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1. 发明授权

US08003815B2 Method for preparation of cross-condensed compound between amino acids and aminoalkylsilane having alkoxy groups using microwave 失效
标题翻译：使用微波制备具有烷氧基的氨基酸和氨基烷基硅烷之间交联的化合物的方法
公开(公告)号：US08003815B2
公开(公告)日：2011-08-23
申请号：US12739598
申请日：2008-02-22
申请人： Ik Mo Lee , Dong Hwan Lee , Ho Sub Kim , Sang Eon Park
发明人： Ik Mo Lee , Dong Hwan Lee , Ho Sub Kim , Sang Eon Park
IPC分类号： C07F7/04
CPC分类号： C07F7/1892
摘要： The present invention provides a method of preparing a cross-condensed compound of an amino-acid derivative and (aminoalkyl)trialkoxysilane using microwave, including: irradiating and heating an amino-acid derivative and (aminoalkyl)trialkoxysilane in a microwave reactor to obtain a reaction product (step 1); and refining the reaction product obtained in the step 1 by removing an unreacted solid material from the reaction product and then leaving the reaction product at room temperature under vacuum to remove excess (aminoalkyl)trialkoxysilane therefrom (step 2). According to the method, since a cross-condensation reaction is performed using microwave, unlike a conventional condensation reaction, economic efficiency is increased due to no catalyst, short reaction time and no solvent. Further, the yield and selectivity of products is increased, and the condensation reaction can be environment-friendly performed because a solvent which can badly influence the environment may not be used.
摘要翻译：本发明提供了使用微波制备氨基酸衍生物和（氨基烷基）三烷氧基硅烷的交联稠合化合物的方法，包括：在微波反应器中照射加热氨基酸衍生物和（氨基烷基）三烷氧基硅烷，得到反应产品（步骤1）; 并通过从反应产物中除去未反应的固体物质，然后在真空下将反应产物在室温下离心以从其中除去过量的（氨基烷基）三烷氧基硅烷，从而精制步骤1中获得的反应产物（步骤2）。根据该方法，由于使用微波进行交联缩合反应，与常规的缩合反应不同，由于没有催化剂，反应时间短，无溶剂，经济效率提高。此外，产物的产率和选择性提高，并且缩合反应可以是环境友好的，因为可能不会使用可能严重影响环境的溶剂。

2. 发明授权

US06689427B2 Group IV metal precursors and a method of chemical vapor deposition using the same 有权
标题翻译： IV族金属前体和使用其的化学气相沉积方法
公开(公告)号：US06689427B2
公开(公告)日：2004-02-10
申请号：US09933736
申请日：2001-08-22
申请人： Yo Sep Min , Young Jin Cho , Dae Sig Kim , Ik Mo Lee , Sun Kwon Lim , Wan In Lee , Bo Hyun Choi
发明人： Yo Sep Min , Young Jin Cho , Dae Sig Kim , Ik Mo Lee , Sun Kwon Lim , Wan In Lee , Bo Hyun Choi
IPC分类号： C23C1600
CPC分类号： C23C16/409 , C07C225/14
摘要： An organometallic precursor of a formula M(L)2 for use in formation of metal oxide thin films, in which M is a group IV metal ion having a charge of +4 and L is a tridentate ligand having a charge of −2, the ligand being represented by the following formula (I): wherein each of R1 and R2, independently, is a linear or branched C1-8 alkyl group; and R3 is a linear or branched C1-8 alkylene group. Also disclosed is a chemical vapor deposition method wherein a metal oxide thin film is formed on a substrate using the organometallic precursor. The precursor exhibits excellent volatility, thermal property and hydrolytic stability and is particularly suitable for the deposition of a multi-component metal oxide thin film containing a group IV metal such as titanium.
摘要翻译：用于形成金属氧化物薄膜的式M（L）2的有机金属前体，其中M是电荷为+4的第IV族金属离子，L为带电荷的三齿配体，配体由下式（I）表示：其中R 1和R 2各自独立地为直链或支链C 1-8烷基; 且R 3为直链或支链C 1-8亚烷基。还公开了一种化学气相沉积方法，其中使用有机金属前体在基板上形成金属氧化物薄膜。前体表现出优异的挥发性，热性质和水解稳定性，特别适用于沉积含有IV族金属如钛的多组分金属氧化物薄膜。

3. 发明申请

US20100249444A1 Method for Preparation of Cross-Condensed Compound Between Amino Acids and Aminoalkylsilane Having Alkoxy Groups Using Microwave 失效
标题翻译：使用微波制备具有烷氧基的氨基酸和氨基烷基硅烷之间交联化合物的方法
公开(公告)号：US20100249444A1
公开(公告)日：2010-09-30
申请号：US12739598
申请日：2008-02-22
申请人： Ik Mo Lee , Dong Hwan Lee , Ho Sub Kim , Sang Eon Park
发明人： Ik Mo Lee , Dong Hwan Lee , Ho Sub Kim , Sang Eon Park
IPC分类号： C07F7/10
CPC分类号： C07F7/1892
摘要： The present invention provides a method of preparing a cross-condensed compound of an amino-acid derivative and (aminoalkyl) trialkoxysilane using microwave, including: irradiating and heating an amino-acid derivative and (aminoalkyl) trialkoxysilane in a microwave reactor to obtain a reaction product (step 1); and refining the reaction product obtained in the step 1 by removing an unreacted solid material from the reaction product and then leaving the reaction product at room temperature under vacuum to remove excess (aminoalkyl) trialkoxysilane therefrom (step 2). According to the method, since a cross-condensation reaction is performed using microwave, unlike a conventional condensation reaction, economic efficiency is increased due to no catalyst, short reaction time and no solvent. Further, the yield and selectivity of products is increased, and the condensation reaction can be environment-friendly performed because a solvent which can badly influence the environment may not be used.
摘要翻译：本发明提供了使用微波制备氨基酸衍生物和（氨基烷基）三烷氧基硅烷的交联稠合化合物的方法，包括：在微波反应器中照射加热氨基酸衍生物和（氨基烷基）三烷氧基硅烷，得到反应产品（步骤1）; 并通过从反应产物中除去未反应的固体物质，然后在真空下将反应产物在室温下离心以从其中除去过量的（氨基烷基）三烷氧基硅烷，从而精制步骤1中获得的反应产物（步骤2）。根据该方法，由于使用微波进行交联缩合反应，与常规的缩合反应不同，由于没有催化剂，反应时间短，无溶剂，经济效率提高。此外，产物的产率和选择性提高，并且缩合反应可以是环境友好的，因为可能不会使用可能严重影响环境的溶剂。

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