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    • 2. 发明申请
    • Aqueous compositions comprising alkyl polyethylene glycol ether sulfates
    • 包含烷基聚乙二醇醚硫酸盐的水性组合物
    • US20090023817A1
    • 2009-01-22
    • US12217938
    • 2008-07-10
    • Hendrik AhrensGuillermo MaierKlaus Raab
    • Hendrik AhrensGuillermo MaierKlaus Raab
    • A61K8/86C11D17/00C08L81/00B01F17/52
    • B01F17/0057C08F2/26C09B67/0086C11D1/29
    • The present invention provides aqueous compositions comprising, as well as water, 75% to 90% by weight of alkyl polyethylene glycol ether sulfates which are a mixture of compounds of formula (1) R1—O—(CH2—CH2—O)x—SO3M  (1) where R1 is a branched alkyl or alkenyl group having 8 to 14 carbon atoms and at least one tertiary carbon atom, x is from 3 to 15, M is an alkali metal ion or an ammonium ion, with compounds of formula (2) R2—O—(CH2—CH2—O)y—SO3M′  (2) where R2 is a linear alkyl or alkenyl group having 8 to 14 carbon atoms, y is from 3 to 15, M′ is an alkali metal ion or an ammonium ion, wherein the mixing ratio of compounds of formulae (1) and (2) is chosen such that the compounds of formula (1) comprise at least 10% by weight and at most 99% by weight of the total amount of compounds of formulae (1) and (2).
    • 本发明提供含有75%至90%(重量)的烷基聚乙二醇醚硫酸盐的水性组合物,它们是式(1)化合物的混合物。 公式“end =”lead“?> R1-O-(CH2-CH2-O)x-SO3M(1)<?in-line-formula description =”In-line Formulas“end =”tail“?>其中R1 是具有8至14个碳原子和至少一个叔碳原子的支链烷基或烯基,x为3至15,M为碱金属离子或铵离子,式(2)化合物< line-formula description =“In-line Formulas”end =“lead”?> R2-O-(CH2-CH2-O)y-SO3M'(2)<?in-line-formula description = “end =”tail“?>其中R2是具有8至14个碳原子的直链烷基或烯基,y为3至15,M'为碱金属离子或铵离子,其中化合物 选择式(1)和(2)使得式(1)的化合物包含至少10重量%和至多99 (1)和(2)化合物的总量的重量百分比。
    • 4. 发明授权
    • Process for the preparation of aqueous betaine solutions
    • 制备甜菜碱水溶液的方法
    • US5292942A
    • 1994-03-08
    • US42115
    • 1993-04-02
    • Rudolf AignerGuillermo MaierRainer MullerHubert Seitz
    • Rudolf AignerGuillermo MaierRainer MullerHubert Seitz
    • C07C227/08C07C229/12C07C229/16C07C231/12C07C233/36C11D1/90C07C229/00
    • A61K8/44C07C227/08C07C231/12A61Q19/10
    • A process is described for the preparation of aqueous solutions of betaines of the formula ##STR1## in which: R.sup.1 is an alkyl radical having 6 to 22 carbon atoms or is a radical of the formula R'CONH(CH.sub.2).sub.z --, in which R' has the meaning of R.sup.1 and z is 2, 3 or 4, R.sup.2 is an alkyl radical having 1 to 4 carbon atoms or is a radical of the formula --(CH.sub.2).sub.m --OH, in which m is 1, 2 or 3, R.sup.3 is an alkyl radical having 1 to 4 carbon atoms or is a radical of said formula --(CH.sub.2).sub.m --OH and y is 1, 2 or 3. The aqueous betaine solutions are prepared by quaternization of the corresponding tertiary amines with an .omega.-halocarboxylic acid and with an alkali metal hydroxide in the aqueous phase. The quaternization is carried out continuously in two or three stirred tanks arranged in a cascade, defined process characteristics being maintained in each tank. Using the novel process, aqueous betaine solutions are obtained in high yield and purity in a simple manner.
    • 描述了制备式“β”的甜菜碱水溶液的方法,其中:R 1是具有6至22个碳原子的烷基,或者是式R'CONH(CH 2)z - 的基团,其中 R'具有R 1的含义,z是2,3或4,R 2是具有1至4个碳原子的烷基,或者是式 - (CH 2)m -OH的基团,其中m是1,2或 3,R 3是具有1至4个碳原子的烷基或是所述式 - (CH 2)m -OH的基团,y是1,2或3.通过季铵化相应的叔胺与 ω-卤代羧酸和碱金属氢氧化物在水相中。 季铵化在连续排列的两个或三个搅拌槽中连续进行,在每个罐中保持定义的工艺特性。 使用该新方法,以简单的方式以高产率和纯度获得甜菜碱水溶液。