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1. 发明授权

US4547487A Process for preparing catalysts 失效
标题翻译：制备催化剂的方法
公开(公告)号：US4547487A
公开(公告)日：1985-10-15
申请号：US495968
申请日：1983-05-19
申请人： Roger F. Vogel , Raymond J. Rennard , Joseph A. Tabacek
发明人： Roger F. Vogel , Raymond J. Rennard , Joseph A. Tabacek
IPC分类号： B01J21/04 , B01J21/06 , B01J23/02 , B01J23/06 , B01J23/10 , B01J23/14 , B01J23/18 , B01J23/28 , B01J23/72 , B01J23/74 , B01J37/00 , B01J37/02 , B01J37/04 , B01J23/30
CPC分类号： B01J21/066 , B01J21/063 , B01J23/28 , B01J37/0009 , B01J37/04
摘要： A process for preparing novel catalysts of increased activity, which comprises mixing alumina with (1) at least one metal compound and (2) an aqueous solution containing at least one dissolved compound therein that imparts to said aqueous solution a pH below 6.
摘要翻译：一种制备增加活性的新型催化剂的方法，其包括将氧化铝与（1）至少一种金属化合物混合，和（2）含有至少一种溶解化合物的水溶液，其中所述溶液赋予所述水溶液pH低于6。

2. 发明授权

US4490479A Process for preparing catalysts 失效
标题翻译：制备催化剂的方法
公开(公告)号：US4490479A
公开(公告)日：1984-12-25
申请号：US495967
申请日：1983-05-19
申请人： Roger F. Vogel , Raymond J. Rennard , Joseph A. Tabacek
发明人： Roger F. Vogel , Raymond J. Rennard , Joseph A. Tabacek
IPC分类号： B01J23/22 , B01J23/88 , C10G45/04 , B01J21/04 , B01J21/06 , B01J23/28
CPC分类号： B01J23/883 , B01J23/22 , B01J23/88 , B01J37/0207 , C10G45/04 , B01J21/063 , B01J21/066
摘要： A process for preparing novel catalysts of increased activity which comprises (1) mixing alumina with at least one metal compound selected from the group consisting of Group IVB metal compounds and compounds of vanadium, chromium, manganese, tungsten, nickel and cobalt and an aqueous solution containing at least one dissolved compound therein that imparts to said aqueous solution a pH below 6 and (2) thereafter adding to the resulting product at least one metal compound not previously added thereto.
摘要翻译：一种制备增加活性的新型催化剂的方法，其包括（1）将氧化铝与至少一种选自ⅣB族金属化合物和钒，铬，锰，钨，镍和钴的化合物和水溶液含有至少一种溶解的化合物，其赋予所述水溶液pH低于6，和（2）然后向所得产物中加入至少一种先前未加入的金属化合物。

3. 发明授权

US4490483A Process for preparing catalysts 失效
标题翻译：制备催化剂的方法
公开(公告)号：US4490483A
公开(公告)日：1984-12-25
申请号：US495966
申请日：1983-05-19
申请人： Roger F. Vogel , Raymond J. Rennard , Joseph A. Tabacek
发明人： Roger F. Vogel , Raymond J. Rennard , Joseph A. Tabacek
IPC分类号： B01J21/06 , B01J23/28 , B01J37/02 , B01J21/04
CPC分类号： B01J21/063 , B01J21/06 , B01J23/28 , B01J37/0205
摘要： A process for preparing novel catalysts of increased activity which comprises (1) mixing alumina with at least a Group IVB metal compound and a molybdenum compound and an aqueous solution containing at least one dissolved compound therein that imparts to said aqueous solution a pH below 6 and (2) thereafter adding to the resulting product at least one metal compound not previously added thereto.
摘要翻译：一种制备增加活性的新型催化剂的方法，其包括（1）将氧化铝与至少一种IVB族金属化合物和钼化合物混合，以及含有至少一种溶解的化合物的水溶液，其中所述水溶液的pH低于6，（2）之后，向所得到的产物中加入至少一种以前未加入的金属化合物。

