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1. 发明授权

US08158572B2 Linear polydimethylsiloxane-polyether copolymers with amino and/or quaternary ammonium groups and use thereof 有权
标题翻译：具有氨基和/或季铵基团的线性聚二甲基硅氧烷 - 聚醚共聚物及其用途
公开(公告)号：US08158572B2
公开(公告)日：2012-04-17
申请号：US13015852
申请日：2011-01-28
申请人： Frank Schubert , Wilfried Knott , Michael Ferenz , Klaus-Dieter Klein , Tobias Maurer , Ralph Scheuermann , Bernard William Kluesener , Rajan Keshav Panadiker
发明人： Frank Schubert , Wilfried Knott , Michael Ferenz , Klaus-Dieter Klein , Tobias Maurer , Ralph Scheuermann , Bernard William Kluesener , Rajan Keshav Panadiker
IPC分类号： C11D3/37
CPC分类号： C11D3/3742 , C08G77/388 , C08G77/46 , C08L83/12 , C11D3/001
摘要： Household care compositions having a linear polydimethylsiloxane-polyether copolymers with amino and/or quaternary ammonium groups, obtainable by the reaction of organopolysiloxanes functionalized with secondary aminoalkyl groups with the reaction products formed from compounds containing epoxy groups and amines, the use thereof and process for preparation thereof.
摘要翻译：具有具有氨基和/或季铵基团的直链聚二甲基硅氧烷 - 聚醚共聚物的家用护理组合物，其通过用仲氨基烷基官能化的有机聚硅氧烷与由含有环氧基和胺的化合物形成的反应产物的反应获得，其用途和制备方法其中。

2. 发明申请

US20110190190A1 Novel Linear Polydimethylsiloxane-Polyether Copolymers with Amino and/or Quaternary Ammonium Groups and Use Thereof 有权
标题翻译：具有氨基和/或季铵基团的新型线性聚二甲基硅氧烷 - 聚醚共聚物及其用途
公开(公告)号：US20110190190A1
公开(公告)日：2011-08-04
申请号：US13015852
申请日：2011-01-28
申请人： Frank Schubert , Wilfried Knott , Michael Ferenz , Klaus-Dieter Klein , Tobias Maurer , Ralph Scheuermann , Bernard William Kluesener , Rajan Keshav Panadiker
发明人： Frank Schubert , Wilfried Knott , Michael Ferenz , Klaus-Dieter Klein , Tobias Maurer , Ralph Scheuermann , Bernard William Kluesener , Rajan Keshav Panadiker
IPC分类号： C11D3/60 , C08G77/04
CPC分类号： C11D3/3742 , C08G77/388 , C08G77/46 , C08L83/12 , C11D3/001
摘要： Household care compositions having a linear polydimethylsiloxane-polyether copolymers with amino and/or quaternary ammonium groups, obtainable by the reaction of organopolysiloxanes functionalized with secondary aminoalkyl groups with the reaction products formed from compounds containing epoxy groups and amines, the use thereof and process for preparation thereof.
摘要翻译：具有具有氨基和/或季铵基团的直链聚二甲基硅氧烷 - 聚醚共聚物的家用护理组合物，其通过用仲氨基烷基官能化的有机聚硅氧烷与由含有环氧基和胺的化合物形成的反应产物的反应获得，其用途及其制备方法其中。

3. 发明申请

US20110172373A1 Equilibration of Siloxanes on Water-Containing Sulphonated Cation Exchange Resins 有权
标题翻译：硅氧烷在含水磺化阳离子交换树脂上的平衡
公开(公告)号：US20110172373A1
公开(公告)日：2011-07-14
申请号：US13119822
申请日：2009-08-21
申请人： Wilfried Knott , Frauke Henning , Klaus-Dieter Klein , Horst Dudzik
发明人： Wilfried Knott , Frauke Henning , Klaus-Dieter Klein , Horst Dudzik
IPC分类号： C08G77/46 , C07F7/08
CPC分类号： C08G77/10 , C08G77/46 , Y02P20/582
摘要： The invention relates to a process for producing equilibration products of organosiloxanes by rearrangement of the siloxane bond to a cation exchange resin, the organopolysiloxanes thus obtainable, and the use thereof.
摘要翻译：本发明涉及通过将硅氧烷键重排为阳离子交换树脂，由此得到的有机聚硅氧烷及其用途来生产有机硅氧烷的平衡产物的方法。

