optical waveguide 失效
标题翻译：光波导
公开(公告)号：US06549714B1
公开(公告)日：2003-04-15
申请号：US09551869
申请日：2000-04-18
申请人： Jung-Hee Kim , Kwan-Soo Han , Woo-Hyuk Jang , Dong-Hack Suh , Tae-Hyung Rhee
发明人： Jung-Hee Kim , Kwan-Soo Han , Woo-Hyuk Jang , Dong-Hack Suh , Tae-Hyung Rhee
IPC分类号： G02B610
CPC分类号： G02B6/138 , C08G73/10 , C08G73/1039 , C08G73/1042 , G02B1/046 , G02B1/048 , Y10T428/23 , Y10T428/24942 , C08L79/08
摘要： An optical waveguide including a core layer formed of a polymer, and a cladding layer placed in proximate to the core layer, the cladding layer being formed of a polymer having a refractive index smaller than the refractive index of the polymer for the core layer, wherein the polymers for the core and cladding layers are selected from the copolymers having the formula (1): where X is Y is and n is a mole fraction in the range of 0.05≦n
摘要翻译：包括由聚合物形成的芯层和放置在芯层附近的包层的光波导，包层由折射率小于芯层聚合物的折射率的聚合物形成，其中芯和包覆层的聚合物选自具有式（1）的共聚物：其中X是Y是并且n是在0.05 <= n <1的范围内的摩尔分数。

2. 发明授权

US06486292B2 Optical polyimide precursor, optical polyimide compound and fabricating method thereof 有权
标题翻译：光学聚酰亚胺前体，光学聚酰亚胺化合物及其制造方法
公开(公告)号：US06486292B2
公开(公告)日：2002-11-26
申请号：US09799665
申请日：2001-03-07
申请人： Kyung-Hee You , Kwan-Soo Han , Tae-Hyung Rhee , Eun-Ji Kim , Jung-Hee Kim , Woo-Hyeuk Jang
发明人： Kyung-Hee You , Kwan-Soo Han , Tae-Hyung Rhee , Eun-Ji Kim , Jung-Hee Kim , Woo-Hyeuk Jang
IPC分类号： C08G7310
CPC分类号： C07D487/04 , C07C217/90 , C08G73/105 , G02B1/045 , C08L79/08
摘要： The present invention provides an optical polyimide compound defined by the following formula in an optical high polymer material: wherein X is Cl, Br, oxo-halide, or fully halogenated alkyl; A is a divalent aromatic or halogenated aromatic moiety; and Z is a tetravalent moiety which may be a partly or fully fluorinated aromatic ring, a partly or fully chlorinated aromatic ring, a partly or fully fluorinated cycloaliphatic group, a partly or fully chlorinated aliphatic group, or combinations thereof connected via hetero atoms.
摘要翻译：本发明提供光学高分子材料中由下式定义的光学聚酰亚胺化合物：其中X为Cl，Br，氧代卤化物或完全卤代烷基; A是二价芳族或卤代芳族部分; Z是四价部分，其可以是部分或完全氟化的芳族环，部分或完全氯化的芳族环，部分或完全氟化的脂环族基团，部分或完全氯化的脂族基团，或其通过杂原子连接的组合。

