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1. 发明授权

US5756752A Process for preparing substituted oxadiazolones 失效
标题翻译：取代的恶二唑酮的制备方法
公开(公告)号：US5756752A
公开(公告)日：1998-05-26
申请号：US842585
申请日：1997-04-15
申请人： Hans Joachim Diehr , Reinhard Lantzsch , Jacqueline M. Applegate , Klaus Jelich
发明人： Hans Joachim Diehr , Reinhard Lantzsch , Jacqueline M. Applegate , Klaus Jelich
IPC分类号： C07C241/04 , C07C243/28 , C07D271/10 , C07D271/113 , C07D271/07 , C07B41/04 , C07C243/20
CPC分类号： C07D271/113 , C07C241/04
摘要： Substituted oxadiazolones of the formula (I) ##STR1## in which R represents optionally substituted alkyl, are obtained in good yields and high purity on reacting in a first step carboxylic acids of the general formula (II) R--COOH (II) with hydrazine hydrate in the presence of a catalyst and an inert diluent at temperatures between 0.degree. C. and 150.degree. C. with elimination of water and removal of said catalyst and reacting the resulting carboxylic hydrazides of the general formula (III) R--CO--NH--NH.sub.2 (III) in a second step with phosgene (COCl.sub.2) at temperatures between 20.degree. C. and 120.degree. C.
摘要翻译：在通式（II）中，R-COOH（II）的第一步羧酸反应获得式（I）的取代的恶二唑酮，其中R表示任选取代的烷基，产率高，纯度高）与肼水合物在催化剂和惰性稀释剂存在下，在0℃至150℃之间的温度下，除去水并除去所述催化剂，并使所得的通式（III）的羧酰肼与R- CO-NH-NH 2（III）在第二步中与光气（COCl 2）在20℃至120℃之间。

2. 发明授权

US5166165A Fungicidal agents based on heterocyclically substituted sulphones 失效
标题翻译：基于杂环取代的磺化物的杀真菌剂
公开(公告)号：US5166165A
公开(公告)日：1992-11-24
申请号：US775632
申请日：1991-10-10
申请人： Gerd Kleefeld , Hans-Joachim Diehr , Wilhelm Haas , Heinz-Wilhelm Dehne , Wilhelm Brandes
发明人： Gerd Kleefeld , Hans-Joachim Diehr , Wilhelm Haas , Heinz-Wilhelm Dehne , Wilhelm Brandes
IPC分类号： A01N43/82 , A01N43/824 , C07D271/10 , C07D271/113 , C07D285/12 , C07D285/125
CPC分类号： C07D271/113 , A01N43/82 , C07D285/125
摘要： Use of compounds of the formula (I) ##STR1## in which Ar, R and X have the meaning indicated in the description, for combating phytopathogenic fungi in agriculture.The compounds of the formula (I), are known and can be prepared by analogous processes, for example by oxidizing the corresponding thio compounds, for example using potassium permanganate.
摘要翻译：使用式（I）化合物（Ⅰ）其中Ar，R和X具有说明书所述的含义，用于防治农业中的植物病原真菌。式（I）的化合物是已知的，并且可以通过类似的方法制备，例如通过氧化相应的硫代化合物，例如使用高锰酸钾。

3. 发明授权

US5162539A Preparation of 2-alkylthio-1,3,4-thiadiazoles 失效
标题翻译： 2-烷基硫代-1,3,4-噻二唑的制备
公开(公告)号：US5162539A
公开(公告)日：1992-11-10
申请号：US646563
申请日：1991-01-25
申请人： Hans-Joachim Diehr
发明人： Hans-Joachim Diehr
IPC分类号： C07B61/00 , C07D285/12 , C07D285/125
CPC分类号： C07D285/125
摘要： A process for the preparation of a 2-alkylthio-1,3,4-thiadiazole of the formula ##STR1## in which R.sup.1 represents alkyl which is optionally substituted by halogen andR.sup.2 represents alkyl or aralkyl,which comprises reacting a carboxylic acid of the formulaR.sup.1 --COOH (II),with a dithiocarbazic ester of the formula ##STR2## in the presence of phosphoryl chloride (POCl.sub.3) at a temperature between -20.degree. C. and +120.degree. C.
摘要翻译：制备式（I）的2-烷硫基-1,3,4-噻二唑的方法，其中R 1表示任选被卤素取代的烷基，R 2表示烷基或芳烷基，其包括使羧酸式Ⅱ的酸与式（III）的二硫代肼基酯在磷酰氯（POCl 3）存在下，在-20℃至+ 120℃的温度下反应。

