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1. 发明授权

US5688898A Polyesters production process 失效
标题翻译：聚酯生产工艺
公开(公告)号：US5688898A
公开(公告)日：1997-11-18
申请号：US734656
申请日：1996-10-21
申请人： Kamlesh Kumar Bhatia
发明人： Kamlesh Kumar Bhatia
IPC分类号： C08G63/78 , C08G63/02 , C08F6/00
CPC分类号： C08G63/78
摘要： An atmospheric pressure process for the continuous production of polyester is disclosed wherein a melt of bis(3-hydroxy propyl) terephthalate, or its low molecular oligomers, obtained by esterifying terephthalic acid or transesterifying dimethyl terephthalate with propylene glycol, is intimately contacted with an inert gas to facilitate polymerization and removal of the reaction by-products. The propylene glycol evolved and the inert gas are recycled.
摘要翻译：公开了用于连续生产聚酯的常压法，其中通过酯化对苯二甲酸或用丙二醇酯交换对苯二甲酸二甲酯来获得的双（3-羟基丙基）对苯二甲酸酯或其低分子量低聚物的熔体与惰性物质紧密接触气体以促进反应副产物的聚合和除去。丙二醇放出，惰性气体被回收。

2. 发明授权

US07201289B2 Method for introducing a catalyst solution into a coating formulation 失效
标题翻译：将催化剂溶液引入涂料制剂中的方法
公开(公告)号：US07201289B2
公开(公告)日：2007-04-10
申请号：US10869646
申请日：2004-06-16
申请人： Kamlesh Kumar Bhatia
发明人： Kamlesh Kumar Bhatia
IPC分类号： A62C13/62
CPC分类号： B05B7/2408 , B05B7/2405 , B05B7/2472 , B05B7/2478
摘要： A method for introducing a polymerization catalyst into a coating formulation as the formulation flows from a reservoir includes the steps of: opening the first end of a sealed dispenser holding a predetermined volume of a polymerization catalyst solution and inserting the dispenser into the reservoir such that the open end of the dispenser is positioned near the outlet of the reservoir; with the dispenser so positioned, opening the second end of the dispenser to atmosphere. The head of the liquid coating formulation in the reservoir prevents flow of the catalyst solution from the dispenser until the liquid coating formulation flows from the reservoir into the flow channel. Thus, the catalyst solution mixes with the coating formulation in a way that a predetermined concentration of the catalyst solution is maintained in the coating formulation as the coating formulation flows from the reservoir.
摘要翻译：当制剂从储存器流动时，将聚合催化剂引入涂料制剂中的方法包括以下步骤

3. 发明授权

US07028921B2 Catalyst solution dispenser for a hand-held liquid spraying apparatus 失效
标题翻译：用于手持式液体喷涂装置的催化剂溶液分配器
公开(公告)号：US07028921B2
公开(公告)日：2006-04-18
申请号：US10869677
申请日：2004-06-16
申请人： Kamlesh Kumar Bhatia
发明人： Kamlesh Kumar Bhatia
IPC分类号： A62C13/62 , A63C13/66 , A63C35/58 , B05B9/03
CPC分类号： B05B7/2408 , B05B7/2405 , B05B7/2472 , B05B7/2478
摘要： A dispenser for dispensing a polymerization catalyst solution into a liquid coating formulation has a cross sectional area “a” given by the relationship: a≅P·A·[W/w]·10−6, where “A” is the cross sectional area of the reservoir holding a liquid coating formulation having “W” weight percent of solids; “w” is the weight percent of catalyst in the dispenser; and P is the ratio by weight of the catalyst to the solids desired in the finished coating, in parts per million.
摘要翻译：用于将聚合催化剂溶液分配到液体涂料制剂中的分配器具有由以下关系给出的横截面积“a”：<？in-line-formula description =“In-line Formulas”end =“lead”？>a≅ PA [W / W] .10 ，<？in-line-formula description =“In-line formula”end =“tail”？>其中“A”是横截面积储存器容纳具有“W”重量百分比的固体的液体涂料制剂; “w”是分配器中催化剂的重量百分比; 和P是催化剂与成品涂料中所需固体的重量比，以百万分之几。

4. 发明授权

US06407266B2 Continuous process for the manufacture of anhydro sugar alcohols and reactor useful therefor 失效
标题翻译：用于制造用于其的有用的脱水糖醇和反应器的连续方法
公开(公告)号：US06407266B2
公开(公告)日：2002-06-18
申请号：US09864466
申请日：2001-05-24
申请人： Kamlesh Kumar Bhatia
发明人： Kamlesh Kumar Bhatia
IPC分类号： C07D49304
CPC分类号： C07D493/04
摘要： This invention concerns a process for the manufacture of anhydro- and dianhydro-hexitols, pentitols, and tetritols by the dehydration of sugar alcohols (alditols) in the presence of a dehydration catalyst.
摘要翻译：本发明涉及通过在脱水催化剂存在下脱水糖醇（糖醇）来制备脱水 - 和二脱水 - 己醇，戊醇和四异恶唑的方法。

