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    • 1. 发明申请
    • Production process and system for insoluble azo pigments
    • 不溶性偶氮颜料的生产工艺和体系
    • US20060086290A1
    • 2006-04-27
    • US11230625
    • 2005-09-21
    • Shigeru InoueKouichi NagatsukaMasahiro MoriShotoku TakamiKazuo IoharaShigemitsu KibeKazuhiko Kaneko
    • Shigeru InoueKouichi NagatsukaMasahiro MoriShotoku TakamiKazuo IoharaShigemitsu KibeKazuhiko Kaneko
    • C09B27/00C09B41/00
    • C09B41/008B01J4/02B01J19/18B01J2219/00164
    • An insoluble azo pigment is produced by ejecting a diazo solution and a grounding solution continuously into an ejector such that within the ejector, the diazo solution and grounding solution are mixed with each other and are subjected to a coupling reaction. A production system for the insoluble azo pigment includes the following units (1) to (4): (1) a first feed tank (2) for a first fluid selected from the diazo solution or grounding solution, a first flow path (a) for feeding the first fluid to nozzles of an ejector (1), and a pump (d) for feeding the first fluid through the first flow path; (2) the ejector (1) provided with the nozzles, a suction chamber, a diffuser, and a temperature control device (g); (3) a second feed tank (3) for a second fluid, a second flow path (b) for guiding the second fluid into the suction chamber, and a flow control device (e) for controlling a flow rate of the second fluid through the second flowpath (b); and (4) a heat treatment tank (5) for subjecting to heat treatment a suspension of the insoluble azo pigment formed by a reaction between the first fluid and the second fluid, and a third flow path (a′) for guiding the suspension from the diffuser to the heat treatment tank.
    • 通过将重氮溶液和接地溶液连续地喷射到喷射器中,使得在喷射器内将重氮溶液和接地溶液彼此混合并进行偶联反应来制备不溶性偶氮颜料。 用于不溶性偶氮颜料的生产系统包括以下单元(1)至(4):(1)用于选自重氮溶液或接地溶液的第一流体的第一进料罐(2),第一流动路径(a) 用于将第一流体供给到喷射器(1)的喷嘴;以及泵(d),用于通过第一流路供给第一流体; (2)设置有喷嘴的喷射器(1),吸入室,扩散器和温度控制装置(g); (3)用于第二流体的第二进料罐(3),用于将第二流体引导到吸入室中的第二流动路径(b)和用于控制第二流体通过的流量的流量控制装置(e) 第二个流路(b); 和(4)热处理槽(5),用于对由第一流体和第二流体之间的反应形成的不溶性偶氮颜料的悬浮液进行热处理,以及用于引导悬浮液从第 扩散器到热处理槽。