4. 发明授权

US4988379A Sulphonyliso(thio)urea derivatives as herbicides 失效
标题翻译：磺酰基（硫代）脲衍生物作为除草剂
公开(公告)号：US4988379A
公开(公告)日：1991-01-29
申请号：US293275
申请日：1989-01-04
申请人： Hans-Joachim Diehr , Christa Fest , Rolf Kirsten , Joachim Kluth , Klaus-Helmut Muller , Theodor Pfister , Uwe Priesnitz , Hans-Jochem Riebel , Wolfgang Roy , Hans-Joachim Santel , Robert R. Schmidt , Ludwig Eue
发明人： Hans-Joachim Diehr , Christa Fest , Rolf Kirsten , Joachim Kluth , Klaus-Helmut Muller , Theodor Pfister , Uwe Priesnitz , Hans-Jochem Riebel , Wolfgang Roy , Hans-Joachim Santel , Robert R. Schmidt , Ludwig Eue
IPC分类号： A01N47/42 , C07D521/00
CPC分类号： C07D521/00 , A01N47/42
摘要： The invention relates to new sulphonyliso(thio)-urea derivatives of the general formula (I) ##STR1## in which R.sup.1 represents an optionally substituted radical from the series comprising alkyl, aralkyl, aryl and heteroaryl,R.sup.2 represents an optionally substituted and/or optionally fused 6-membered aromatic heterocyclic radical containing at least one nitrogen atom,R.sup.3 represents an optically substituted aromatic or heteroaromatic radical,X represents oxygen or sulphur andM represents hydrogen or an equivalent of a metal,and adducts of compounds of the formula (I) with strong acids, processes for their preparation, and their use as herbicides.

