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1. 发明授权

US4713389A Fungicidally and bactericidally active acylated saccharin derivatives 失效
标题翻译：杀真菌和杀菌活性酰化糖精衍生物
公开(公告)号：US4713389A
公开(公告)日：1987-12-15
申请号：US774271
申请日：1985-09-10
申请人： Herbert Salzburg , Manfred Hajek , Hermann Hagemann , Engelbert Kuhle , Wolfgang Fuhrer , Gerd Hanssler , Wilhelm Brandes , Paul Reinecke
发明人： Herbert Salzburg , Manfred Hajek , Hermann Hagemann , Engelbert Kuhle , Wolfgang Fuhrer , Gerd Hanssler , Wilhelm Brandes , Paul Reinecke
IPC分类号： A01N47/38 , A61K31/425 , A61K31/428 , A61P31/04 , C07D275/06
CPC分类号： C07D275/06 , A01N47/38
摘要： Fungicidally and bactericidally active novel acylated saccharins of the formula ##STR1## in which X is oxygen or sulphur andR is --CO--R.sup.1 or --SO.sub.2 --OR.sup.2,R.sup.1 is alkyl, halogenalkyl, alkoxy, halogenoalkoxy or alkylthio, or is optionally substituted aryl, aryloxy or arylthio, cycloalkoxy or --NR.sup.3 R.sup.4,R.sup.2 is alkyl or phenyl,R.sup.3 is alkyl, andR.sup.4 is alkyl, phenyl, halogenoalkylthio, alkoxycarbonyl or phenoxycarbonyl, or--NR.sup.3 R.sup.4 is a saccharin radical.
摘要翻译：式中：X为氧或硫，R为-CO-R 1或-SO 2 OR 2的杀真菌杀菌活性新型酰化糖精，R1为烷基，卤代烷基，烷氧基，卤代烷氧基或烷硫基，或为任选取代的芳基芳氧基或芳硫基，环烷氧基或-NR3R4，R2是烷基或苯基，R3是烷基，R4是烷基，苯基，卤代烷硫基，烷氧基羰基或苯氧羰基，或-NR3R4是糖精基。

2. 发明授权

US4683233A Salts of 2-keto-2H, 3H-1,2-benzisothiazole 1,1-dioxide as microbicides 失效
公开(公告)号：US4683233A
公开(公告)日：1987-07-28
申请号：US704439
申请日：1985-02-22
申请人： Herbert Salzburg , Manfred Hajek , Gerd Hanssler , Varl-Heinz Kuck
发明人： Herbert Salzburg , Manfred Hajek , Gerd Hanssler , Varl-Heinz Kuck
IPC分类号： A01N47/44 , A01N20060101 , A01N37/44 , A01N43/16 , A01N43/40 , A01N43/50 , A01N43/54 , A01N43/56 , A01N43/60 , A01N43/653 , A01N43/76 , A01N43/80 , A01N43/84 , A01N43/90 , A01N47/42
CPC分类号： A01N43/56 , A01N37/44 , A01N43/16 , A01N43/40 , A01N43/50 , A01N43/54 , A01N43/60 , A01N43/653 , A01N43/76 , A01N43/80 , A01N43/84 , A01N43/90 , A01N47/44
摘要： A method of combating fungi and bacteria which comprises applying to such fungi, bacteria or a habitat thereof, a fungicidally or bactericidally effective amount of at least one salt of 3-keto-2-, 3H-1,2-benzisothiazole 1,1-dioxide of the formula ##STR1## in which R.sup.1 represents hydrogen, alkyl having 1 to 18 carbon atoms, or alkyl which has 1 to 6 carbon atoms and is optionally monosubstituted to trisubstituted by hydroxyl and/or monosubstituted to trisubstituted by amino, or represents carboxyl-substituted alkyl having 1 to 4 carbon atoms, or phenyl which is optionally monosubstituted to trisubstituted by identical or different substituents from amongst nitro and chlorine, or represents cycloalkyl having 5 or 6 carbon atoms, or represents heterocyclic structures which are optionally saturated or unsaturated, are optionally monosubstituted to tetrasubstituted by alkyl having 1 to 4 carbon atoms or hydroxyl, and have 1 to 3 identical or different heteroatoms, and a total of 5 or 6 ring members,R.sup.2 represents alkyl having 1 to 18 atoms, or alkyl which has 1 to 6 carbon atoms and is optionally monosubstituted to trisubstituted by hydroxyl and/or monosubstituted to trisubstituted by amino, or represents carboxyl-substituted alkyl having 1 to 4 carbon atoms, or phenyl which is optionally monosubstituted to trisubstituted by identical or different substituents from amongst nitro and chlorine, or represent cycloalkyl having 5 or 6 carbon atoms, or represents heterocyclic structures which are optionally saturated or unsaturated, are optionally monosubstituted to tetrasubstituted by alkyl having 1 to 4 carbon atoms or hydroxyl, and have 1 to 3 identical or different heteroatoms, and a total of 5 or 6 ring members, andR.sup.3 represents hydrogen, alkyl, having 1 to 6 carbon atoms, NH.sub.2, ##STR2## benzyl, or hydroxyalkyl having 1 to 3 carbon atoms, with the exception of the mono-, di- and triethanolamine compounds, orR.sup.1 and R.sup.2 together with the nitrogen atom at which they are located, form a 5-membered or 6-membered ring which can optionally contain further heteroatoms, and can optionally be substituted by keto groups or fused-on 5-membered or 6-membered rings and/or alkyl having 1 to 4 carbon atoms, with the exception of the pyridine ring which is optionally mono- or disubstituted by methyl.

