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1. 发明授权

US5233054A Process for the preparation of halophthalic anhydrides 失效
标题翻译：制备卤代邻苯二甲酸酐的方法
公开(公告)号：US5233054A
公开(公告)日：1993-08-03
申请号：US721004
申请日：1991-06-26
申请人： David Y. Tang , Mary K. Cocoman , Harry E. Buckholtz
发明人： David Y. Tang , Mary K. Cocoman , Harry E. Buckholtz
IPC分类号： C07C51/377 , C07C51/567 , C07C253/30
CPC分类号： C07C253/30 , C07C51/377 , C07C51/567
摘要： Halophthalic anhydrides are prepared by the liquid phase reaction of a brominating agent with halogen substituted hexa- or tetra-hydrophthalic anhydrides.
摘要翻译：卤代邻苯二甲酸酐通过溴化剂与卤素取代的六 - 或四 - 邻苯二甲酸酐的液相反应来制备。

2. 发明授权

US4935213A Zero discharge process for preparing potassium tripolyphosphate 失效
标题翻译：零排放工艺制备三聚磷酸三钾
公开(公告)号：US4935213A
公开(公告)日：1990-06-19
申请号：US387210
申请日：1989-07-31
申请人： Harry E. Buckholtz
发明人： Harry E. Buckholtz
IPC分类号： C01B25/41
CPC分类号： C01B25/41
摘要： Disclosed is a method of making potassium tripolyphosphate by loading an ion exchange resin with either potassium or hydrogen ions and passing an aqueous solution of sodium tripolyphosphate through the resin so that the sodium ions of the sodium tripolyphosphate are exchanged with the ions loaded onto the resin, forming either potassium tripolyphosphate or tripolyphosphoric acid, respectively. The tripolyphosphoric acid is reacted with potassium hydroxide to form potassium tripolyphosphate. When the ion exchange resin becomes exhausted it is regenerated using a potassium-containing ionic solution, forming a sodium ion containing stream. The sodium ion containing stream is reacted with a phosphoric acid to form a stream of sodium phosphates.
摘要翻译：公开了通过将离子交换树脂与钾离子或氢离子负载并使三聚磷酸钠水溶液通过树脂使三聚磷酸钠的钠离子与负载在树脂上的离子交换而制备三聚磷酸钾的方法，分别形成三聚磷酸钾或三聚磷酸。使三聚磷酸与氢氧化钾反应形成三聚磷酸钾。当离子交换树脂耗尽时，其使用含钾离子溶液再生，形成含钠离子的流。含钠离子的物流与磷酸反应形成磷酸钠流。

3. 发明授权

US4997638A Production of hexametaphosphates from other phosphates 失效
标题翻译：从其他磷酸盐生产六偏磷酸盐
公开(公告)号：US4997638A
公开(公告)日：1991-03-05
申请号：US535623
申请日：1990-06-11
申请人： Harry E. Buckholtz
发明人： Harry E. Buckholtz
IPC分类号： C01B25/41
CPC分类号： C01B25/41
摘要： Disclosed is a method of making hexametaphosphates by reacting sodium tripolyphosphate, tetrasodium pyrophosphate, or trisodium phosphate with phosphoric acid, forming a molten glass of said mixture, and chilling said molten glass to form a solid.
摘要翻译：公开了通过使三聚磷酸钠，焦磷酸四钠或磷酸三钠与磷酸反应形成六偏磷酸盐的方法，形成所述混合物的熔融玻璃，并冷却所述熔融玻璃以形成固体。