5. 发明授权

US4780126A 3-substituted 1-(2-halogenoalkoxy-benzenesulphonyl)-3-heteroaryl-(thio)ureas 失效
标题翻译： 3-取代的1-（2-卤代烷氧基 - 苯磺酰基）-3-杂芳基 - （硫代）脲
公开(公告)号：US4780126A
公开(公告)日：1988-10-25
申请号：US060187
申请日：1987-06-09
申请人： Hans-Joachim Diehr , Christa Fest , Rolf Kirsten , Joachim Kluth , Klaus-Helmut Muller , Theodor Pfister , Uwe Priesnitz , Hans-Jochem Riebel , Wolfgang Roy , Hans-Joachim Santel , Robert R. Schmidt , Ludwig Eue , Ernst Kysela
发明人： Hans-Joachim Diehr , Christa Fest , Rolf Kirsten , Joachim Kluth , Klaus-Helmut Muller , Theodor Pfister , Uwe Priesnitz , Hans-Jochem Riebel , Wolfgang Roy , Hans-Joachim Santel , Robert R. Schmidt , Ludwig Eue , Ernst Kysela
IPC分类号： A01N47/36 , C07C311/65 , C07C331/32 , C07D521/00 , C07D251/42 , A01N43/66 , C07D251/46
CPC分类号： C07D521/00 , A01N47/36 , C07C311/65 , C07C331/32
摘要： 3-Substituted 1-(2-halogenoalkoxy-benzenesulphonyl)-3-heteroaryl-(thio)urea herbicides of the formula ##STR1## in which (A)R is CF.sub.3,Q is O,R.sup.1 is CH.sub.3, C.sub.2 H.sub.5, C.sub.3 H.sub.7 -n, C.sub.3 H.sub.7 -i, CH.sub.2 --CH.dbd.CH.sub.2, CH.sub.2 --C.tbd.CH or CH.sub.2 --C.sub.6 H.sub.5,R.sup.2 is CH.sub.3, OCH.sub.3, OC.sub.2 H.sub.5, SCH.sub.3, NH--CH.sub.3 or NH--C.sub.2 H.sub.5,X is N,Y is N andZ is C--CH.sub.3, C--C.sub.2 H.sub.5, C--OCH.sub.3 or C--OC.sub.2 H.sub.5 ; or(B)R is CF.sub.3,Q is O,R.sup.1 is CH.sub.3, C.sub.2 H.sub.5, C.sub.3 H.sub.7 -n, C.sub.3 H.sub.7 -i, CH.sub.2 --CH.dbd.CH.sub.2, CH.sub.2 --C.tbd.CH or CH.sub.2 --C.sub.6 H.sub.5,R.sup.2 is CH.sub.3, OCH.sub.3 or OC.sub.2 H.sub.5,X is N,Y is C--H andZ is C--C.sub.2 H.sub.5, C--OCH.sub.3 or C--OC.sub.2 H.sub.5 ; or(C)R is CH.sub.2 --CH.sub.2 Cl,Q is O,R.sup.1 is CH.sub.3, C.sub.2 H.sub.5, C.sub.3 H.sub.7 -n, C.sub.3 H.sub.7 -i, CH.sub.2 --CH.dbd.CH.sub.2, CH.sub.2 --C.tbd.CH or CH.sub.2 --C.sub.6 H.sub.5,R.sup.2 is CH.sub.3, OCH.sub.3, OC.sub.2 H.sub.5, SCH.sub.3, NH--CH.sub.3 or NH--C.sub.2 H.sub.5,X is N,Y is N andZ is C--CH.sub.3, C--C.sub.2 H.sub.5, C--OCH.sub.3 or C--OC.sub.2 H.sub.5 ; or(D)R is CH.sub.2 --CH.sub.2 Cl,Q is O,R.sup.1 is CH.sub.3, C.sub.2 H.sub.5, C.sub.3 H.sub.7 -n, C.sub.3 H.sub.7 -i, CH.sub.2 --CH.dbd.CH.sub.2, CH.sub.2 --C.tbd.CH or CH.sub.2 --C.sub.6 H.sub.5,R.sup.2 is CH.sub.3, OCH.sub.3 or OC.sub.2 H.sub.5,X is N,Y is C--H andZ is C--CH.sub.3, C--C.sub.2 H.sub.5, C--OCH.sub.3 or C--OC.sub.2 H.sub.5 ; or(E)R is CHF.sub.2,Q is O,R.sup.1 is CH.sub.3,R.sup.2 is CH.sub.3,X is N,Y is N andZ is C--CH.sub.3,or a salt thereof with a metal or basic organic nitrogen compound.
摘要翻译：（A）R为CF 3，Q为O，R 1为CH 3，C 2 H 5，C 3 H 7 -n的3-取代的1-（2-卤代烷氧基 - 苯磺酰基）-3-杂芳基 - （硫代）脲除草剂，C 3 H 7 -i，CH 2 -CH = CH 2，CH 2 -C 3 CH 2或CH 2 -C 6 H 5，R 2是CH 3，OCH 3，OC 2 H 5，SCH 3，NH-CH 3或NH-C 2 H 5，X是N，Y是N，Z是C -CH 3，C-C 2 H 5，C-OCH 3或C-OC 2 H 5; 或（B）R是CF 3，Q是O，R 1是CH 3，C 2 H 5，C 3 H 7-n，C 3 H 7-i，CH 2 -CH = CH 2，CH 2 -C 3 CH 2或CH 2 -C 6 H 5，R 2是CH 3，OCH 3或OC 2 H 5， X是N，Y是CH，Z是C-C 2 H 5，C-OCH 3或C-OC 2 H 5; 或（C）R是CH 2 -CH 2 Cl，Q是O，R 1是CH 3，C 2 H 5，C 3 H 7-n，C 3 H 7 -i，CH 2 -CH = CH 2，CH 2 -C 3 CH 2或CH 2 -C 6 H 5，R 2是CH 3，OCH 3， OC2H5，SCH3，NH-CH3或NH-C2H5，X是N，Y是N，Z是C-CH3，C-C2H5，C-OCH3或C-OC2H5; 或（D）R是CH 2 -CH 2 Cl，Q是O，R 1是CH 3，C 2 H 5，C 3 H 7-n，C 3 H 7 -i，CH 2 -CH = CH 2，CH 2 -C 3 CH 2或CH 2 -C 6 H 5，R 2是CH 3，OCH 3或 OC2H5，X是N，Y是CH，Z是C-CH3，C-C2H5，C-OCH3或C-OC2H5; 或（E）R是CHF 2，Q是O，R 1是CH 3，R 2是CH 3，X是N，Y是N，Z是C-CH 3，或其与金属或碱性有机氮化合物的盐。