3. 发明授权

US4642344A Polyamines 失效
标题翻译：多胺
公开(公告)号：US4642344A
公开(公告)日：1987-02-10
申请号：US690445
申请日：1985-01-11
申请人： Manfred Hajek , Herbert Salzburg , Heinz Ziemann
发明人： Manfred Hajek , Herbert Salzburg , Heinz Ziemann
IPC分类号： C07D251/70
CPC分类号： C07D251/70
摘要： The present invention relates to new polyamines corresponding to the formula ##STR1## in which R.sup.1 represents an alkyl, cycloalkyl or aryl group andR.sup.2 represents hydrogen or an alkyl group.The present invention is also directed to a process for the preparation of these amines by hydrogenating the corresponding trinitriles.
摘要翻译：本发明涉及对应于式“IMAGE”的新的多胺，其中R 1表示烷基，环烷基或芳基，R 2表示氢或烷基。本发明还涉及通过氢化相应的三腈来制备这些胺的方法。

4. 发明授权

US5587511A Process for obtaining adipic acid 失效
标题翻译：获得己二酸的方法
公开(公告)号：US5587511A
公开(公告)日：1996-12-24
申请号：US556572
申请日：1995-11-13
申请人： Herbert Salzburg , Georg Steinhoff , Andreas Gosch , Gerd Hufen
发明人： Herbert Salzburg , Georg Steinhoff , Andreas Gosch , Gerd Hufen
IPC分类号： C07C51/43 , C07C51/47 , C07C51/48 , C07C55/12 , C07C55/14 , C07C51/00
CPC分类号： C07C51/43
摘要： The present invention relates to a process for obtaining adipic acid from the aqueous nitric acid mother liquors that arise during industrial adipic acid production by(i) removing nitric acid from the aqueous mother liquor by evaporation to a concentrate having a residual content of at most about 2.5 wt. % of HNO.sub.3,(ii) mixing the concentrate obtained according to step (i) with water or dilute aqueous nitric acid in a quantity corresponding to a weight ratio of solid to liquid of about 1:2.1 to about 1:1.2,(iii) allowing the water added in step (ii) or the nitric acid added in step (ii) to act upon the concentrate for at least about 10 minutes at about 20.degree. to about 80.degree. C., and(iv) separating adipic acid as crystals that are formed (1) during step (iii) at temperatures of no more than about 35.degree. C. or (2) after step (iii) by cooling the mixture from step (iii) to about 10.degree. to about 35.degree. C.
摘要翻译：本发明涉及一种从工业己二酸生产过程中产生的硝酸母液中获得己二酸的方法，该方法是（i）通过蒸发从含水母液中除去硝酸至具有至多约 2.5重量％％的HNO 3，（ii）将根据步骤（i）获得的浓缩物与水或稀的硝酸水溶液混合，其量相当于固体与液体的重量比为约1：2.1至约1：1.2，（iii）允许在步骤（ii）中加入的水或步骤（ii）中加入的硝酸在约20℃至约80℃下对浓缩物作用至少约10分钟，和（iv）将己二酸分离成晶体在步骤（iii）中在不超过约35℃的温度下形成（1）或（2）在步骤（iii）之后通过将步骤（iii）的混合物冷却至约10℃至约35℃来形成（1）