4. 发明申请

US20090030097A1 LINEAR POLYDIMETHYLSILOXANE-POLYOXYALKYLENE BLOCK COPOLYMERS LINKED VIA SIC GROUPS AND VIA CARBOXYLIC ESTER GROUPS, A PROCESS FOR PREPARING THEM AND THEIR USE 失效
标题翻译：线性聚二甲基硅氧烷 - 聚氧乙烯嵌段共聚物通过SIC基团和通过羧酸酯基团连接，其制备方法及其使用
公开(公告)号：US20090030097A1
公开(公告)日：2009-01-29
申请号：US12179944
申请日：2008-07-25
申请人： Wilfried Knott , Oliver Thum , Klaus-Dieter Klein , Dagmar Windbiel , Claudia Hierath
发明人： Wilfried Knott , Oliver Thum , Klaus-Dieter Klein , Dagmar Windbiel , Claudia Hierath
IPC分类号： C08G77/06 , C08G77/04 , C08J9/00
CPC分类号： C08G77/46
摘要： The invention provides linear polydimethylsiloxane-polyoxyalkylene block copolymers containing Si—C groups and carboxylic ester groups and having repeating (A1BA2B) units where A1 and A2 are two different polydimethylsiloxane units of the general formula (I) with a number of Si atoms N=(n+2) of 15≦N≦30 and NA1≠NA2 and B is a unit of the formula (II) —CH2—CH2—(CH2)a—CO[O—CH2—CH(R)]c—O-[D-O]e—[—CH2—CH(R)—O]d—OC—(CH2)b—CH2—CH2— (II) where R independently at each occurrence is H, —CH3 or —C2H5, a and b independently of one another are 0 to 20, c and d independently of one another are values ≧1, e is 0 or 1 and D is a hydrocarbon radical having 2 to 10 C atoms, the overall molar weight of the unit of the formula II being from 600 to 10000 g/mol, with the proviso that the average mixed molar weight of the polydimethylsiloxane units (A1+A2) is from >1665 to 0% to ≦50% by weight, based on the overall weight of [O—CH2—CH(R)] in B, a process for preparing them and their use.
摘要翻译：本发明提供含有Si-C基团和羧酸酯基并具有重复（A1BA2B）单元的线性聚二甲基硅氧烷 - 聚氧化烯嵌段共聚物，其中A1和A2是通式（I）的两种不同聚二甲基硅氧烷单元，其数量为Si原子N =（（II）-CH2-CH2-（CH2）a-CO [O-CH2-CH（R）] cO的单元，其中n为0≤n≤30且NA1 < - [DO] e - [ - CH 2 -CH（R）-O] d-OC-（CH 2）b -CH 2 -CH 2 - （II）其中R在每次出现时独立地为H，-CH 3或-C 2 H 5，a和 b彼此独立地为0至20，c和d彼此独立地为值> = 1，e为0或1，D为具有2至10个C原子的烃基，单位的总摩尔量式II为600至10000g / mol，条件是聚二甲基硅氧烷单元（A1 + A2）的平均混合摩尔数为> 1665至<1998g / mol，[O-CH 2 -CH（ R）]，相对于B中的[O-CH 2 -CH（R）]的总重量，RH> 0重量％〜<50重量％一个准备和使用它们的过程。