4. 发明授权

US5206391A Process for the preparation of halophthalic anhydrides 失效
标题翻译：制备卤代邻苯二甲酸酐的方法
公开(公告)号：US5206391A
公开(公告)日：1993-04-27
申请号：US751841
申请日：1991-08-29
申请人： Karl W. Seper , Edward J. Colman , David Y. Tang , Mary K. Cocoman , Harry E. Buckholtz
发明人： Karl W. Seper , Edward J. Colman , David Y. Tang , Mary K. Cocoman , Harry E. Buckholtz
IPC分类号： C07C51/377 , C07C51/567 , C07C253/30
CPC分类号： C07C253/30 , C07C51/377 , C07C51/567
摘要： A process for the preparation of a halophthalic anhydride, such as chlorophthalic anhydride, comprising the liquid phase reaction of bromine with a halogen substituted hexa- or tetra-hydrophthalic anhydride to produce halophthalic anhydride and gaseous HBr, and reacting the gaseous HBr with chlorine to regenerate bromine.
摘要翻译：制备卤代邻苯二甲酸酐如氯邻苯二甲酸酐的方法，包括溴与卤素取代的六 - 或四邻苯二甲酸酐的液相反应产生卤代邻苯二甲酸酐和气态HBr，并使气态HBr与氯反应再生溴。

5. 发明授权

US4967838A Oil well and method using completion fluid 失效
标题翻译：油井和使用完井液的方法
公开(公告)号：US4967838A
公开(公告)日：1990-11-06
申请号：US407007
申请日：1989-09-14
申请人： Harry E. Buckholtz
发明人： Harry E. Buckholtz
IPC分类号： C09K8/04 , C09K8/84
CPC分类号： C09K8/845 , C09K8/04 , Y10S166/902
摘要： Disclosed is a method of preventing fluids in the ground from rising around an oil well pipe by filling the space around the pipe with an oil well completion fluid comprising water, about 50 to about 65% by weight, based on total fluid weight, of dipotassium phosphate, and at least about 10 ppm hexavalent chromium. The fluid can be prepared by neutralizing wet process phosphoric acid with potassium hydroxide to a pH of less than 12 and filtering off any solids. Also disclosed is an oil well employing the completion fluid.
摘要翻译：公开了一种通过用包含水的油井完井流体填充管道周围的空间来防止地面中的流体在油井管周围上升的方法，所述油井完井流体基于总流体重量为约50重量％至约65重量％磷酸盐和至少约10ppm的六价铬。流体可以通过用氢氧化钾将湿法磷酸中和至小于12的pH并过滤掉任何固体来制备。还公开了采用完井液的油井。

6. 发明授权

US5368832A Zero discharge process for manufacturing of phosphorous acid and hypophosphorous acid 失效
标题翻译：用于制造亚磷酸和次磷酸的零排放工艺
公开(公告)号：US5368832A
公开(公告)日：1994-11-29
申请号：US711841
申请日：1991-06-07
申请人： Harry E. Buckholtz , Mohan S. Saran , Frederick C. Leitert , David A. Flautt
发明人： Harry E. Buckholtz , Mohan S. Saran , Frederick C. Leitert , David A. Flautt
IPC分类号： C01B25/163 , C01B25/165
CPC分类号： C01B25/165 , C01B25/163
摘要： Disclosed is a method of making phosphorous acid or hypophosphorous acid by reacting hydrogen chloride with a sodium phosphite or a sodium hypophosphite, respectively, in the presence of water to precipitate sodium chloride crystals and form the acid. The acid is separated from the sodium chloride crystals and can be passed through an anion exchange column that is preferably loaded with phosphite or hypophosphite ions, respectively, to remove residual chloride ions.
摘要翻译：公开了在水存在下分别使氯化氢与亚磷酸钠或次磷酸钠反应制备亚磷酸或次磷酸以沉淀氯化钠晶体并形成酸的方法。酸与氯化钠晶体分离，可分别通过负载有亚磷酸盐或次磷酸根离子的阴离子交换柱，以除去残留的氯离子。

7. 发明授权

US5019157A Method of making eutectic mixture of copper and tricopper phosphide 失效
标题翻译：铜和三磷酸铁的共晶混合物的制备方法
公开(公告)号：US5019157A
公开(公告)日：1991-05-28
申请号：US383502
申请日：1989-07-24
申请人： Harry E. Buckholtz , George T. Miller
发明人： Harry E. Buckholtz , George T. Miller
IPC分类号： C22C1/00
CPC分类号： C22C1/00
摘要： Disclosed is a method of making a eutectic mixture of copper and tricopper phosphide by reacting elemental copper with phosphine. The elemental copper is heated to a temperature above about 714.degree. C. and the liquid eutectic mixture runs off of the cooper as it is formed, exposing more copper for reaction. The liquid eutectic mixture can be used as a source of copper and phosphorus in making metal alloys.
摘要翻译：公开了通过使元素铜与磷化氢反应制备铜和三磷酸铁的共晶混合物的方法。将元素铜加热至高于约714℃的温度，并且液体共晶混合物在其形成时从铜离开，暴露更多的铜作为反应。液体共晶混合物可用作制造金属合金中铜和磷的来源。

