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1. 发明申请

US20080131353A1 Methods For Purification Of Trimetallic Nitride Endohedral Metallofullerenes And Related Fullerene Derivatives 审中-公开
标题翻译：金属氮化物内含金属富勒烯和相关富勒烯衍生物的纯化方法
公开(公告)号：US20080131353A1
公开(公告)日：2008-06-05
申请号：US11570700
申请日：2005-06-23
申请人： Harry W. Gibson , Harry C. Dorn , Zhongxin Ge , Ting Cai
发明人： Harry W. Gibson , Harry C. Dorn , Zhongxin Ge , Ting Cai
IPC分类号： C01B31/00
CPC分类号： C01B21/0627 , B82Y30/00 , B82Y40/00 , C01B32/152 , C01B32/17 , C01P2002/72
摘要： Methods for separating and purifying carbon nanomaterials such as trimetallic nitride endohedral metallofullerenes are described. In certain embodiments, carbon nanomaterials are contacted with a carbon nanomaterial reactive agent. The reactive agent binds empty cage fullerenes, nanotubes, and endohedral metallofullerenes without appreciably binding trimetallic nitride endohedral metallofullerenes. According to some embodiments, purified forms of trimetallic nitride endohedral metallofullerenes may be prepared.
摘要翻译：描述了分离和纯化碳纳米材料如三金属氮化物内嵌金属富勒烯的方法。在某些实施方案中，碳纳米材料与碳纳米材料反应剂接触。活性剂结合空笼富勒烯，纳米管和内嵌金属富勒烯，而不会明显地结合三金属氮化物内嵌金属富勒烯。根据一些实施方案，可以制备纯化形式的三金属氮化物内嵌金属富勒烯。

2. 发明授权

US06303760B1 Endohedral metallofullerenes and method for making the same 有权
标题翻译：内在金属富勒烯及其制造方法
公开(公告)号：US06303760B1
公开(公告)日：2001-10-16
申请号：US09458289
申请日：1999-12-10
申请人： Harry C. Dorn , Steven A. Stevenson
发明人： Harry C. Dorn , Steven A. Stevenson
IPC分类号： C07F500
CPC分类号： C01B21/0627 , B01J27/22 , B01J27/24 , B82Y10/00 , B82Y30/00 , B82Y40/00 , C01B32/15 , C01B32/152 , C01P2002/72 , C01P2002/77 , C01P2002/84 , C01P2002/85 , C01P2002/86 , C01P2002/89 , C07F5/00 , H01L51/0046 , Y10S977/734 , Y10S977/736 , Y10S977/777 , Y10S977/835 , Y10S977/844 , Y10S977/846
摘要： A family of trimetallic nitride endohedral metallofullerenes and their preparation are described. The trimetallic nitride endohedral metallofullerenes have the general formula A3-nXn@Cm where n ranges from 0 to 3, A and X may be trivalent metals and may be either rare earth metal or group IIIB metals, and m is between about 60 and about 200. Further, the A3-nXn@C68, A3-nXn@C78, A3-nXn@C80 families of endohedral fullerenes are described. The trimetallic nitride endohedral metallofullerenes are produced by charging a reactor with a cored graphite rod that has been filled with a metal oxide graphite mixture. The metal oxides correspond to the metals for A and X. The graphite rod is arc discharged in a helium and nitrogen atmosphere to produce the desired trimetallic nitride endohedral metallofullerenes.
摘要翻译：描述了一系列三金属氮化物内嵌金属富勒烯及其制备方法。三金属氮化物内嵌金属富勒烯具有通式A3-nXn @ Cm，其中n的范围为0至3，A和X可以是三价金属，并且可以是稀土金属或IIIB族金属，m在约60和约200之间此外，描述了A3-nXn @ C68，A3-nXn @ C78，A3-nXn @ C80族内含式富勒烯。通过将填充有金属氧化物石墨混合物的芯状石墨棒装入反应器来制备三金属氮化物内嵌金属富勒烯。金属氧化物对应于A和X的金属。石墨棒在氦和氮气氛中电弧放电以产生所需的三金属氮化物内嵌金属富勒烯。