5. 发明申请

US20080153995A1 Process for the preparation of SiOC-linked, linear polydimethylsiloxane-polyoxyalkylene block copolymers and their use 有权
标题翻译：用于制备SiOC连接的线性聚二甲基硅氧烷 - 聚氧化烯嵌段共聚物的方法及其用途
公开(公告)号：US20080153995A1
公开(公告)日：2008-06-26
申请号：US11956483
申请日：2007-12-14
申请人： Wilfried Knott , Klaus-Dieter Klein , Rudiger Landers , Dagmar Windbiel
发明人： Wilfried Knott , Klaus-Dieter Klein , Rudiger Landers , Dagmar Windbiel
IPC分类号： C08G77/42
CPC分类号： C08G77/46 , C08L83/12
摘要： The invention relates to a process for the preparation of SiOC-linked, linear polydimethylsiloxane-polyoxyalkylene block copolymers having (AB) repeat units, via reaction of one or more polyetherdiols with a stoichiometric excess of α,ω-dihydropoly-dimethylsiloxanes and at least one tertiary amine as catalyst, which comprises, after completed reaction of the alcohol component, continuing the reaction in the presence of small amounts of water until no remaining ≡Si(H) groups are detectable by a gas-volumetric method.
摘要翻译：本发明涉及通过一种或多种聚醚二醇与化学计量过量的α，ω-二氢聚二甲基硅氧烷和至少一种聚醚二醇的反应制备具有（AB）重复单元的SiOC连接的线性聚二甲基硅氧烷 - 聚氧化烯嵌段共聚物的方法叔胺作为催化剂，其包括在醇组分完全反应之后，在少量水存在下继续反应，直到通过气体容积法不能检测到剩余的≡Si（H）基团。

6. 发明申请

US20080153992A1 Process for the preparation of SiOC-linked, linear polydimethylsiloxane-polyoxyalkylene block copolymers and their use 有权
标题翻译：用于制备SiOC连接的线性聚二甲基硅氧烷 - 聚氧化烯嵌段共聚物的方法及其用途
公开(公告)号：US20080153992A1
公开(公告)日：2008-06-26
申请号：US11956423
申请日：2007-12-14
申请人： Wilfred Knott , Juergen Droese , Klaus Dieter Klein , Rudiger Landers , Dagmar Windbiel
发明人： Wilfred Knott , Juergen Droese , Klaus Dieter Klein , Rudiger Landers , Dagmar Windbiel
IPC分类号： C08G77/46
CPC分类号： C08G77/46 , C08G18/48 , C08G77/12 , C08G2101/0083
摘要： The invention relates to a process for the preparation of SiOC-linked, linear polydimethylsiloxane-polyoxyalkylene block copolymers having (AB) repeat units, via reaction by methods known per se of polyetherdiols with a stoichiometric excess of α,ω-dihydropolydimethylsiloxanes, in the presence of one or more compounds of elements of main group 13 and/or of transition group 3 as catalyst, which comprises, after completed reaction of the alcohol component, continuing the reaction until no remaining ≡Si(H) groups are detectable by a gas-volumetric method, and also to the compounds thus prepared, and to their use as surfactant additives for the production of polyurethane ether foams.
摘要翻译：本发明涉及一种制备具有（AB）重复单元的SiOC连接的线性聚二甲基硅氧烷 - 聚氧化烯嵌段共聚物的方法，其通过本身已知的聚醚二醇与化学计量过量的α，ω-二氢聚二甲基硅氧烷的反应，在存在下的主要组分13和/或过渡组3的元素的一种或多种化合物作为催化剂，其包括在醇组分完全反应之后继续反应，直到没有剩余的≡Si（H）基团可被气 - 体积法，以及由此制备的化合物，以及它们作为用于生产聚氨酯醚泡沫的表面活性剂添加剂的用途。

