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1. 发明授权

US5922191A Foam control using a fluidized bed of particles 失效
标题翻译：使用颗粒流化床进行泡沫控制
公开(公告)号：US5922191A
公开(公告)日：1999-07-13
申请号：US882316
申请日：1997-06-25
申请人： Clara Mata , Jose Guitian , Daniel D. Joseph , Julio Krasuk
发明人： Clara Mata , Jose Guitian , Daniel D. Joseph , Julio Krasuk
IPC分类号： B01D19/02 , B01D19/04 , B01J8/22 , B01J19/00
CPC分类号： B01D19/02 , B01D19/04 , B01J19/002 , B01J8/22 , B01J2219/00162 , B01J2219/0025
摘要： A process for suppressing foam formation in a vessel includes the steps of feeding a liquid and a gas to a vessel at a liquid velocity and a gas velocity respectively; adding particles of a solid material to the liquid, the particles having a particle size and particle density; and selecting at least one of the liquid velocity, particle size and particle density so as to fluidize the particles in the liquid, whereby foam formation in the vessel is suppressed. The particles are preferably liquid phase phobic particles.
摘要翻译：抑制容器中泡沫形成的方法包括以液体速度和气体速度分别向容器供给液体和气体的步骤; 向液体中加入固体物质颗粒，颗粒具有颗粒尺寸和颗粒密度; 并选择液体速度，粒度和颗粒密度中的至少一种，以使液体中的颗粒流化，从而抑制容器中的泡沫形成。颗粒优选为液相恐怕颗粒。

2. 发明授权

US4751210A Regeneration of an iron based natural catalyst used in the hydroconversion of heavy crudes and residues 失效
标题翻译：用于重质原油和残渣加氢转化的铁基天然催化剂的再生
公开(公告)号：US4751210A
公开(公告)日：1988-06-14
申请号：US52403
申请日：1987-05-21
申请人： M. M. Ramirez de Agudelo , Jose M. Larrauri Derteano , Julio Krasuk
发明人： M. M. Ramirez de Agudelo , Jose M. Larrauri Derteano , Julio Krasuk
IPC分类号： B01J23/94 , B01J38/16 , C10G11/04 , C10G49/02 , C10G47/04
CPC分类号： B01J38/16 , B01J23/94 , C10G11/04 , C10G49/02
摘要： A process for regenerating a spent, naturally occurring catalyst characterized by an iron content of about 10 to 70 wt. % as metal comprises contacting the spent catalyst with a mixture of water vapor and air in a water vapor/air ratio of between 1:1 to 20:1 at a flow rate of about 0.1 to 50 l/min., a temperature of about 200.degree. to 700.degree. C., a pressure of about 0.3 to 80 atmospheres for a time of about 0.1 to 20 hours so as to obtain a regenerated catalyst having a crystallinity value of about 1.0 to 6.5.
摘要翻译：用于再生废弃的天然存在的催化剂的方法，其特征在于铁含量为约10至70wt。％的金属包括使废催化剂与水蒸气和空气的混合物在水蒸气/空气比为1:1至20:1之间，流速为约0.1-50升/分钟，约为 200〜700℃，压力为约0.3〜80个大气压的时间约0.1〜20小时，得到结晶度为约1.0〜6.5的再生催化剂。

3. 发明授权

US4676886A Process for producing anode grade coke employing heavy crudes characterized by high metal and sulfur levels 失效
标题翻译：使用重金属和硫含量高的重质原油生产阳极级焦炭的方法
公开(公告)号：US4676886A
公开(公告)日：1987-06-30
申请号：US892309
申请日：1986-08-04
申请人： Georgette Rahbe , Roger Marzin , Ivan Cavicchioli , Julio Krasuk , Rodolfo B. Solari
发明人： Georgette Rahbe , Roger Marzin , Ivan Cavicchioli , Julio Krasuk , Rodolfo B. Solari
IPC分类号： C10B55/00 , C10G67/04 , C10G69/06 , C10G31/14
CPC分类号： C10G67/0445 , C10B55/00 , C10G69/06
摘要： The present invention is drawn to a process for the production of anode grade coke from a hydrocarbon feed characterized by high levels of sulfurs and metals. The hydrocarbon feed is hydrocracked in a hydrocracking reactor so as to produce an overhead effluent which is fed to a hot separator wherein a light hydrocarbon stream and a slurry hydrocracked product are produced. The hydrocracked product is fed to a separator and mixed with a solvent wherein the solids are separated out from the hydrocracked residual so as to produce a clean hydrocracked residual which is fed to a coking drum and coked so as to leave a mass of green anode grade coke.
摘要翻译：本发明涉及一种以高含量硫磺和金属为特征的烃源生产阳极级焦炭的方法。烃加料在加氢裂化反应器中进行加氢裂化，以产生塔顶流出物，该塔顶流出物被送入热分离器，其中产生轻烃流和浆料加氢裂化产物。将加氢裂化产物进料到分离器并与溶剂混合，其中固体从加氢裂化的残余物中分离出来，以产生干净的加氢裂化残余物，将其进料到焦化鼓并焦化，以便留下大量的阳极阳极级可乐。