4. 发明授权

US4399058A Impregnating solution for hydrogenation catalyst manufacture and production thereof 失效
标题翻译：用于氢化催化剂的浸渍溶液的制造及其生产
公开(公告)号：US4399058A
公开(公告)日：1983-08-16
申请号：US241018
申请日：1981-03-06
申请人： John J. Stanulonis , Joseph A. Tabacek , Roger F. Vogel
发明人： John J. Stanulonis , Joseph A. Tabacek , Roger F. Vogel
IPC分类号： B01J23/883 , B01J23/64 , B01J27/24
CPC分类号： B01J23/883
摘要： An aqueous, alkaline impregnating solution for the one-step impregnation of nickel and molybdenum onto a catalyst support is provided by admixing nickel sulfate, preferably an ammoniacal solution of nickel sulfate and an ammoniacal solution of Mo.sup.+VI oxide to form a compatible impregnating solution. Nickel and sulfate ions are present in a ratio of substantially 1 to 1. The use of nickel sulfate in a predissolved ammoniacal solution for admixture with the ammoniacal solution of the Mo.sup.+VI oxide permits a higher metals loading of the impregnating solution and renders the resulting impregnating solution highly suitable for impregnation of nickel and molybdenum onto a catalyst support by the incipient wetness technique in one-step. The catalyst produced using the present impregnating solution is highly active for desulfurization of naphthas, middle distillate oils and asphalt-containing oils.
摘要翻译：通过将硫酸镍，优选硝酸镍的氨溶液和Mo + VI氧化物的氨溶液混合以形成相容的浸渍溶液来提供用于将镍和钼一步浸渍到催化剂载体上的水性碱性浸渍溶液。镍和硫酸根离子以基本上1比1的比例存在。在预溶解的氨溶液中使用硫酸镍与Mo + VI氧化物的氨溶液混合，允许浸渍溶液的较高的金属负载，并使得到浸渍溶液非常适合于通过初始润湿技术在一步中将镍和钼浸渍到催化剂载体上。使用本发明的浸渍溶液制备的催化剂对于石脑油，中间馏分油和含沥青的油的脱硫具有高度的活性。

5. 发明授权

US4285807A Lubricating oil hydrotreating process 失效
标题翻译：润滑油加氢处理工艺
公开(公告)号：US4285807A
公开(公告)日：1981-08-25
申请号：US72232
申请日：1979-09-04
申请人： John J. Stanulonis , Joseph A. Tabacek , Roger F. Vogel
发明人： John J. Stanulonis , Joseph A. Tabacek , Roger F. Vogel
IPC分类号： B01J23/883 , B01J27/12 , B01J37/02 , C10G45/08 , C10G45/04 , B01J37/00 , C10G17/00 , C10G45/60
CPC分类号： B01J37/0201 , B01J23/883 , B01J27/12 , C10G2400/10
摘要： A lube oil feedstock is subjected to hydrotreating in the presence of hydrogen and a fluorine-promoted catalyst comprising nickel and molybdenum on a support wherein the nickel and fluorine are derived from an ammoniacal solution of nickel fluoride. The catalyst can be prepared by contacting the support with an alkaline impregnating solution consisting essentially of NH.sub.4.sup.+, Ni.sup.++, MO.sup.+VI and F.sup.-, said Ni.sup.++ and F.sup.- being supplied from nickel fluoride, in a single step employing the incipient wetness technique. The impregnated support is thereafter heated to drive off the alkaline component of the solution and thereby deposit the fluorine, nickel and molybdenum on the support.
摘要翻译：润滑油原料在氢气存在下进行加氢处理，在载体上含有镍和钼的氟促进催化剂，其中镍和氟源自硝酸镍的氨溶液。催化剂可以通过使载体与基本上由NH4 +，Ni ++，MO + VI和F-组成的碱性浸渍溶液接触来制备，所述Ni ++和F-由氟化镍提供，采用初始润湿技术的单步骤。然后将浸渍的载体加热以驱除溶液的碱性组分，从而将氟，镍和钼沉积在载体上。

6. 发明授权

US4328128A Hydrotreating catalyst and manufacture thereof 失效
标题翻译：加氢处理催化剂及其制造
公开(公告)号：US4328128A
公开(公告)日：1982-05-04
申请号：US72240
申请日：1979-09-04
申请人： John J. Stanulonis , Joseph A. Tabacek , Roger F. Vogel
发明人： John J. Stanulonis , Joseph A. Tabacek , Roger F. Vogel
IPC分类号： B01J27/12 , B01J27/132 , C10G45/08 , B01J37/00 , B01J29/00 , C10G17/00 , C10G45/00
CPC分类号： B01J27/12 , C10G2400/10
摘要： A tungsten-free hydrotreating catalyst is produced by contacting a refractory metal oxide support with an aqueous impregnating solution formed from an ammoniacal solution of nickel fluoride, preferably predissolved, and an Mo.sup.+VI oxide. The impregnating solution consists essentially of NH.sub.4.sup.+, Ni.sup.++, Mo.sup.+VI and F.sup.-, said Ni.sup.++ and F.sup.- being supplied from nickel fluoride and preferably contains nickel and fluoride ions in a ratio of substantially 1 to 2, and is used in an amount necessary for impregnating by the incipient wetness technique in a one-step impregnation. The impregnated catalyst support is then heated to a temperature sufficient to drive off ammonia and thereby deposit fluorine, nickel and molybdenum. The resulting catalyst is highly active for hydrotreating lube oil feedstocks.
摘要翻译：通过使难熔金属氧化物载体与由优选预先溶解的氟化铵的氨溶液和Mo + VI氧化物形成的含水浸渍溶液接触来制备无钨的加氢处理催化剂。浸渍溶液基本上由NH4 +，Ni ++，Mo + VI和F-组成，所述Ni ++和F-由氟化镍提供，优选含有基本上为1至2的比例的镍和氟离子，并且以必要量使用用于初步润湿技术浸渍在一步浸渍中。然后将浸渍的催化剂载体加热到足以驱除氨并由此沉积氟，镍和钼的温度。所得催化剂对加氢处理润滑油原料具有高度的活性。