3. 发明申请

US20090250661A1 Trimetallic Nitride Clusters Entrapped Within CnN Heteroatom Cages 审中-公开
标题翻译：夹杂在CnN杂原子笼中的三金属氮化物簇
公开(公告)号：US20090250661A1
公开(公告)日：2009-10-08
申请号：US12354086
申请日：2009-01-15
申请人： Steven A. Stevenson , Harry C. Dorn , Tianming Zuo
发明人： Steven A. Stevenson , Harry C. Dorn , Tianming Zuo
IPC分类号： C09K3/00
CPC分类号： B82Y40/00 , B82Y30/00 , C01B21/0627 , C01B32/15 , C01B32/152 , C01P2002/89 , C07F5/003
摘要： The present invention is directed to a family of trimetallic nitride endohedral metalloheterofullerenes having the formula Ax X3-x N@Cn N, (x=0, 1, 2 or 3) (n=number of carbon atoms in the cage, typically between 59 and 199), wherein A and X are metal atoms encased within the cage, C is carbon and N is nitrogen. A and X are preferably selected from rare earth elements or group IIIB elements. A or X metal atoms are scandium, yttrium, lanthanum, gadolinium, lutetium, holmium, erbium, thulium, dysprosium, neodymium, cerium, praseodymium and ytterbium. Representative embodiments include Sc3N@C79N, Y3N@C79N, La3N@C79N, Tb3N@C79N, Ho3N@C79N, LaSc2N@C79N, PrSc2N@C79N, GdSc2N@C79N, La2ScN@C79N, and Gd2ScN@C79N. The present invention is also directed to a method of making the inventive endohedral metalloheterofullerenes having the formula AxX3-xN@CnN. These methods involve use of oxidizing gases (e.g. O2 and NOx) coupled with combustion as a means for making trimetallic nitride clusters encapsulated in heteroatom CnN cages made of both carbon and nitrogen.
摘要翻译：本发明涉及一种具有式ⅩⅩX3-x N @ Cn N（x = 0,1,2或3）的三金属氮化物内嵌型金属杂多富勒烯（n =笼中的碳原子数，通常为59 和199），其中A和X是包封在笼中的金属原子，C是碳，N是氮。 A和X优选选自稀土元素或IIIB族元素。 A或X金属原子是钪，钇，镧，钆，镥，钬，铒，ium，镝，钕，铈，镨和镱。代表性的实施方案包括Sc3N @ C79N，Y3N @ C79N，La3N @ C79N，Tb3N @ C79N，Ho3N @ C79N，LaSc2N @ C79N，PrSc2N @ C79N，GdSc2N @ C79N，La2ScN @ C79N和Gd2ScN @ C79N。本发明还涉及制备具有式AxX3-xN @ CnN的本发明的内嵌金属热富勒烯的方法。这些方法包括使用与燃烧耦合的氧化气体（例如O 2和NO x）作为用于制造包封在由碳和氮两者制成的杂原子CnN笼中的三金属氮化物团簇的手段。

4. 发明授权

US07358343B2 Endohedral metallofullerene derivatives 有权
标题翻译：内含金属富勒烯衍生物
公开(公告)号：US07358343B2
公开(公告)日：2008-04-15
申请号：US10244747
申请日：2002-09-17
申请人： Harry C. Dorn , Erick B. Iezzi , James Duchamp
发明人： Harry C. Dorn , Erick B. Iezzi , James Duchamp
IPC分类号： C07F5/00
CPC分类号： C07F5/003
摘要： Trimetallic nitride endohedral metallofullerene derivatives and their preparation are described. The trimetallic nitride endohedral metallofullerene derivatives have the general formula A3-nXn@Cm(R) where n ranges from 0 to 3, A and X may be trivalent metals and may be either rare earth metal or group IIIB metals, m is between about 60 and about 200, and R is preferably an organic group. Derivatives where the R group forms cyclized derivatives with the fullerene cage are also described.
摘要翻译：描述了三金属氮化物内嵌金属富勒烯衍生物及其制备方法。三金属氮化物内嵌金属富勒烯衍生物具有通式3其中n的范围为0至3 A和X可以是三价金属，并且可以是稀土金属或IIIB族金属，m在约60和约200之间，R优选是有机基团。还描述了R基团与富勒烯笼形成环化衍生物的衍生物。