7. 发明授权

US5430166A Silanes with hydrophilic groups, their synthesis and use as surfactants in aqueous media 失效
标题翻译：具有亲水基团的硅烷，它们的合成和用作水性介质中的表面活性剂
公开(公告)号：US5430166A
公开(公告)日：1995-07-04
申请号：US265078
申请日：1994-06-24
申请人： Klaus-Dieter Klein , Wilfried Knott , Gotz Koerner
发明人： Klaus-Dieter Klein , Wilfried Knott , Gotz Koerner
IPC分类号： B01F17/54 , B01J23/42 , C07B61/00 , C07F7/08 , C08G65/32 , C08G77/46 , C08L71/02 , C08L101/16 , C11D1/00 , C11D1/14 , C11D1/29 , C11D1/82 , C11D3/16 , C07F7/18
CPC分类号： B01F17/0071 , C07F7/0818 , C07F7/0829 , C07F7/083 , C11D1/146 , C11D1/29 , C11D1/82 , C11D3/162 , Y10S516/01 , Y10S516/03
摘要： Silanes of the general formula ##STR1## are prepared wherein R.sup.1, R.sup.2 and R.sup.3 in the molecule are the same or different and represent aliphatic hydrocarbon groups,R.sup.4 is a divalent hydrocarbon group with 3 to 14 carbon atoms,R.sup.5 is a group having the formula --O(CH.sub.2).sub.b -- or a polyether group having the formula --(OC.sub.n H.sub.2n).sub.c --, wherein b has a value of 1 to 6, n has an average value of 2 to 2.5 and c has a value of 1 to 10,R.sup.6 is an --OSO.sub.3 X group or an --OR.sup.7 group, wherein X is a hydrogen, an alkali or an optionally substituted ammonium ion and R.sup.7 is an alkyl group with 1 to 4 carbon atoms or an acetyl group,a is 0 or 1,with the proviso that, when R.sup.6 represents the --OR.sup.7 group, a=1. The silanes are biologically degradable, resistant to hydrolysis and have pronounced surfactant properties.
摘要翻译：制备通式“IMAGE”的硅烷，其中分子中的R 1，R 2和R 3相同或不同，表示脂族烃基，R 4是具有3至14个碳原子的二价烃基，R 5是具有式 -O（CH 2）b - 或具有式 - （OC n H 2n）c - 的聚醚基团，其中b的值为1至6，n的平均值为2至2.5，c的值为1至10， R6是-OSO3X基团或-OR7基团，其中X是氢，碱或任选取代的铵离子，R 7是具有1至4个碳原子的烷基或乙酰基，a是0或1，与条件是当R6表示-OR7基团时，a = 1。硅烷是生物可降解的，耐水解的并且具有显着的表面活性剂性质。

8. 发明授权

US5221499A Method for the preparation of dialkylmagnesium compounds by the reaction of magnesium hydride with an olefin 失效
标题翻译：通过氢氧化镁与烯烃的反应制备二氨基甲烷化合物的方法
公开(公告)号：US5221499A
公开(公告)日：1993-06-22
申请号：US869260
申请日：1992-04-15
申请人： Klaus-Dieter Klein , Wilfried Knott , Goetz Koerner
发明人： Klaus-Dieter Klein , Wilfried Knott , Goetz Koerner
IPC分类号： C07F3/02
CPC分类号： C07F3/02
摘要： A method for the preparation of dialkylmagnesium compounds is disclosed, wherein magnesium hydride is reacted with an olefin in the presence of a halide of sub-groups IV to VIII of the Periodic Table and in the presence of an ether as reaction medium at a temperature of about between 1 to 300 bar and in a temperature range of about 0.degree. to 200.degree. C. According to the disclosed invention, the magnesium hydride is activated by grinding to a particle size of .ltoreq.10 .mu.m and the method is carried out in the absence of complex catalysts. The grinding of the magnesium hydride takes place prior to the reaction with the olefin, but may also be conducted during the reaction.
摘要翻译：公开了一种制备二烷基镁化合物的方法，其中氢化镁与烯烃在元素周期表的Ⅳ-Ⅷ族Ⅷ族卤化物存在下反应，在乙醚存在下，作为反应介质，在温度为约1至300巴，在约0至200℃的温度范围内。根据所公开的发明，通过研磨将氢化镁活化至粒径为10μm的方法，并进行该方法在没有复合催化剂的情况下。氢化镁的研磨在与烯烃反应之前进行，但也可以在反应期间进行。