4. 发明授权

US4655903A Recycle of unconverted hydrocracked residual to hydrocracker after removal of unstable polynuclear hydrocarbons 失效
标题翻译：去除不稳定多核烃后，将未转化的加氢裂化残渣循环回加氢裂化器
公开(公告)号：US4655903A
公开(公告)日：1987-04-07
申请号：US735694
申请日：1985-05-20
申请人： Georgette Rahbe , Roger Marzin , Ivan Cavicchioli , Julio Krasuk
发明人： Georgette Rahbe , Roger Marzin , Ivan Cavicchioli , Julio Krasuk
IPC分类号： C10G67/04 , C10G37/00
CPC分类号： C10G67/0445
摘要： Hydrocracking and separating process for upgrading unconverted residuals so as to increase liquid yields while at the same time decrease fouling of the hydrocracking reactor upon recycling of the upgraded residual to the hydrocracker. The unconverted residual from the hydrocracking unit is treated in a separation stage with a light hydrocarbon solvent so as to remove the polynuclear hydrocarbons from the residual prior to recycling.
摘要翻译：用于升级未转化残余物的加氢裂化和分离过程，以便提高液体产率，同时减少加氢裂化反应器在将升级的残余物再循环至加氢裂化器时的结垢。来自加氢裂化装置的未转化残余物在与轻质烃溶剂的分离阶段进行处理，以便在再循环之前从残余物中除去多核烃。

5. 发明授权

US4572781A Solvent deasphalting in solid phase 失效
标题翻译：固相溶剂脱沥青
公开(公告)号：US4572781A
公开(公告)日：1986-02-25
申请号：US584955
申请日：1984-02-29
申请人： Julio Krasuk , Rodolfo B. Solari , Luis G. Aquino , Jose V. Rodriguez , Alejandro Granados
发明人： Julio Krasuk , Rodolfo B. Solari , Luis G. Aquino , Jose V. Rodriguez , Alejandro Granados
IPC分类号： C10G21/00 , C10C3/00 , C10C3/08
CPC分类号： C10G21/003
摘要： A process for separating substantially dry asphaltenes of high softening point from heavy hydrocarbon material comprising:(a) admixing heavy hydrocarbon material containing asphaltenes with a solution of deasphalted oil and an aliphatic hydrocarbon precipitant in a first mixing zone to form a mixture and precipitate asphaltenes;(b) in a first separation zone the mixture from step (a) into (i) a first solution of deasphalted oil and precipitant and (ii) a slurry of solid asphaltene particles in a solution of precipitant and desasphalted oil;(c) separating the first solution of step (b) to obtain said precipitant and the deasphalted oil almost free of asphaltenes;(d) introducing the slurry of asphaltenes of step (b) into a second mixing zone and washing the slurry with a volume of fresh precipitant to remove deasphalted oil;(e) introducing the mixture from the second mixing zone into a second separation zone that comprises a centrifugal decanter to separate a liquid phase from a highly concentrated slurry of solid asphaltenes;(f) recycling the liquid phase from the second separation zone to said first mixing zone;(g) introducing the concentrated slurry of solid asphaltenes from the second separation zone into a solvent removal system to recover the solvent and to obtain a product comprising fine particles of high softening point asphaltenes; and(h) recycling the solvent recovered in the solvent removal system to the second mixing zone.
摘要翻译：从重质烃材料中分离出高软化点的基本上干燥的沥青质的方法，包括：（a）在第一混合区中将含有沥青质的重质烃材料与脱沥青油和脂族烃沉淀剂的溶液混合以形成混合物并沉淀沥青质; （b）在第一分离区中将来自步骤（a）的混合物转化为（i）脱沥青油和沉淀剂的第一溶液和（ii）固体沥青质颗粒在沉淀剂和脱沥青油溶液中的浆料; （c）分离步骤（b）的第一溶液以获得所述沉淀剂，脱沥青油几乎不含沥青质; （d）将步骤（b）的沥青质浆液引入第二混合区，并用一定体积的新鲜沉淀剂洗涤浆料以除去脱沥青的油; （e）将来自第二混合区的混合物引入第二分离区，该分离区包括离心沉降器，以将液相与固体沥青质的高浓度浆料分离; （f）将液相从第二分离区再循环到所述第一混合区; （g）将固体沥青质的浓缩浆料从第二分离区引入溶剂除去系统中以回收溶剂，并获得包含高软化点沥青质细颗粒的产品; 和（h）将在溶剂去除系统中回收的溶剂回收到第二混合区。