8. 发明授权

US4091031A Process for the manufacture of substituted thianthrene based products 失效
标题翻译：制备取代噻蒽类产品的方法
公开(公告)号：US4091031A
公开(公告)日：1978-05-23
申请号：US737320
申请日：1976-11-01
申请人： Harry E. Buckholtz , Arun C. Bose
发明人： Harry E. Buckholtz , Arun C. Bose
IPC分类号： C07D339/08 , C09B57/00
CPC分类号： C07D339/08
摘要： Thianthrene compounds are prepared by adding sulfur monochloride to an excess of a benzene compound in the presence of aluminum chloride, and reacting to form a thianthrene compound as an insoluble aluminum chloride complex; slurrying the complex in an inert organic liquid; treating the slurry with a Lewis base, such as ammonia to free the thianthrene compound from the complex.
摘要翻译：通过在氯化铝的存在下，向过量的苯化合物中加入一氯化硫，并使其形成作为不溶性氯化铝络合物的噻喃化合物而制备噻蒽类化合物; 将络合物在惰性有机液体中制浆; 用诸如氨的路易斯碱处理浆料以从络合物中释放噻喃化合物。

9. 发明授权

US3997560A Process for the manufacture of thianthrene 失效
标题翻译：生产噻蒽的工艺
公开(公告)号：US3997560A
公开(公告)日：1976-12-14
申请号：US521108
申请日：1974-11-05
申请人： Harry E. Buckholtz , Arun C. Bose
发明人： Harry E. Buckholtz , Arun C. Bose
IPC分类号： C07D339/08 , C09B57/00
CPC分类号： C07D339/08
摘要： Thianthrene is prepared by adding sulfur monochloride to an excess of benzene in the presence of aluminum chloride, and reacting at a temperature of 60.degree. to 80.degree. C to form thianthrene as an insoluble thianthrene-aluminum chloride complex; separating the complex by filtration, slurrying the complex in an inert organic liquid; treating the slurry with a Lewis base, such as ammonia to free the thianthrene from the complex and recovering a relatively high purity thianthrene product.
摘要翻译：在氯化铝存在下，通过在过量的苯中加入一氯化硫制备噻蒽，并在60〜80℃的温度下反应形成不溶性噻蒽 - 氯化铝络合物的噻蒽; 通过过滤分离复合物，将络合物在惰性有机液体中制浆; 用诸如氨的路易斯碱处理浆料以从络合物中释放噻蒽并回收较高纯度的噻蒽产品。

10. 发明授权

US06685904B1 Process for making phosphorus halides and oxyhalides 失效
标题翻译：制备卤化磷和卤氧化物的方法
公开(公告)号：US06685904B1
公开(公告)日：2004-02-03
申请号：US09061754
申请日：1998-04-16
申请人： Harry E. Buckholtz , Mohamed W. Hisham
发明人： Harry E. Buckholtz , Mohamed W. Hisham
IPC分类号： C01B2510
CPC分类号： C01B25/10
摘要： Disclosed is a process for producing phosphorous trichloride, phosphorous pentachloride, or phosphorous tribromide by reacting phosphine gas with chlorine gas or bromine gas, in a mixture with hydrogen gas. The phosphine is dried and the reaction is performed at a temperature up to about 250° C. The phosphorous trichloride or phosphorous tribromide product can be reacted with oxygen to form phosphorous oxychloride or phosphorous oxybromide, respectively.
摘要翻译：公开了一种通过使磷氢气与氯气或溴气在氢气的混合物中反应生成三氯化磷，五氯化磷或三溴化磷的方法。将磷化氢干燥，反应在高达约250℃的温度下进行。三氯化磷或三溴化磷产物可与氧反应，分别形成三氯氧化磷或三溴氧化磷。

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