5. 发明授权

US5856423A Apparatus and process for a polycondensation reaction 失效
标题翻译：缩聚反应的装置和方法
公开(公告)号：US5856423A
公开(公告)日：1999-01-05
申请号：US771494
申请日：1996-12-23
申请人： Kamlesh Kumar Bhatia
发明人： Kamlesh Kumar Bhatia
IPC分类号： B01J19/18 , C08G63/78 , C08G64/00
CPC分类号： B01J19/1887 , C08G63/785 , B01J2219/182
摘要： An improved process and apparatus for the production of a polyester or other condensation polymer is disclosed. In particular, polymerization is conducted in a reaction vessel equipped with a specially designed agitator that exposes the polymer melt partially filling the reaction vessel to inert gas flowing through the vessel. The agitator comprises a plurality of elements that lift a portion of a polymer melt in the reaction vessel and generate films of the polymer melt which films extends in planes that are parallel to the axis of the agitator and the flow of gas through the reaction vessel. In a preferred process, a melt of bis(2-hydroxyethyl) terephthalate, or its low molecular oligomers, obtained by esterifying terephthalic acid or transesterifying dimethyl terephthalate with ethylene glycol, is contacted with an inert gas at about atmospheric pressure in order to remove the reaction by-products and facilitate polymerization.
摘要翻译：公开了用于生产聚酯或其它缩合聚合物的改进方法和设备。特别地，在装有特别设计的搅拌器的反应容器中进行聚合，所述搅拌器将部分填充反应容器的聚合物熔体暴露于流过容器的惰性气体。搅拌器包括多个元件，其提升反应容器中聚合物熔体的一部分并产生聚合物熔体的膜，该膜在平行于搅拌器的轴线的平面中延伸，并且气体通过反应容器流动。在优选的方法中，通过将对苯二甲酸酯或酯交换对苯二甲酸二甲酯与乙二醇酯酯化的双（2-羟乙基）对苯二甲酸酯或其低分子量低聚物的熔体在大气压下与惰性气体接触，以除去反应副产物并促进聚合。

6. 发明授权

US5849849A Polyesters production process 失效
标题翻译：聚酯生产工艺
公开(公告)号：US5849849A
公开(公告)日：1998-12-15
申请号：US847545
申请日：1997-04-23
申请人： Kamlesh Kumar Bhatia
发明人： Kamlesh Kumar Bhatia
IPC分类号： C08G63/78
CPC分类号： C08G63/78
摘要： An atmospheric pressure process for the continuous production of polyester is disclosed wherein a melt of bis(3-hydroxy propyl) terephthalate, or its low molecular oligomers, obtained by esterifying terephthalic acid or transesterifying dimethyl terephthalate with propylene glycol, is intimately contacted with an inert gas to facilitate polymerization and removal of the reaction by-products. The propylene glycol evolved and the inert gas are recycled.
摘要翻译：公开了用于连续生产聚酯的常压法，其中通过酯化对苯二甲酸或用丙二醇酯交换对苯二甲酸二甲酯来获得的双（3-羟基丙基）对苯二甲酸酯或其低分子量低聚物的熔体与惰性物质紧密接触气体以促进反应副产物的聚合和除去。丙二醇放出，惰性气体被回收。

7. 发明授权

US4096192A Process for the preparation of 2-methyl-1,3-propanediol 失效
标题翻译： 2-甲基-1,3-丙二醇的制备方法
公开(公告)号：US4096192A
公开(公告)日：1978-06-20
申请号：US672033
申请日：1976-03-30
申请人： Kamlesh Kumar Bhatia , Charles Carmen Cumbo
发明人： Kamlesh Kumar Bhatia , Charles Carmen Cumbo
IPC分类号： C07C29/16 , C07C27/00 , C07C29/10 , C07C29/132 , C07C29/141 , C07C31/20 , C07C67/00 , C07D319/06 , C07C29/00
CPC分类号： C07D319/06 , C07C29/10 , C07C29/141
摘要： A process for the preparation of 2-methyl-1,3-propanediol (MPD) by recycling mixed diols from the process for the preparation of 1,4-butanediol from acrolein and aliphatic diols until the final product is essentially 1,4-butanediol and MPD.
摘要翻译：通过从丙烯醛和脂族二醇制备1,4-丁二醇的方法中回收混合的二醇直到最终产物基本上为1,4-丁二醇来制备2-甲基-1,3-丙二醇（MPD）的方法和MPD。