5. 发明申请

US20090240042A1 ENDOHEDRAL METALLOFULLERENE DERIVATIVES 审中-公开
公开(公告)号：US20090240042A1
公开(公告)日：2009-09-24
申请号：US11469563
申请日：2006-09-01
申请人： Harry C. Dorn , Erick B. Iezzi , James Duchamp
发明人： Harry C. Dorn , Erick B. Iezzi , James Duchamp
IPC分类号： C07F5/00
CPC分类号： C07F5/003
摘要： Trimetallic nitride endohedral metallofullerene derivatives and their preparation are described. The trimetallic nitride endohedral metallofullerene derivatives have the general formula A3-nXn@Cm(R) where n ranges from 0 to 3, A and X may be trivalent metals and may be either rare earth metal or group IIIB metals, m is between about 60 and about 200, and R is preferably an organic group. Derivatives where the R group forms cyclized derivatives with the fullerene cage are also described.
摘要翻译：描述了三金属氮化物内嵌金属富勒烯衍生物及其制备方法。三金属氮化物内嵌金属富勒烯衍生物具有通式A3-nXn @ Cm（R），其中n的范围为0至3，A和X可以是三价金属，并且可以是稀土金属或IIIB族金属，m在约60 约200，R优选为有机基团。还描述了R基团与富勒烯笼形成环化衍生物的衍生物。

6. 发明申请

US20080279745A1 Endohedral Metalloheterofullerenes 审中-公开
标题翻译：内含金属杂环
公开(公告)号：US20080279745A1
公开(公告)日：2008-11-13
申请号：US12116910
申请日：2008-05-07
申请人： Harry C. Dorn , Tianming Zuo
发明人： Harry C. Dorn , Tianming Zuo
IPC分类号： C01F17/00 , C01B31/00
CPC分类号： B82Y40/00 , B82Y30/00 , C01B32/15 , C01B32/152
摘要： The present invention is directed to a family of endohedral metalloheterofullerenes representative generally as AX@C79N where A and X metal atoms. A and X may be lanthanide metals or rare earth metals. In some embodiments, A and X may be Yttrium, Scandium, Terbium, Lanthanum, Gadolinium, Holmium, Erbium, Thulium, or Ytterbium. A and X may be the same type of metal atom or they may be different. The endohedral metalloheterofullerenes are neutral compounds that can be readily isolated using standard chromatographic techniques. The endohedral metalloheterofullerenes exhibit parmagnetic properties.
摘要翻译：本发明涉及通常以AX和C N N N代表A和X金属原子的内在金属多不饱和聚醚系列。 A和X可以是镧系金属或稀土金属。在一些实施方案中，A和X可以是钇，钪，铽，镧，钆，钬，铒，ium或镱。 A和X可以是相同类型的金属原子，或者它们可以是不同的。内嵌金属杂多富勒烯是中性化合物，可以使用标准色谱技术容易地分离。内嵌金属多毛菌具有顺磁性。

7. 发明授权

US08119092B2 Pegylation and hydroxylation of trimetallic nitride endohedral metallofullerenes 有权
标题翻译：三羟甲基氮化物内嵌金属富勒烯的聚乙二醇化和羟基化
公开(公告)号：US08119092B2
公开(公告)日：2012-02-21
申请号：US10594432
申请日：2005-03-25
申请人： Zhongxin Ge , Harry C. Dorn , J. Paige Phillips
发明人： Zhongxin Ge , Harry C. Dorn , J. Paige Phillips
IPC分类号： C01B31/02
CPC分类号： B82Y30/00 , C07F5/00 , Y10S977/736 , Y10S977/737 , Y10S977/738
摘要： A pegylated and hydroxlated trimetallic nitride endohedral metallofullerene is provided comprising a plurality of hydroxyl groups and one or more polyethylene glycol (PEG) moieties covalently bonded to a fullerene encapsulating a trimetallic nitride. Methods of pegylation and hydroxylation of trimetallic nitride endohedral metallofullerene and methods of using pegylated and hydroxlated trimetallic nitride endohedral metallofullerene are described.
摘要翻译：提供聚乙二醇化和羟基化的三金属氮化物内嵌金属富勒烯，其包含多个羟基和一个或多个共价键合到包封三金属氮化物的富勒烯的聚乙二醇（PEG）部分。描述了三金属氮化物内嵌金属富勒烯的聚乙二醇化和羟基化的方法以及使用聚乙二醇化和羟基化的三金属氮化物内嵌金属富勒烯的方法。