6. 发明授权

US4743294A N'-(substituted-1,3,5- triazin-2-yl)-N"-amino-N"'-(substituted-benzenesulphonyl)-guanidines as herbicides 失效
标题翻译： N' - （取代-1,3,5-三嗪-2-基）-N“ - 氨基-N” - （取代苯磺酰基） - 胍为除草剂
公开(公告)号：US4743294A
公开(公告)日：1988-05-10
申请号：US41260
申请日：1987-04-22
申请人： Hans-Joachim Diehr , Christa Fest , Rolf Kirsten , Joachim Kluth , Klaus-Helmut Muller , Theodor Pfister , Uwe Priesnitz , Hans-Jochem Riebel , Wolfgang Roy , Hans-Joachim Santel , Robert R. Schmidt , Koichi Moriya , Ludwig Eue , Klaus Lurssen
发明人： Hans-Joachim Diehr , Christa Fest , Rolf Kirsten , Joachim Kluth , Klaus-Helmut Muller , Theodor Pfister , Uwe Priesnitz , Hans-Jochem Riebel , Wolfgang Roy , Hans-Joachim Santel , Robert R. Schmidt , Koichi Moriya , Ludwig Eue , Klaus Lurssen
IPC分类号： A01N47/44 , A01N51/00 , C07D239/42 , C07D239/46 , C07D251/46 , C07D409/12 , C07D521/00 , A01N43/66 , C07D251/22 , C07D401/12
CPC分类号： C07D239/42 , A01N47/44 , A01N51/00 , C07C309/00 , C07D239/47 , C07D251/46 , C07D409/12 , C07D521/00
摘要： A selective herbicide of the formula ##STR1## in which m is 0, 1 or 2,R.sup.5 is an organic radical,R.sup.3 is hydrogen or an organic radical,R.sup.9 is hydrogen or an optionally substituted alkyl radical,R.sup.10 is an organic radical or forms a ring with R.sup.9,R.sup.40 and R.sup.41 are alkyl or alkoxy, andM is hydrogen or a metal or ammonium radical, or an acid adduct thereof.
摘要翻译：式（I）的选择性除草剂，其中m为0,1或2，R 5为有机基团，R 3为氢或有机基团，R 9为氢或任选取代的烷基，R 10为有机基团或基团具有R 9，R 40和R 41的环是烷基或烷氧基，M是氢或金属或铵基或其酸加合物。

7. 发明授权

US4658027A Process for the preparation of 1-(2-oxyaminosulphonyl-phenylsulphonyl)-3-heteroaryl-ureas 失效
标题翻译： 1-（2-氧氨基磺酰基 - 苯基磺酰基）-3-杂芳基脲的制备方法
公开(公告)号：US4658027A
公开(公告)日：1987-04-14
申请号：US769184
申请日：1985-08-23
申请人： Hans-Joachim Diehr , Christa Fest , Rolf Kirsten , Joachim Kluth , Klaus-Helmut Muller , Theodor Pfister , Uwe Priesnitz , Hans-Jochem Riebel , Wolfgang Roy
发明人： Hans-Joachim Diehr , Christa Fest , Rolf Kirsten , Joachim Kluth , Klaus-Helmut Muller , Theodor Pfister , Uwe Priesnitz , Hans-Jochem Riebel , Wolfgang Roy
IPC分类号： A01N47/34 , A01N47/36 , C07D213/75 , C07D239/42 , C07D239/46 , C07D239/48 , C07D239/54 , C07D251/44 , C07D251/50 , C07D251/52 , C07D417/12 , C07D521/00 , C07D239/47 , C07D251/42 , C07D257/08
CPC分类号： C07D521/00 , A01N47/36
摘要： A process for the preparation of a 1-(2-oxyaminosulphonyl-phenylsulphonyl)-urea of the formula ##STR1## in which R.sup.1 is an optionally substituted radical from the series comprising alkyl, alkenyl, alkinyl, cycloalkyl, cycloalkylalkyl, aralkyl and aryl,R.sup.2 is hydrogen or an optionally substituted radical from the series comprising alkyl, alkenyl, alkinyl and aralkyl, andR.sup.3 is an optionally substituted and/or optionally fused six-membered aromatic heterocyclic radical containing at least one nitrogen atom,comprising reacting water with a benzodisultam of the formula ##STR2## at a temperature between 0.degree. C. and 100.degree. C. The products are herbicidally active.
摘要翻译：一种制备式（IMAGE）的1-（2-氧氨基磺酰基 - 苯基磺酰基） - 脲的方法，其中R 1是包含烷基，链烯基，炔基，环烷基，环烷基烷基，芳烷基和芳基的任意取代的基团， R 2是氢或任选取代的基团，其包含烷基，链烯基，炔基和芳烷基，并且R 3是任选被取代的和/或任选地稠合的含有至少一个氮原子的六元芳族杂环基团，包括使水与苯并二枯基在0℃至100℃之间的温度下，该产物具有除草活性。