3. 发明授权

US06303743B1 Polyimide for optical communications, method of preparing the same, and method of forming multiple polyimide film using the polyimide 失效
标题翻译：用于光通信的聚酰亚胺，其制备方法以及使用该聚酰亚胺形成多个聚酰亚胺膜的方法
公开(公告)号：US06303743B1
公开(公告)日：2001-10-16
申请号：US09441888
申请日：1999-11-17
申请人： Kyung-hee You , Kwan-soo Han , Tae-hyung Rhee
发明人： Kyung-hee You , Kwan-soo Han , Tae-hyung Rhee
IPC分类号： C05G7310
CPC分类号： C08G73/1039 , C08G73/1014 , G02B1/045 , C08L79/08
摘要： A polyimide for optical communications, which is expressed by the formula (1), a method of preparing the same, and a method of forming multiple polyimide films using the polyimide, wherein the formula (1) is given by X1, X2, X3, A1, A2, B1, B2, B3, D1, D2, E1, E2, Y1, Y2, Y3, Y4, Y5, Y6, Y7, and Y8, are independently selected from the group consisting of hydrogen atom, halogen atom, alkyl group, halogenated alkyl group, aryl group and halogenated aryl group; Z is a simple chemical bond or selected from the group consisting of —O—, —CO—, —SO3—, —S—, —(T)m—, —(OT)m— and —(OTO)m—, wherein T is alkylene or arylene group substituted by at least one of halogen atom and halogenated alkyl group and m is an integer from 1 to 10; and n is an integer from 1 to 39. Because the polyimide expressed by the formula (1) has a lower birefringence than a common polyimide used as a material for optical waveguiding, a problem associated with the dependency of optical characteristics on polarization can be solved. Also, the solubility of the polyimide in an organic solvent is lowered, so that the occurrence of cracks in a polyimide layer can be avoided in the case of forming multiple polyimide films.
摘要翻译：一种用于光通信的聚酰亚胺，其由式（1）表示，其制备方法和使用该聚酰亚胺形成多个聚酰亚胺膜的方法，其中式（1）由X 1，X 2，X 3，A 1给出，A2，B1，B2，B3，D1，D2，E1，E2，Y1，Y2，Y3，Y4，Y5，Y6，Y7和Y8独立地选自氢原子，卤素原子，烷基卤代烷基，芳基和卤代芳基; Z是简单的化学键或选自-O - ， - CO - ， - SO 3 - ， - S-， - （T）m - ， - （OT）m-和 - （OTO）其中T是被卤素原子和卤代烷基中的至少一个取代的亚烷基或亚芳基，m是1至10的整数; n是1〜39的整数。由于式（1）表示的聚酰亚胺具有比用作光波导材料的普通聚酰亚胺更低的双折射率，所以可以解决光学特性对极化的依赖性的问题。此外，聚酰亚胺在有机溶剂中的溶解度降低，从而在形成多个聚酰亚胺膜的情况下可以避免在聚酰亚胺层中出现裂纹。

4. 发明授权

US06233388B1 Polymer optical waveguide and method for fabricating the same 失效
标题翻译：聚合物光波导及其制造方法
公开(公告)号：US06233388B1
公开(公告)日：2001-05-15
申请号：US09186361
申请日：1998-11-05
申请人： Eun-Ji Kim , Jung-Hee Kim , Woo-Hyuk Jang , Kwan-Soo Han , Tae-Hyung Rhee
发明人： Eun-Ji Kim , Jung-Hee Kim , Woo-Hyuk Jang , Kwan-Soo Han , Tae-Hyung Rhee
IPC分类号： G02B613
CPC分类号： G02B6/1221
摘要： The present invention discloses a polymer optical waveguide and a method of fabricating the same. The polymer optical waveguide comprises a core formed of polymer containing fluoride (F) of a 12-37 wt % on the basis of total weight of the polymer, and having repeating units with at least two —C(═O)—N—C(═O) functional groups or at least four —N—C(═O)— functional groups; and a cladding in contact with the core and formed of polymer having a refractive index lower than the polymer for forming the core. If a core layer is etched according to the ICP etching method, the etch rate becomes at least three times faster than that of the conventional RIE etching method. Also, etching characteristics including uniformity of an etched plane and vertical profile are improved, thereby reducing damage to an optical waveguide. Thus, the light scattering loss of the optical waveguide can be minimized. Also, the method for fabricating of a polymer optical waveguide according to the present invention is useful for mass production of polymer optical waveguides.
摘要翻译：本发明公开了一种聚合物光波导及其制造方法。聚合物光波导包括由基于聚合物总重量的12-37重量％的氟化物（F）的聚合物形成的芯，并且具有至少两个-C（= O）-NC（= O）官能团或至少四个-NC（= O） - 官能团; 以及与芯部接触并由聚合物形成的包层，其折射率低于用于形成芯的聚合物的折射率。如果根据ICP蚀刻方法蚀刻芯层，则蚀刻速率比常规RIE蚀刻方法的蚀刻速率快至少三倍。此外，包括蚀刻平面的均匀性和垂直剖面的蚀刻特性得到改善，从而减少对光波导的损伤。因此，可以使光波导的光散射损失最小化。此外，根据本发明的聚合物光波导的制造方法对聚合物光波导的批量生产是有用的。