5. 再颁专利

USRE33748E Process for the preparation of polyurethane plastics using dianhydro-hexite diols 失效
公开(公告)号：USRE33748E
公开(公告)日：1991-11-19
申请号：US733284
申请日：1985-05-10
申请人： Holger Meyborg , Kuno Wagner , James M. Barnes , Herbert Salzburg
发明人： Holger Meyborg , Kuno Wagner , James M. Barnes , Herbert Salzburg
IPC分类号： C08L65/00 , C08G18/00 , C08G18/10 , C08G18/32 , C08G18/65 , C08L7/00 , C08L21/00 , C08L67/00 , C08L77/00
CPC分类号： C08G18/6511 , C08G18/10 , C08G18/3218
摘要： A process for the preparation of homogeneous and cellular polyurethane plastics by the reaction of(a) organic polyisocyanates;(b) compounds containing at least 2 Zerewitinoff-active hydrogen atoms and having molecular weights of from 400 to 10,000;(c) chain extenders, and, optionally, additional(d) short-chained compounds containing at least 2 Zerewitinoff-active hydrogen atoms and having a molar mass of from 32 to 400, as well as, optionally,(e) catalysts, blowing agents and other known additives,is described, which is characterized in that 1,4-3,6-dianhydro-hexites, preferably 1,4-3,6-dianhydro-D-sorbitol and/or 1,4-3,6-dianhydro-D-mannitol, optionally mixed with lower molecular weight compounds, preferably with polyols having a molecular weight of from 62 to 400, particularly preferably butane diol-1,4 are used as the chain extenders. The new chain extenders produce high quality elastomers and foams.

6. 发明授权

US4667041A Process for the preparation of 3-hydrazino-1,2-benz-isothiazole 1,1-dioxides 失效
标题翻译： 3-肼基-1,2-苯并异噻唑1,1-二氧化物的制备方法
公开(公告)号：US4667041A
公开(公告)日：1987-05-19
申请号：US706577
申请日：1985-02-28
申请人： Herbert Salzburg , Manfred Hajek , Gerd Hanssler
发明人： Herbert Salzburg , Manfred Hajek , Gerd Hanssler
IPC分类号： A01N43/80 , C07D275/06
CPC分类号： C07D275/06 , A01N43/80
摘要： A process for the preparation of a 3-hydrazino-1, 2-benzisothiazole 1,1-dioxide of the formula ##STR1## in which R.sup.1 and R.sup.2 each independently is hydrogen, alkyl, halogen, amino, hydroxyl or carboxyl, andR.sup.3 and R.sup.4 each independently is hydrogen, alkyl, cycloalkyl or aryl,comprising reacting a 3-keto-2H,3H-1,2-benzisothiazole 1,1-dioxide of the formula ##STR2## with a hydrazine of the formula ##STR3## in a molar ratio of 1:1 to 1:50, in an inert solvent, at a temperature between 75.degree. C. and 200.degree. C. and for a reaction time of 15 to 40 hours. The products, some of which are known, are fungicidally active and can also be used as intermediates.
摘要翻译：制备式“IMAGE”的3-肼基-1,2-苯并异噻唑1,1-二氧化物的方法，其中R 1和R 2各自独立地为氢，烷基，卤素，氨基，羟基或羧基，以及R 3和 R 4各自独立地是氢，烷基，环烷基或芳基，包括使式IMAGE的3-酮基-2H，3H-1,2-苯并异噻唑1,1-二氧化物与式IMAMA的肼反应摩尔比为1:1至1:50，在惰性溶剂中，在75℃至200℃之间，反应时间为15至40小时。其中一些已知的产品是杀真菌活性的并且也可以用作中间体。