6. 发明授权

US5922190A Process for suppressing foam formation in a bubble column reactor 失效
标题翻译：抑制泡罩塔反应器中泡沫形成的方法
公开(公告)号：US5922190A
公开(公告)日：1999-07-13
申请号：US725485
申请日：1996-10-04
申请人： Jose Guitian , Daniel D. Joseph , Julio Krasuk
发明人： Jose Guitian , Daniel D. Joseph , Julio Krasuk
IPC分类号： B01D19/02 , B01D19/04 , B01J8/22 , B01J19/00
CPC分类号： B01J8/22 , B01D19/02 , B01D19/04 , B01J19/002 , B01J2219/00162 , B01J2219/0025
摘要： A process for suppressing foam formation in a bubble column reactor includes the steps of feeding a liquid and a gas to a reactor at a liquid velocity and a gas velocity respectively; and adding particles of a solid material to the liquid, wherein the particles are wettable by the liquid, and whereby foam formation in the reactor is suppressed
摘要翻译：抑制气泡塔型反应器中的泡沫形成的方法包括以液体速度和气体速度将液体和气体供给反应器的步骤; 并将固体材料颗粒加入到液体中，其中颗粒可被液体润湿，从而抑制反应器中的泡沫形成

7. 发明授权

US5166118A Catalyst for the hydrogenation of hydrocarbon material 失效
标题翻译：用于氢化烃材料的催化剂
公开(公告)号：US5166118A
公开(公告)日：1992-11-24
申请号：US340535
申请日：1989-04-19
申请人： Klaus Kretschmar , Ludwig Merz , Klaus Niemann , Jose Guitian , Julio Krasuk , Franzo Marruffo , Klaus Kurzeja
发明人： Klaus Kretschmar , Ludwig Merz , Klaus Niemann , Jose Guitian , Julio Krasuk , Franzo Marruffo , Klaus Kurzeja
IPC分类号： C10C1/20 , C10G1/08 , C10G47/26 , C10M175/00
CPC分类号： C10G1/086 , C10C1/205 , C10G47/26 , C10M175/0041
摘要： A catalyst for the hydrogenation of a hydrocarbon material which is a member selected from the group consisting of red mud, iron oxides, iron ores, hard coals, lignites impregnated with heavy metal salts, carbon black, soots from gasifiers, and cokes produced by the hydrogenation of virgin residues, the catalyst being comprised of at least two separate particle size fractions such that the combined fractions have a particle size distribution between 0.1 and 2,000 microns with 10-40 wt. % of the particles having a particle size greater than 100 microns, and the mixture of fractions not being represented by a straight line when the accumulative weight of the particles vs. particle size which is plotted on log (minus log) vs. log graph paper has a correlation coefficient R.sup.2 less than 0.96 as determined from the equation: ##EQU1## wherein n is the number of experimental points, y is ln [-ln (n/1000)] and x is ln (dp), wherein dp is the particle size (.mu.m) of the particles.
摘要翻译：用于氢化烃材料的催化剂，其是选自红泥，氧化铁，铁矿石，硬煤，浸渍有重金属盐的褐煤，炭黑，来自气化器的烟灰，以及由原始残余物的氢化，催化剂由至少两个分开的粒度级分组成，使得组合级分的粒度分布在0.1至2,000微米之间，10-40重量％当颗粒的累积重量与绘制在对数（减去对数）上的对比粒径相对于对数图纸时，颗粒的粒度大于100微米的颗粒的比例不是直线表示的。具有从以下等式确定的相关系数R2小于0.96：其中n是实验点的数量，y是ln [-ln（n / 1000）]，x是ln（dp），其中dp是颗粒的粒径（μm）。

8. 发明授权

US4851107A Process for the hydrogenation of heavy and residual oils 失效
标题翻译：重油和残油加氢工艺
公开(公告)号：US4851107A
公开(公告)日：1989-07-25
申请号：US105290
申请日：1987-10-07
申请人： Klaus Kretschmar , Ludwig Merz , Klaus Niemann , Jose Guitian , Julio Krasuk , Franzo Marruffo
发明人： Klaus Kretschmar , Ludwig Merz , Klaus Niemann , Jose Guitian , Julio Krasuk , Franzo Marruffo
IPC分类号： C10G1/00 , C10C1/20 , C10G1/08 , C10G47/02 , C10G47/26 , C10M175/00
CPC分类号： C10M175/0041 , C10C1/205 , C10G1/086 , C10G47/26
摘要： A process for the hydrogenation of heavy oils, residual oils, waste oils, used oils, shell oils, and tar sand oils by hydrogenating a slurry of the oil at a partial hydrogen pressure of 50-300 bar, a temperature of 250.degree.-500.degree. C., a space velocity of 0.1-5 T/m.sup.3 h, and a gas/liquid ratio of 100-10000 Nm.sup.3/ T, wherein the additive comprises two different grain size portions, a fine grain portion having a grain size of 90 microns or less and a coarse grain portion having a grain size of 100-1000 microns.
摘要翻译：通过在50-300巴的部分氢气压力下，在250-500℃的温度下氢化油的浆料来氢化重油，残油，废油，二手油，壳油和焦油砂油的方法 ℃，空速为0.1-5T / m3h，气/液比为100-10000Nm 3 / T，其中添加剂包括两个不同的粒度部分，粒度为90微米的细晶粒部分或更小的粗粒部分和粒径为100-1000微米的粗粒部分。

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