8. 发明授权

US4334073A Process for the preparation of alpha-hydroxycarboxylic acid amide compounds 失效
标题翻译： α-羟基羧酸酰胺化合物的制备方法
公开(公告)号：US4334073A
公开(公告)日：1982-06-08
申请号：US211989
申请日：1980-12-01
申请人： Hans-Joachim Diehr
发明人： Hans-Joachim Diehr
IPC分类号： C07B41/02 , B01J31/00 , B01J31/02 , C07B31/00 , C07C67/00 , C07C231/00 , C07C231/12 , C07C235/06 , C07C235/14 , C07C235/16 , C07C235/34 , C07D209/08 , C07D211/16 , C07D215/08 , C07D295/16 , C07D295/182 , C07D295/185 , C07D85/24
CPC分类号： C07D295/185 , C07D209/08 , C07D215/08 , C07D295/182
摘要： Process for the preparation of an alpha-hydroxycarboxylic acid amide compound of the formula ##STR1## wherein R.sup.1 is hydrogen or alkyl; andR.sup.2 and R.sup.3 are individually selected from hydrogen, alkyl, alkenyl, alkynyl, aralkyl, cycloalkyl or aryl, each of which may be optionally substituted, or a nitrogen-containing heterocyclic radical; orR.sup.2 and R.sup.3, together with the nitrogen atom to which they are bonded, represent an optionally benzo-fused monocyclic or bicyclic ring, which ring may be substituted and may be partially unsaturated,which process comprises reacting in a first stage an alpha-halocarboxylic acid amide of the formula ##STR2## wherein R.sup.1, R.sup.2 and R.sup.3 are identified as above; andHal is chlorine or bromine,with an alkali metal acetate or alkaline earth metal acetate in the presence of a quaternary ammonium salt at a temperature between 20.degree. and 200.degree. C., and, in a second stage, deacylating the alpha-acetoxycarboxylic acid amide produced, having the general formula ##STR3## in which R.sup.1, R.sup.2 and R.sup.3, are identified as above by reacting said amide III with an alcohol of the general formulaR.sup.4 --OH (IV)in which R.sup.4 is alkyl in the presence of a catalytic amount of a catalyst selected from alkali metal hydroxides, alkaline earth metal hydroxides, alkali metal carbonates, and alkaline earth metal carbonates, at a temperature between 20.degree. and 150.degree. C., these compounds are useful as intermediates in the preparation of herbicides, e.g., substituted sulfonyl glycol amides and anilides.
摘要翻译：制备式（I）的α-羟基羧酸酰胺化合物的方法，其中R 1是氢或烷基; R 2和R 3各自独立地选自氢，烷基，烯基，炔基，芳烷基，环烷基或芳基，其各自可以被任选取代，或含氮杂环基; 或R 2和R 3与它们所键合的氮原子一起代表任选的苯并稠合单环或双环，该环可以被取代并且可以是部分不饱和的，该方法包括在第一阶段使α-卤代羧酸式（II）的酰胺，其中R1，R2和R3如上所述鉴定; 和Hal是氯或溴，与碱金属乙酸盐或碱土金属乙酸盐在季铵盐的存在下在20至200℃的温度下进行，并且在第二阶段中，将α-乙酰氧基羧酸酰胺，其通式如下：其中R 1，R 2和R 3如上所定义，通过使所述酰胺III与通式为R4-OH（Ⅳ）的醇反应，其中R 4为烷基，在20至150℃的温度下，存在催化量的选自碱金属氢氧化物，碱土金属氢氧化物，碱金属碳酸盐和碱土金属碳酸盐的催化剂，这些化合物可用作制备中的中间体的除草剂，例如取代的磺酰基二醇酰胺和酰苯胺。

