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1. 发明授权

US07074922B2 Method for producing the tautomeric form of (1) of 2,4,6-trianilino-p-(carbo-1′-ethylhexyl-1′oxyl)-1, 3, 5-triazine 有权
标题翻译：制备（1）2,4,6-三苯胺基 - 对 - （碳-1'-乙基己基-1'-氧基）-1,3,5-三嗪的互变异构形式的方法
公开(公告)号：US07074922B2
公开(公告)日：2006-07-11
申请号：US10503305
申请日：2003-02-26
申请人： Helmut Gümbel , Heinz-Josef Kneuper , Rainer Becker , Gerhard Bertlein , Michael Drögemüller
发明人： Helmut Gümbel , Heinz-Josef Kneuper , Rainer Becker , Gerhard Bertlein , Michael Drögemüller
IPC分类号： C07D251/70 , A61K7/42
CPC分类号： C07D251/70
摘要： The invention relates to a method for producing the tautomeric form (I) of 2,4,6-trianilino-p-(carbo-2′-ethylhexyl-1′-oxy)-1,3,5-triazine by the crystallization of a tautoner mixture in the presence of one or more solvents selected from the group consisting of aliphatic alcohol having 2 8 C-atoms made of aliphatic alcohol, aliphatic carboxylic acid alkyl esters having a total of between 3–10 C-atoms, aromatic carboxylic acid alkyl esters having a total of between 8–12 C-atoms, aliphatic carboxylic acid esters having a total of between 3 9 C-atoms, carboxylic acid nitriles having a total of between 2–8 C-atoms, dialkylketones having a total of between 3–6 C-atoms and aliphatic sulphones having a total of between 3–6 C-atoms. The solvent or solvent mixture can additionally contain up to 30 wt % of a hydrocarbon (I) acts as a light protecting agent in cosmetic preparations.
摘要翻译：本发明涉及通过结晶形成2,4,6-三苯胺基 - 对 - （碳 - 2'-乙基己基-1'-氧）-1,3,5-三嗪的互变异构体形式（I）的方法，在一种或多种选自由脂族醇制成的具有28个碳原子的脂族醇，总共3-10个碳原子的脂族羧酸烷基酯，芳族羧酸总共有8-12个C原子的烷基酯，总共有3 9个C原子的脂族羧酸酯，总共有2-8个C原子的羧酸腈，总共有2-8个碳原子之间的二烷基酮 3-6个C原子和总共3-6个碳原子的脂肪族砜。溶剂或溶剂混合物可另外含有至多30重量％的化合物（I）作为化妆品制剂中的防光剂。

2. 发明申请

US20070167653A1 Method for producing acylphosphine oxide solids 有权
标题翻译：生产酰基氧化膦固体的方法
公开(公告)号：US20070167653A1
公开(公告)日：2007-07-19
申请号：US10551994
申请日：2004-03-30
申请人： Gerhard Bertlein , Karl Schall , Matthias Maase , Jorg Heilek , Dieter Baumann , Hermann Ascherl
发明人： Gerhard Bertlein , Karl Schall , Matthias Maase , Jorg Heilek , Dieter Baumann , Hermann Ascherl
IPC分类号： C07F9/02
CPC分类号： C07F9/5337
摘要： The present invention relates to a process for the preparation of solid acylphosphine oxides by converting an acylphosphine oxide which is in the form of a melt or in dispersed form into the solid state of aggregation with mechanical stress, shearing/internal agitation of the melt.
摘要翻译：本发明涉及一种制备固体酰基氧化膦的方法，该方法是将熔体形式或分散形式的酰基氧化膦转化成具有机械应力，熔体的剪切/内部搅拌的聚集状态。

3. 发明授权

US07776109B2 Method for producing acylphosphine oxide solids 有权
标题翻译：生产酰基氧化膦固体的方法
公开(公告)号：US07776109B2
公开(公告)日：2010-08-17
申请号：US10551994
申请日：2004-03-30
申请人： Gerhard Bertlein , Karl Heinz Schall , Matthias Maase , Joerg Heilek , Dieter Baumann , Hermann Ascherl
发明人： Gerhard Bertlein , Karl Heinz Schall , Matthias Maase , Joerg Heilek , Dieter Baumann , Hermann Ascherl
IPC分类号： B01J6/00
CPC分类号： C07F9/5337
摘要： The present invention relates to a process for the preparation of solid acylphosphine oxides by converting an acylphosphine oxide which is in the form of a melt or in dispersed form into the solid state of aggregation with mechanical stress, shearing/internal agitation of the melt.
摘要翻译：本发明涉及一种制备固体酰基氧化膦的方法，该方法是将熔体形式或分散形式的酰基氧化膦转化成具有机械应力，熔体的剪切/内部搅拌的聚集状态。

