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    • 5. 发明授权
    • Method for the production of plane-parallel platelets by using organic separating agents
    • 通过使用有机分离剂生产平面血小板的方法
    • US07157116B2
    • 2007-01-02
    • US10478190
    • 2002-05-21
    • Hilmar Weinert
    • Hilmar Weinert
    • C23C14/00C23C14/22
    • B82Y30/00C01P2004/20C01P2004/62C01P2004/64C01P2006/12C09C1/62C09C1/627C09C1/64C23C14/0005C23C14/024Y10T428/31663
    • A new method is proposed for the production of plane-parallel platelets, comprising the steps a) vapor-deposition, at a pressure below atmospheric pressure, of a separating agent onto a carrier to produce a separating agent layer, b) vapor-deposition, at a pressure below atmospheric pressure, of at least one product layer onto the separating agent layer, c) dissolution of the separating agent layer in a solvent and production of a suspension in which the at least one product layer is present in the form of plane-parallel platelets, in which method the separating agent is selected from the group consisting of anthracene, anthraquinone, acetamidophenol, acetylsalicylic acid, camphoric anhydride, benzimidazole, benzene-1,2,4-tricarboxylic acid, biphenyl-2,2-dicarboxylic acid, bis(4-hydroxyphenyl)-sulfone, dihydroxyanthraquinone, hydantoin, 3-hydroxybenzoic acid, 8-hydroxyquinoline-5-sulfonic acid monohydrate, 4-hydroxycoumarin, 7-hydroxycoumarin, 3-hydroxynaphthalene-2-carboxylic acid, isophthalic acid, 4,4-methylene-bis-3-hydroxynaphthalene-2-carboxylic acid, naphthalene-1,8-dicarboxylic anhydride, phthalimide and its potassium salt, phenol-phthalein, phenothiazine, saccharin and its salts, tetraphenylmethane, triphenylene, triphenylmethanol, and also mixtures of at least two of those substances. Separating agents that have been found to be especially suitable are aromatic compounds having at least one benzene ring. The present invention relates also to the use of the plane-parallel platelets thereby produced and also to the products obtainable using such methods.
    • 提出了一种生产平面平行血小板的新方法,包括以下步骤:a)在低于大气压的压力下将分离剂气相沉积到载体上以产生分离剂层,b)气相沉积, 在低于大气压的压力下,至少一个产品层到分离剂层上,c)将分离剂层溶解在溶剂中并产生其中至少一个产物层以平面形式存在的悬浮液 平行血小板,其中分离剂选自蒽,蒽醌,乙酰氨基苯酚,乙酰水杨酸,樟脑酸酐,苯并咪唑,苯-1,2,4-三羧酸,联苯-2,2-二羧酸 ,双(4-羟基苯基)砜,二羟基蒽醌,乙内酰脲,3-羟基苯甲酸,8-羟基喹啉-5-磺酸一水合物,4-羟基香豆素,7-羟基香豆素,3-羟基萘-2-羧酸是 邻苯二甲酸,4,4'-亚甲基双-3-羟基萘-2-羧酸,萘-1,8-二羧酸酐,邻苯二甲酰亚胺及其钾盐,苯酚酞,吩噻嗪,糖精及其盐,四苯基甲烷,三亚苯基, 三苯基甲醇,以及这些物质中的至少两种的混合物。 已经发现特别合适的分离剂是具有至少一个苯环的芳族化合物。 本发明还涉及由此制备的平面平行血小板的用途,以及使用这些方法可获得的产品。
    • 10. 发明授权
    • Series evaporator
    • 系列蒸发器
    • US5239611A
    • 1993-08-24
    • US830685
    • 1992-02-04
    • Hilmar Weinert
    • Hilmar Weinert
    • C23C14/26C23C14/24
    • C23C14/243Y02T50/67
    • A device for heating a material to an evaporation temperature so that the material can be coated on a substrate is provided which includes a series evaporator for containing the material to be coated. There is also provided a plurality of radiant heaters disposed above the evaporator and the material to be evaporated, the heaters each being essentially flat and disposed parallel and adjacent to the upper surface of the material. Heat shields are also disposed above the radiant heaters and below a substrate to be coated and have an area sufficient to prevent direct radiant heat contact with the substrate to be coated. A plurality of vapor outlet openings are formed between each adjacent heat shield of the series evaporator and face the substrate to be coated. The outlets are in vapor communication with the material being evaporated. Each of the radiant heaters are located beneath an upper heat shield and within the area protected by the heat shields.
    • 提供了一种用于将材料加热至蒸发温度以使材料可以涂覆在基底上的装置,其包括用于容纳待涂覆材料的串联蒸发器。 还设置了多个辐射加热器,其设置在蒸发器上方和待蒸发的材料上,每个加热器基本上是平的并且平行并邻近材料的上表面设置。 隔热罩也设置在辐射加热器之上并在待涂覆的基底下方,并且具有足以防止与待涂覆的基底的直接辐射热接触的面积。 在串联蒸发器的每个相邻的隔热罩之间形成多个蒸气出口,并且面对待涂覆的基板。 出口与被蒸发的材料蒸汽连通。 每个辐射加热器位于上部隔热罩的下方,并在由隔热罩保护的区域内。