7. 发明授权

US4476253A Process for the preparation of polyurethane elastomers using diols of the anhydro-tetritol series 失效
标题翻译：使用脱水四氢呋喃系列的二醇制备聚氨酯弹性体的方法
公开(公告)号：US4476253A
公开(公告)日：1984-10-09
申请号：US570045
申请日：1984-01-11
申请人： Herbert Salzburg , Holger Meyborg , Wilhelm Goyert , James M. Barnes
发明人： Herbert Salzburg , Holger Meyborg , Wilhelm Goyert , James M. Barnes
IPC分类号： C08G18/10 , C08G18/32 , C08G18/14
CPC分类号： C08G18/3218 , C08G18/10
摘要： Polyurethane elastomers are made by reacting organic polyisocyanates with compounds having at least two groups containing isocyanate-reactive hydrogen atoms and a molecular weight of from 400 to 10,000 and a 1,4-monoanhydro-tetritol in accordance with techniques known to those in the art. Known chain-lengthening agents, auxiliaries and additives may be included in the reaction mixture. The reaction mixtures employed in the process of the present invention have a longer pot life than prior art reaction mixtures. The elastomers produced by this process are shrink stable.
摘要翻译：根据本领域已知的技术，聚氨酯弹性体是通过有机多异氰酸酯与具有至少两个含异氰酸酯反应性氢原子和分子量为400至10,000的化合物和1,4-单羟基 - 氢化四醇反应制备的。已知的增链剂，助剂和添加剂可以包括在反应混合物中。在本发明方法中使用的反应混合物具有比现有技术的反应混合物更长的适用期。由该方法生产的弹性体收缩稳定。

8. 发明授权

US4408061A Process for the preparation of 1,4-3,6-dianhydro-hexitols 失效
标题翻译：制备1,4-3,6-二氢 - 己醇的方法
公开(公告)号：US4408061A
公开(公告)日：1983-10-04
申请号：US357353
申请日：1982-03-11
申请人： Herbert Salzburg , Holger Meyborg , Heinz Ziemann
发明人： Herbert Salzburg , Holger Meyborg , Heinz Ziemann
IPC分类号： C07D493/04
CPC分类号： C07D493/04
摘要： A process for the preparation of 1,4-3,6-dianhydro-hexitols from hexitols by elimination of water is described, characterized in that gaseous hydrogen halide is used as the acid dehydrating agent optionally with carboxylic acids, carboxylic acid halides and/or carboxylic acid anhydrides in quantities of up to 600 mol percent, based on the hexitols, as cocatalysts. The reaction is carried out in the absence of water and organic solvents, preferably using gaseous hydrogen chloride, temperatures of up to 300.degree. C. and pressures of up to 250 bar. Very high yields are obtained after working up of the product by distillation or extraction.
摘要翻译：描述了通过除去水从己醇制备1,4-3,6-二脱氢 - 己醇的方法，其特征在于，使用气态卤化氢作为酸脱水剂，任选地与羧酸，羧酸卤化物和/或羧酸酐，其量为至多600摩尔％，基于己二醇，作为助催化剂。反应在没有水和有机溶剂的情况下进行，优选使用气态氯化氢，温度高达300℃，压力高达250巴。通过蒸馏或萃取处理产物后可获得非常高的产率。