8. 发明申请

US20090012276A1 Polyhydroxy Hydrogensulfated Trimetallic Nitride Endohedral Metallofullerenes 审中-公开
标题翻译：多羟基硫酸氢化三氟化氮内置金属富勒烯
公开(公告)号：US20090012276A1
公开(公告)日：2009-01-08
申请号：US10594429
申请日：2005-03-25
申请人： Zhongxin Ge , Harry C. Dorn
发明人： Zhongxin Ge , Harry C. Dorn
IPC分类号： C07F3/00
CPC分类号： B82Y30/00 , C07F5/00
摘要： Polyhydroxy hydrogensulfated trimetallic nitride endohedral metallofullerenes, can be utilized in a number of applications, for example, as proton conductors in electrochemical devices. The presence of encapsulated metal atoms, preferably trivalent metals including lanthanides, rare earths or HIB group metals, polyhydroxy hydrogensulfated trimetallic nitride endohedral metallofullerenes with properties not found in empty-cage polyhydroxy hydrogensulated fullerenes.
摘要翻译：多羟基硫酸化的多金属氮化物内嵌金属富勒烯可用于许多应用中，例如作为电化学装置中的质子导体。封装的金属原子，优选包括镧系元素，稀土或HIB族金属的三价金属的存在，具有在空笼多聚氢化富勒烯中没有发现的性质的多羟基硫酸氢化的三金属氮化物内嵌金属富勒烯。

9. 发明申请

US20080166285A1 Pegylation and Hydroxylation of Trimetallic Nitride Endohedral Metallofullerenes 有权
标题翻译：三金属氮化物内聚金属富勒烯的聚乙二醇化和羟基化
公开(公告)号：US20080166285A1
公开(公告)日：2008-07-10
申请号：US10594432
申请日：2005-03-25
申请人： Zhongxin Ge , Harry C. Dorn , J. Paige Phillips
发明人： Zhongxin Ge , Harry C. Dorn , J. Paige Phillips
IPC分类号： C01F17/00
CPC分类号： B82Y30/00 , C07F5/00 , Y10S977/736 , Y10S977/737 , Y10S977/738
摘要： A pegylated and hydroxiated trimetallic nitride endohedral metallofullerene is provided comprising a plurality of hydroxyl groups and one or more polyethylene glycol (PEG) moieties covalently bonded to a fullerene encapsulating a trimetallic nitride. Methods of pegylation and hydroxylation of trimetallic nitride endohedral metallofullerene and methods of using pegylated and hydroxlated trimetallic nitride endohedral metallofullerene are described.
摘要翻译：提供聚乙二醇化和羟基化的三金属氮化物内嵌金属富勒烯，其包含多个羟基和一个或多个共价键合到包封三金属氮化物的富勒烯的聚乙二醇（PEG）部分。描述了三金属氮化物内嵌金属富勒烯的聚乙二醇化和羟基化的方法以及使用聚乙二醇化和羟基化的三金属氮化物内嵌金属富勒烯的方法。

10. 发明授权

US06471942B1 Imaging and treatment method for body 失效
标题翻译：身体的成像和治疗方法
公开(公告)号：US06471942B1
公开(公告)日：2002-10-29
申请号：US09839797
申请日：2001-04-20
申请人： Michael B. Miller , Kent A. Murphy , Harry C. Dorn , Steven A. Stevenson , Janice P. Stevenson , Shufang Luo
发明人： Michael B. Miller , Kent A. Murphy , Harry C. Dorn , Steven A. Stevenson , Janice P. Stevenson , Shufang Luo
IPC分类号： A61K4900
CPC分类号： B82Y5/00 , A61K49/189 , Y10S977/927
摘要： A method for imagining and treating a body employing at least one trimetallic nitride template endohedral metallofullerene compound is disclosed. The compound has at least one diagnostic and at least one treatment atom encapsulated within a fullerene cage. The two atoms are different from each other. The compound is administered into a body, traced, and allowed to react at a targeted area of the body.
摘要翻译：公开了一种使用至少一种三金属氮化物模板内嵌金属富勒烯化合物来想象和处理身体的方法。该化合物具有包封在富勒烯笼内的至少一种诊断和至少一种治疗原子。两个原子彼此不同。将化合物施用于身体，追踪并允许在身体的目标区域发生反应。

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