5. 发明授权

US6107402A Optical polymer composition 有权
标题翻译：光学聚合物组成
公开(公告)号：US6107402A
公开(公告)日：2000-08-22
申请号：US193135
申请日：1998-11-17
申请人： Eun-Ji Kim , Kwan-Soo Han , Woo-Hyuk Jang , Tae-Hyung Rhee
发明人： Eun-Ji Kim , Kwan-Soo Han , Woo-Hyuk Jang , Tae-Hyung Rhee
IPC分类号： G02B6/12 , C08L27/12 , C08L53/00 , C08L53/02 , C08L101/12 , G02B1/04 , C08L51/04
CPC分类号： G02B1/04 , C08L27/12 , C08L53/00 , C08L53/02 , C08L2205/02
摘要： An optical polymer composition in which polymers having the same repeating units with different polymerization ratios are mixed in an arbitrary ratio. An optical material having a desired refractive index can be attained by appropriately adjusting the mixing ratio based on weight. With such a composition, it is easy to finely adjust the difference in refractive indices between a core and a cladding forming an optical waveguide, thus an optical waveguide device can be easily fabricated.
摘要翻译：将具有不同聚合比例的具有相同重复单元的聚合物以任意比例混合的光学聚合物组合物。可以通过适当地调节基于重量的混合比来获得具有所需折射率的光学材料。通过这样的组成，可以容易地精细地调整形成光波导的芯和包层之间的折射率差，从而可以容易地制造光波导器件。

6. 发明授权

US06891067B2 Optical polyimide precursor, optical polyimide compound and fabricating method thereof 有权
标题翻译：光聚酰亚胺前体，光学聚酰亚胺化合物及其制造方法
公开(公告)号：US06891067B2
公开(公告)日：2005-05-10
申请号：US10265705
申请日：2002-10-08
申请人： Kyung-Hee You , Kwan-Soo Han , Tae-Hyung Rhee , Eun-Ji Kim , Jung-Hee Kim , Woo-Hyeuk Jang
发明人： Kyung-Hee You , Kwan-Soo Han , Tae-Hyung Rhee , Eun-Ji Kim , Jung-Hee Kim , Woo-Hyeuk Jang
IPC分类号： C07C217/90 , C07D487/04 , C08G73/10 , G02B1/04 , C07C209/36 , C08G69/26 , G02B6/00
CPC分类号： C07D487/04 , C07C217/90 , C08G73/105 , G02B1/045 , C08L79/08
摘要： The present invention provides an optical polyimide precursor for use in making a polyimide. The precursor is defined by the following formula: wherein X is Cl, Br, oxo-halide, or fully halogenated alkyl, and A is a divalent aromatic or halogenated aromatic moiety. The present invention provides a method of preparing a diamine compound for use as an optical polyimide precursor. The method includes the steps of dissolving 2-chloro-5-nitrobenzotrifluoride and a diol in N,N-dimethylacetamide to form a solution, adding potassium carbonate, tert-butylammonium chloride and copper powder to said solution and heating the resulting mixture, removing the copper, precipitating and recrystallizing a dinitro-compound resulting from heating the mixture, and dissolving the dinitro-compound and reducing the dinitro-compound to yield a diamine compound.
摘要翻译：本发明提供一种用于制造聚酰亚胺的光学聚酰亚胺前体。前体由下式定义：其中X是Cl，Br，氧代卤化物或完全卤化的烷基，A是二价芳族或卤代芳族部分。本发明提供了制备用作光学聚酰亚胺前体的二胺化合物的方法。该方法包括将2-氯-5-硝基三氟甲苯和二醇溶解在N，N-二甲基乙酰胺中以形成溶液，向所述溶液中加入碳酸钾，叔丁基氯化铵和铜粉末并加热所得混合物，铜，沉淀并重结晶由加热混合物产生的二硝基化合物，并溶解二硝基化合物并还原二硝基化合物，得到二胺化合物。