4. 发明授权

US07495130B2 Method for producing substituted arylcarboxylic acid chlorides 有权
标题翻译：取代芳基羧酸氯化物的制备方法
公开(公告)号：US07495130B2
公开(公告)日：2009-02-24
申请号：US10564855
申请日：2004-07-14
申请人： Matthias Maase , Gerhard Bertlein , Holger Ganz , Matthias Dust
发明人： Matthias Maase , Gerhard Bertlein , Holger Ganz , Matthias Dust
IPC分类号： C07C51/58 , C07C63/10
CPC分类号： C07C51/58 , C07C63/04
摘要： A process for preparing mono- or poly-C1-C20-alkyl- and/or -halogen-substituted arylcarbonyl chlorides (I), by, in a first stage, reacting a mono- or poly-C1-C20-alkyl- and/or -halogen-substituted aromatic (II) with CCl4 in the presence of a Friedel-Crafts catalyst to give the corresponding mono- or poly-C1-C20-alkyl- and/or -halogen-substituted trichloromethylated aromatic (III),and, in a second stage, treating the trichloromethylated aromatic (III) with water or a protic acid in the presence of a catalyst to obtain the arylcarbonyl chloride (I).In a particularly preferred embodiment, the trichloromethylated aromatic (III) is not isolated as an intermediate and is used in the second stage dissolved in the solvent of the first stage.
摘要翻译：一种制备单-Ca-C20烷基和/或卤素取代的芳基羰基氯化物（I）的方法，在第一阶段中，使单 - 或多-C1-C20烷基 - 和/ 或 - 卤素取代的芳族（II）与CCl 4在Friedel-Crafts催化剂存在下反应，得到相应的单或多C1-C20烷基 - 和/或 - 卤素取代的三氯甲基化芳族（III）在第二阶段中，在催化剂存在下用水或质子酸处理三氯甲基化芳族化合物（III），得到芳基羰基氯（I）。在特别优选的实施方案中，三氯甲基化芳族（III）不作为中间体分离，并且用于溶解在第一阶段的溶剂中的第二阶段。

5. 发明申请

US20060178530A1 Method for producing substituted arylcarboxylic acid chlorides 有权
标题翻译：取代芳基羧酸氯化物的制备方法
公开(公告)号：US20060178530A1
公开(公告)日：2006-08-10
申请号：US10564855
申请日：2004-07-14
申请人： Matthias Maase , Gerhard Bertlein , Holger Ganz , Matthias Dust
发明人： Matthias Maase , Gerhard Bertlein , Holger Ganz , Matthias Dust
IPC分类号： C07C51/58
CPC分类号： C07C51/58 , C07C63/04
摘要： A process for preparing mono- or poly-C1-C20-alkyl- and/or -halogen-substituted arylcarbonyl chlorides (I), by, in a first stage, reacting a mono- or poly-C1-C20-alkyl- and/or -halogen-substituted aromatic (II) with CCl4 in the presence of a Friedel-Crafts catalyst to give the corresponding mono- or poly-C1-C20-alkyl- and/or -halogen-substituted trichloromethylated aromatic (III), and, in a second stage, treating the trichloromethylated aromatic (III) with water or a protic acid in the presence of a catalyst to obtain the arylcarbonyl chloride (I). In a particularly preferred embodiment, the trichloromethylated aromatic (III) is not isolated as an intermediate and is used in the second stage dissolved in the solvent of the first stage.
摘要翻译：通过在第一阶段中制备单或多-C 1 -C 20 - 烷基 - 和/或 - 卤素取代的芳基羰基氯（I）的方法，使单-CA或多-C 1 -C 20 - 烷基 - 和/或 - 卤素取代的芳族（II）与CCl 4

6. 发明申请

US20050143577A1 Method for producing the automeric form of (1) of 2, 4, 6-trianilino-p- (carbo-2'-ethyl-heyk-1'oxyl)-1, 2, 5-triazine 有权
标题翻译：（1）2,4,6-三苯胺基 - 对 - （碳 - 2'-乙基 - 喔基-1'-氧代）-1,2,5-三嗪的自身形式的方法
公开(公告)号：US20050143577A1
公开(公告)日：2005-06-30
申请号：US10503305
申请日：2003-02-26
申请人： Helmut Gumbel , Heinz-Josef Kneuper , Rainer Becker , Gerhard Bertlein , Michael Drogemuller
发明人： Helmut Gumbel , Heinz-Josef Kneuper , Rainer Becker , Gerhard Bertlein , Michael Drogemuller
IPC分类号： A61K8/00 , A61K8/49 , A61Q17/04 , C07D251/70 , C07D251/54 , A61K7/42
CPC分类号： C07D251/70
摘要： Process for the preparation of the tautomeric form I of 2,4,6-trianilino-p-(carbo-2′-ethylhexyl-1′-oxy)-1,3,5-triazine by crystallization from a tautomer mixture in the presence of one or more solvents chosen from the group consisting of aliphatic alcohols having 2 to 8 carbon atoms, aliphatic carboxylic alkyl esters having a total of 3 to 10 carbon atoms, aromatic carboxylic alkyl esters having a total of 8 to 12 carbon atoms, aliphatic carbonic esters having a total of 3 to 9 carbon atoms, carbonitriles having a total of 2 to 8 carbon atoms, dialkyl ketones having a total of 3 to 6 carbon atoms and aliphatic sulfones having a total of 3 to 6 carbon atoms, where the solvent or the solvent mixture may additionally comprise up to 30% by weight of a hydrocarbon. I is used as light protection agent in cosmetic preparations.
摘要翻译：在存在下由互变异构体混合物结晶制备2,4,6-三苯胺基 - 对 - （碳 - 2'-乙基己基-1'-氧）-1,3,5-三嗪的互变异构形式I的方法选自碳原子数2〜8的脂肪族醇，碳原子数为3〜10的脂肪族羧酸烷基酯，碳原子数为8〜12的芳香族羧酸烷基酯，脂肪族碳酸酯具有总共3至9个碳原子的酯，总共具有2至8个碳原子的碳原子，总共3至6个碳原子的二烷基酮和总共具有3至6个碳原子的脂族砜，其中溶剂或溶剂混合物可以另外包含至多30重量％的烃。我用作化妆品制剂中的防晒剂。

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