9. 发明授权

US5780392A Heterocyclyl-1,3,4-thiadiazolyloxyacetamides and their use as herbicides 失效
标题翻译：杂环基-1,3,4-噻二唑氧基乙酰胺及其作为除草剂的用途
公开(公告)号：US5780392A
公开(公告)日：1998-07-14
申请号：US721981
申请日：1996-10-04
申请人： Heinz Forster , Hans-Joachim Diehr , Hans-Joachim Santel , Markus Dollinger
发明人： Heinz Forster , Hans-Joachim Diehr , Hans-Joachim Santel , Markus Dollinger
IPC分类号： A01N43/82 , A01N43/824 , A01N43/836 , C07D417/04 , C07D417/14
CPC分类号： C07D417/04 , A01N43/82 , C07D417/14
摘要： This invention concerns heterocyclyl-1,3,4-thiadiazolyloxycetamides of the formula ##STR1## in which R.sup.1 is hydrogen or optionally substituted alkyl, alkenyl, alkinyl or aralkyl, R.sup.2 is optionally substituted alkyl, alkenyl, alkinyl, cycloalkyl, cycloalkenyl, aralkyl, aryl, alkoxy, alkenyloxy or alkinyloxy or R.sup.1 and R.sup.2, together with the nitrogen atom to which they are bound, form an optionally substituted, saturated or unsaturated nitrogen heterocycle which may contain other hetero-atoms and to which a benzo-grouping can be fused, and Het is an optionally substituted heterocyclyl group with the exception of thienyl. The Invention also concerns a method of preparing such compounds, intermediates used in their preparation and the use of such compounds as herbicides.
摘要翻译： PCT No.PCT / EP95 / 01174 Sec。 371日期1996年10月4日第 102（e）日期1996年10月4日PCT 1995年3月29日PCT PCT。公开号WO94 / 27711 日期：1995年10月19日本发明涉及式（I）中的R 1为氢或任选取代的烷基，烯基，炔基或芳烷基的杂环基-1,3,4-噻二唑氧基鲸酰胺，R 2为任选取代的烷基，烯基，链烯基，环烷基，环烯基，芳烷基，芳基，烷氧基，烯氧基或烷氧基或R1和R2与它们所连接的氮原子一起形成任选取代的饱和或不饱和的氮杂环，其可含有其它杂原子，其可以稠合苯并基团，Het是除噻吩基以外的任选取代的杂环基。本发明还涉及制备这种化合物的方法，其制备中使用的中间体和除草剂等化合物的用途。

10. 发明授权

US5147443A Microbicidal agents 失效
标题翻译：微生物剂
公开(公告)号：US5147443A
公开(公告)日：1992-09-15
申请号：US767528
申请日：1991-09-26
申请人： Hans-Joachim Diehr , Karl-Heinz Kuck , Wilfried Paulus , Hans-Georg Schmitt
发明人： Hans-Joachim Diehr , Karl-Heinz Kuck , Wilfried Paulus , Hans-Georg Schmitt
IPC分类号： A01N43/82 , A01N43/824 , B27K3/34 , C07D285/12 , C07D285/125
CPC分类号： C07D285/125 , A01N43/82
摘要： The invention relates to the use of 2,5-substituted 1,3,4-thiadiazoles of the formula ##STR1## in which R.sup.1 stands for straight-chain or branched halogenoalkyl,R.sup.2 stands for straight-chain or branched alkyl andn stands for the numbers 1 or 2,as microbicides for protecting industrial materials.
摘要翻译：本发明涉及式（Ⅰ）的2,5-取代的1,3,4-噻二唑，其中R1代表直链或支链卤代烷基，R2代表直链或支链烷基， n代表数字1或2，作为用于保护工业材料的杀菌剂。

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