8. 发明授权

US07063745B2 Coating formulation kit including a catalyst solution dispenser for a hand-held liquid spraying apparatus 失效
标题翻译：涂料制剂试剂盒，包括用于手持式液体喷涂装置的催化剂溶液分配器
公开(公告)号：US07063745B2
公开(公告)日：2006-06-20
申请号：US10869702
申请日：2004-06-16
申请人： Kamlesh Kumar Bhatia
发明人： Kamlesh Kumar Bhatia
IPC分类号： B05B7/00
CPC分类号： B05B7/2408 , B05B7/2405 , B05B7/2472 , B05B7/2478
摘要： A kit for forming a multi-component coating formulation for application using a hand-held spraying apparatus to produce a finished coating on a surface comprises a first and a second container holding respective first and second components of a multi-component coating formulation. The kit also includes at least one dispenser in the form a generally tubular body member having a closure at both a first and a second end thereof. The dispenser holds a predetermined volume of a polymerization catalyst solution having “w” weight percent of catalyst therein.The dispenser has a predetermined cross sectional area “a” given by the relationship: a≅P·A·[W/w]·10−6, where “A” is the cross sectional area of the reservoir holding a liquid coating formulation having “W” weight percent of solids; and P is the ratio by weight of the catalyst to the solids desired in the finished coating, in parts per million.
摘要翻译：用于形成用于使用手持喷涂装置在表面上生产成品涂层的多组分涂料配方的试剂盒包括容纳多组分涂料制剂的相应的第一和第二组分的第一和第二容器。套件还包括至少一个分配器，其形式为大体上管状的本体构件，在其第一和第二端都具有封闭件。分配器保持预定体积的在其中具有“w”重量百分比的催化剂的聚合催化剂溶液。分配器具有由以下关系给出的预定横截面积“a”：<？in-line-formula description =“In-line Formulas”end =“lead”？>a≅PA[W / w] .10 ^{-6 ，<？in-line-formula description =“In-line Formulas”end =“tail”？>其中“A”是储存液体涂料配方的储存器的横截面面积，具有“W “重量百分比的固体; 和P是催化剂与成品涂料中所需固体的重量比，以百万分之几。}

9. 发明授权

US5677415A Apparatus and process for a polycondensation reaction 失效
标题翻译：缩聚反应的装置和方法
公开(公告)号：US5677415A
公开(公告)日：1997-10-14
申请号：US625571
申请日：1996-03-28
申请人： Kamlesh Kumar Bhatia
发明人： Kamlesh Kumar Bhatia
IPC分类号： B01J19/18 , C08G63/78 , C08G63/00
CPC分类号： B01J19/1887 , C08G63/785 , B01J2219/182
摘要： An improved process and apparatus for the production of polyester or other polycondesation polymers is disclosed. In particular, polymerization is conducted in a reaction vessel equipped with a specially designed agitator that exposes the polymer melt partially filling the reaction vessel to inert gas flowing through the vessel. The agitator comprises a plurality of elements that lift a portion of a polymer melt in the reaction vessel and generate films of the polymer melt which films extends in planes that are substantially parallel to the axis of the agitator and the flow of gas through the reaction vessel. In a preferred process, a melt of dihydroxy ethyl terephthalate, or its low molecular oligomers, obtained by esterifying terephthalic acid or transesterifying dimethyl terephthalate with ethylene glycol, is intimately contacted with an inert gas at about atmospheric pressure in order to remove the reaction by-products and facilitate polymerization.
摘要翻译：公开了用于生产聚酯或其它聚合物聚合物的改进的方法和设备。特别地，在装有特别设计的搅拌器的反应容器中进行聚合，所述搅拌器将部分填充反应容器的聚合物熔体暴露于流过容器的惰性气体。搅拌器包括多个元件，其提升反应容器中的聚合物熔体的一部分并产生聚合物熔体的膜，该膜在基本上平行于搅拌器的轴线的平面中延伸，并且气体通过反应容器。在优选的方法中，通过酯化对苯二甲酸或酯交换对苯二甲酸二甲酯与乙二醇获得的对苯二甲酸二羟乙酯或其低分子量低聚物的熔体在约大气压下与惰性气体紧密接触，以除去副反应，产品，促进聚合。

10. 发明授权

US06864378B2 Integrated continuous process for anhydro sugar alcohol manufacture 失效
标题翻译：一体化连续工艺的脱水醇制造
公开(公告)号：US06864378B2
公开(公告)日：2005-03-08
申请号：US10414607
申请日：2003-04-16
申请人： Kamlesh Kumar Bhatia
发明人： Kamlesh Kumar Bhatia
IPC分类号： C07B61/00 , C07D493/04
CPC分类号： C07D493/04
摘要： An integrated continuous process is disclosed for the manufacture of high purity, polymer grade dianhydro sugar alcohols, such as isosorbide, by the dehydration of corresponding sugar alcohols. The water vapors evolved during the dehydration are used to separate product dianhydro sugar alcohols from the high boiling byproducts in the reaction mass. The product is recovered from the vapor stream as high purity crystals. The high boiling reaction byproducts are recycled.
摘要翻译：公开了通过相应的糖醇的脱水来制造高纯度聚合物级二氢糖醇如异山梨醇的综合连续方法。在脱水过程中发生的水蒸汽用于将反应物质中的高沸点副产物的产物二氢糖醇分离出来。产物从蒸气流中以高纯度晶体回收。高沸点反应副产物被回收利用。

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