7. 发明授权

US4318801A Supported nickel-molybdenum catalyst, preparation thereof, and hydrodesulfurization of hydrocarbon fractions using same 失效
$Supported nickel-molybdenum catalyst, preparation thereof, and hydrodesulfurization of hydrocarbon fractions using same$
标题翻译：支持的镍 - 钼催化剂，其制备和使用它们的烃馏分的加氢脱硫
公开(公告)号：US4318801A
公开(公告)日：1982-03-09
申请号：US72233
申请日：1979-09-04
申请人： Henri K. Lese , Raynor T. Sebulsky , John J. Stanulonis , Joseph A. Tabacek , Roger F. Vogel
发明人： Henri K. Lese , Raynor T. Sebulsky , John J. Stanulonis , Joseph A. Tabacek , Roger F. Vogel
IPC分类号： B01J23/883 , C10G45/08 , C10G45/04 , B01J23/64 , B01J27/02 , C10G45/60
CPC分类号： C10G45/08 , B01J23/883
摘要： A nickel-molybdenum catalyst composite is formed by a process which consists essentially of contacting a refractory inorganic oxide support with an aqueous, alkaline impregnating solution consisting essentially of NH.sup.+.sub.4, Ni.sup.++, SO.sub.4 .sup.- and MO.sup.+VI, with substantially all of the Ni.sup.++ being supplied from nickel sulfate, and heating said impregnated support to dry and calcine the catalyst composite. The calcination is an oxidative calcination conducted in the presence of an oxygen-containing gas at a temperature in the range of 427.degree. and about 566.degree. C. such that sulfate remains on said support. The resulting catalyst is used to desulfurize naphthas, middle distillate oils and asphaltic oils.
摘要翻译：一种镍 - 钼催化剂复合材料是通过一种方法形成的，该方法主要包括使耐火无机氧化物载体与基本上由NH + 4，Ni ++，SO4和MO + VI组成的水性碱性浸渍溶液接触，基本上全部为Ni ++由硫酸镍供应，并加热所述浸渍的载体以干燥并煅烧催化剂复合材料。煅烧是在含氧气体的存在下在427℃和约566℃的温度范围内进行的氧化煅烧，使得硫酸盐残留在所述载体上。所得催化剂用于脱硫石脑油，中间馏分油和沥青油。

8. 发明授权

US4285836A Impregnating solution for hydrotreating catalyst manufacture and production thereof 失效
标题翻译：用于加氢处理催化剂制造及其生产的浸渍溶液
公开(公告)号：US4285836A
公开(公告)日：1981-08-25
申请号：US72241
申请日：1979-09-04
申请人： John J. Stanulonis , Joseph A. Tabacek , Roger F. Vogel
发明人： John J. Stanulonis , Joseph A. Tabacek , Roger F. Vogel
IPC分类号： B01J23/883 , B01J37/02 , C10G49/04 , B01J37/00 , B01J23/64 , B01J27/24 , B01J29/00
CPC分类号： B01J23/883 , B01J37/0201 , C10G49/04
摘要： An aqueous, alkaline impregnating solution for the one-step impregnation of fluorine, nickel and molybdenum onto a catalyst support is provided by admixing nickel fluoride, preferably an ammoniacal solution of nickel fluoride and an ammoniacal solution of Mo.sup.+VI to form a compatible impregnating solution consisting essentially of NH.sub.4.sup.+, Ni.sup.++, Mo.sup.+VI and F.sup.-. Nickel and fluorine ions are present in a ratio of substantially 1 to 2. The use of nickel fluoride in a predissolved ammoniacal solution for admixture with the ammoniacal solution of the Mo.sup.+VI renders the resulting impregnating solution highly suitable for impregnation of fluorine, nickel and molybdenum onto a catalyst support by the incipient wetness technique in one-step. The catalyst produced using the present impregnating solution is highly active for hydrotreating lubricating oils.
摘要翻译：通过将氟化镍，优选氟化铵的氨溶液和Mo + VI的氨溶液混合以形成相容的浸渍溶液来提供用于将氟，镍和钼一步浸渍到催化剂载体上的水性碱性浸渍溶液主要由NH4 +，Ni ++，Mo + VI和F-组成。镍和氟离子以基本上为1比2的比率存在。在预溶解的氨溶液中与氟化铵的氨溶液混合使用氟化镍使得所得浸渍溶液非常适合于浸渍氟，镍和钼通过初始湿度技术在一步中催化剂载体上。使用本发明的浸渍溶液制备的催化剂对于加氢处理润滑油是高活性的。

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