9. 发明授权

US5723098A Process for the recovery of catalysts in adipic acid production 失效
标题翻译：在己二酸生产中回收催化剂的方法
公开(公告)号：US5723098A
公开(公告)日：1998-03-03
申请号：US706473
申请日：1996-09-04
申请人： Herbert Salzburg , Georg Steinhoff , Heiko Hoffmann , Helmut Kaponig
发明人： Herbert Salzburg , Georg Steinhoff , Heiko Hoffmann , Helmut Kaponig
IPC分类号： B01J23/22 , B01J23/72 , B01J35/12 , B01J38/74 , C07B61/00 , C07C51/27 , C07C51/47 , C07C55/14 , C07C55/00 , C01G49/00 , C02F1/42
CPC分类号： C07C51/47
摘要： The invention relates to a process for the selective recovery of catalysts used in the production of adipic acid by (a) separating adipic acid from the reaction solution, (b) exposing the resultant reaction solution to a sulfonated ion exchanger, thereby binding iron, copper, and vanadium ions to said sulfonated ion exchanger, (c) separating the ion-exchanger from the reaction solution, (d) washing the separated ion exchanger with nitric acid to obtain an acid eluate, and (e) exposing the acid eluate to an ion exchanger modified with aminophosphonic acid groups, thereby removing the iron ions from the acid eluate.
摘要翻译：本发明涉及通过（a）从反应溶液中分离己二酸来选择性回收用于生产己二酸的催化剂的方法，（b）将所得反应溶液暴露于磺化离子交换剂中，由此将铁，铜和钒离子与所述磺化离子交换剂反应，（c）将离子交换剂与反应溶液分离，（d）用硝酸洗涤分离的离子交换剂以得到酸洗脱液，和（e）将酸洗脱液暴露于离子交换剂用氨基膦酸基团修饰，从而从酸洗脱液中除去铁离子。

10. 发明授权

US4666930A 3-hydrazono-benzisothiazole 1,1-dioxide fungicides 失效
标题翻译： 3-肼基 - 苯并异噻唑1,1-二氧化物杀真菌剂
公开(公告)号：US4666930A
公开(公告)日：1987-05-19
申请号：US707361
申请日：1985-03-01
申请人： Herbert Salzburg , Manfred Hajek , Gerd Hanssler
发明人： Herbert Salzburg , Manfred Hajek , Gerd Hanssler
IPC分类号： A01N43/80 , A01N47/24 , A01N47/34 , C07D275/06 , C07D417/12
CPC分类号： C07D275/06 , A01N43/80 , A01N47/24 , A01N47/34 , C07D417/12
摘要： Compounds of the formula ##STR1## in which R.sup.1 is alkyl, cycloalkyl, aryl or hydrogen,R.sup.2 is --CO--R.sup.3,R.sup.3 is alkyl, alkenyl or cycloalkyl, or is phenyl which is optionally substituted, or is alkoxy or benzyl, or is phenoxy which is optionally substituted, or is phenoxymethyl, alkylamino, cycloalkylamino or phenylamino, orR.sup.1 and R.sup.2 together are a ##STR2## group, R.sup.4 and R.sup.5 each independently is hydrogen, alkyl, cycloalkenyl or phenylalkenyl, or is phenyl which is optionally substituted by alkyl, halogen and/or alkoxy, or is furyl, orR.sup.4 and R.sup.5 together are alkylene having 4 to 6 carbon atoms,are fungicidally active. Those compounds wherein R.sup.3 is alkylamino, cycloalkylamino or phenylamino, with the exception of the compound in which R.sup.1 is hydrogen and R.sup.6 is phenylamino, are new.
摘要翻译：式中，R 1为烷基，环烷基，芳基或氢的化合物，R 2为-CO-R 3，R 3为烷基，烯基或环烷基，或为任选取代的苯基，或为烷氧基或苄基，或为任选被取代的苯氧基，或者是苯氧基甲基，烷基氨基，环烷基氨基或苯基氨基，或者R 1和R 2一起是一个基团，R 4和R 5各自独立地是氢，烷基，环烯基或苯基烯基，或者是任选地被烷基，卤素和/或烷氧基，或是呋喃基，或R4和R5一起是具有4-6个碳原子的亚烷基，是杀真菌活性的。其中R 3是烷基氨基，环烷基氨基或苯基氨基的那些化合物，除了其中R 1是氢和R 6是苯基氨基的化合物外，是新的。

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