9. 发明授权

US08957009B2 Linear polydimethylsiloxane-polyether copolymers having amino and/or quaternary ammonium groups and use thereof 有权
标题翻译：具有氨基和/或季铵基团的线性聚二甲基硅氧烷 - 聚醚共聚物及其用途
公开(公告)号：US08957009B2
公开(公告)日：2015-02-17
申请号：US13520091
申请日：2010-12-29
申请人： Frank Schubert , Wilfried Knott , Michael Ferenz , Klaus-Dieter Klein , Tobias Maurer , Ralph Scheuermann , Bernard William Kluesener , Rajan Keshav Panandiker
发明人： Frank Schubert , Wilfried Knott , Michael Ferenz , Klaus-Dieter Klein , Tobias Maurer , Ralph Scheuermann , Bernard William Kluesener , Rajan Keshav Panandiker
IPC分类号： C08G77/388 , C08G77/46 , A61K8/898 , A61Q19/00 , D06M15/643 , D06M15/647 , A61Q5/00
CPC分类号： C08G77/46 , A61K8/898 , A61Q5/00 , A61Q19/00 , C08G77/388 , D06M15/6436 , D06M15/647
摘要： Linear polydimethylsiloxane-polyether copolymers with amino and/or quaternary ammonium groups, obtainable by the reaction of organopolysiloxanes functionalized with secondary aminoalkyl groups with the reaction products formed from compounds containing epoxy groups and amines, the use thereof and process for preparation thereof.
摘要翻译：具有氨基和/或季铵基团的线性聚二甲基硅氧烷 - 聚醚共聚物，其可通过用仲氨基烷基官能化的有机聚硅氧烷与由含有环氧基和胺的化合物形成的反应产物的反应获得，其用途及其制备方法。

10. 发明申请

US20120308494A1 NOVEL LINEAR POLYDIMETHYLSILOXANE-POLYETHER COPOLYMERS HAVING AMINO AND/OR QUATERNARY AMMONIUM GROUPS AND USE THEREOF 有权
标题翻译：具有氨基和/或季铵基团的新型线性聚二甲基硅氧烷聚合物共聚物及其用途
公开(公告)号：US20120308494A1
公开(公告)日：2012-12-06
申请号：US13520091
申请日：2010-12-29
申请人： Frank Schubert , Wilfried Knott , Michael Ferenz , Klaus-Dieter Klein , Tobias Maurer , Ralph Scheurmann , Bernhard William Kluesener , Rajan Keshav Panandiker
发明人： Frank Schubert , Wilfried Knott , Michael Ferenz , Klaus-Dieter Klein , Tobias Maurer , Ralph Scheurmann , Bernhard William Kluesener , Rajan Keshav Panandiker
IPC分类号： C08G77/388 , A61Q19/10 , A61Q5/12 , A61Q5/06 , D06M15/647 , A61Q5/10 , A61Q15/00 , A61K47/34 , A61Q17/02 , A61K8/898 , A61Q17/04
CPC分类号： C08G77/46 , A61K8/898 , A61Q5/00 , A61Q19/00 , C08G77/388 , D06M15/6436 , D06M15/647
摘要： Linear polydimethylsiloxane-polyether copolymers with amino and/or quaternary ammonium groups, obtainable by the reaction of organopolysiloxanes functionalized with secondary aminoalkyl groups with the reaction products formed from compounds containing epoxy groups and amines, the use thereof and process for preparation thereof.
摘要翻译：具有氨基和/或季铵基团的线性聚二甲基硅氧烷 - 聚醚共聚物，可通过用仲氨基烷基官能化的有机聚硅氧烷与由含有环氧基和胺的化合物形成的反应产物的反应获得，其用途及其制备方法。

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