7. 发明授权

US06316589B1 Polyimide for optical communications 有权
标题翻译：聚酰亚胺用于光通信
公开(公告)号：US06316589B1
公开(公告)日：2001-11-13
申请号：US09547312
申请日：2000-04-11
申请人： Kyung-Hee You , Kwan-Soo Han , Tae-Hyung Rhee
发明人： Kyung-Hee You , Kwan-Soo Han , Tae-Hyung Rhee
IPC分类号： C08G7310
CPC分类号： C08G73/1042 , C08G73/10 , C08G73/1039 , G02B1/046 , C08L79/08
摘要： A polyimide for optical communications, which is expressed by the formula (1) where R1 and R2 are independently selected from the group consisting of CF3, CCl3, unsubstituted aromatic ring group and halogenerated aromatic ring group; R3 and R4 are independently selected from the group consisting of Cl, F, I, Br, CF3, CCl3, unsubstituted aromatic ring group and halogenated aromatic ring group; and n is an integer from 1 to 39. The polyimides have a superior heat resistance, and can avoid the increase in optical absorption loss due to a refractive index increase and deterioration of adhesive and coating properties due to weak surface tension of a polyimide film. In addition, use of the polyimides as a material for a core layer of optical waveguides can expand the selection range of material for the cladding layer of the optical waveguide.
摘要翻译：一种用于光通信的聚酰亚胺，其由式（1）表示，其中R 1和R 2独立地选自CF 3，CCl 3，未取代的芳族环基团和卤代芳族环基团; R 3和R 4独立地选自Cl，F，I，Br，CF 3，CCl 3，未取代的芳环基和卤代芳环基; n为1〜39的整数。聚酰亚胺具有优异的耐热性，并且能够避免由于聚酰亚胺薄膜的表面张力弱导致的折射率增加，粘合剂劣化和涂布性能引起的光吸收损失的增加。此外，使用聚酰亚胺作为光波导的芯层的材料可以扩大光波导的包层的材料的选择范围。

8. 发明授权

US6136929A Polyarylene ether for optical communication 失效
标题翻译：聚亚芳基醚用于光通信
公开(公告)号：US6136929A
公开(公告)日：2000-10-24
申请号：US148695
申请日：1998-09-04
申请人： Kwan-soo Han , Woo-hyuk Jang , Eun-ji Kim , Tae-hyung Rhee
发明人： Kwan-soo Han , Woo-hyuk Jang , Eun-ji Kim , Tae-hyung Rhee
IPC分类号： G02B6/12 , B32B27/00 , C08G65/38 , C08G65/40 , G02B6/00 , C08F283/08 , C08G65/42
CPC分类号： C08G65/4006 , C08G2650/48
摘要： Polyarylene ether for optical communications, expressed by the formula 1: ##STR1## The polyarylene ether has excellent resistance to heat and film processing properties and the light absorption loss in the wavelength range for optical communications is low. Also, by controlling the copolymerization ratio of a monomer whose hydrogen of C--H bond is substituted by F and a monomer whose hydrogen of C--H bond is substituted by Cl, the refractive index of the polymer can be adjusted to a level suitable for an optical material used for optical communications.
摘要翻译：用于光通信的聚芳醚，由式1表示：聚亚芳基醚具有优异的耐热和薄膜加工性能，并且在光通信的波长范围内的光吸收损失低。此外，通过控制由CH取代氢的单体被C取代的单体和CH键的氢被Cl取代的单体的共聚比，聚合物的折射率可以调整到适用于所用光学材料的水平用于光通信。

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