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1. 发明授权

US08460823B1 Electrochemical components employing polysiloxane-derived binders 有权
标题翻译：使用聚硅氧烷衍生的粘合剂的电化学成分
公开(公告)号：US08460823B1
公开(公告)日：2013-06-11
申请号：US12973342
申请日：2010-12-20
申请人： Frank M. Delnick
发明人： Frank M. Delnick
IPC分类号： H01M4/02 , H01M4/13 , H01M4/60
CPC分类号： H01M2/1653 , H01M4/13 , H01M4/139 , H01M4/622
摘要： A processed polysiloxane resin binder for use in electrochemical components and the method for fabricating components with the binder. The binder comprises processed polysiloxane resin that is partially oxidized and retains some of its methyl groups following partial oxidation. The binder is suitable for use in electrodes of various types, separators in electrochemical devices, primary lithium batteries, electrolytic capacitors, electrochemical capacitors, fuel cells and sensors.
摘要翻译：用于电化学组分的加工聚硅氧烷树脂粘合剂和用粘合剂制造组分的方法。粘合剂包括部分氧化的加工聚硅氧烷树脂，并在部分氧化后保留其一部分甲基。粘合剂适用于各种类型的电极，电化学装置中的分离器，一次锂电池，电解电容器，电化学电容器，燃料电池和传感器。

2. 发明授权

US07967875B2 Flexible cathodes 有权
标题翻译：柔性阴极
公开(公告)号：US07967875B2
公开(公告)日：2011-06-28
申请号：US12791221
申请日：2010-06-01
申请人： Christopher Boczer , Frank M. Delnick , Rosauro Del Rosario , Minkoo Kang , Lucyna M. Pawlowska , Michael Pozin , Dharmendra Rana , Maya Stevanovic , John J. Weckesser
发明人： Christopher Boczer , Frank M. Delnick , Rosauro Del Rosario , Minkoo Kang , Lucyna M. Pawlowska , Michael Pozin , Dharmendra Rana , Maya Stevanovic , John J. Weckesser
IPC分类号： H01M4/13 , H01M4/62 , H01M10/0568 , H01M10/0569
CPC分类号： H01M10/0569 , H01M4/0404 , H01M4/0411 , H01M4/131 , H01M4/1391 , H01M4/505 , H01M4/621 , H01M4/622 , H01M4/661 , H01M10/0525 , Y10T29/49108 , Y10T29/49115
摘要： This disclosure relates to methods of making a cathode for a lithium batter. The methods include: (a) treating a cathode current collector with flame or corona; (b) coating a slurry containing iron disulfide, a first solvent, and a binder onto the cathode current collector obtained from step (a) to form a coated cathode current collector, in which the slurry contains about 73-75% by weight solids and the binder contains a polymer selected from the group consisting of linear di- and tri-block copolymers, linear tri-block copolymers cross-linked with melamine resin, ethylene-propylene copolymers, ethylene-propylene-diene terpolymers, tri-block fluorinated thermoplastics, hydrogenated nitrile rubbers, fluoro-ethylene-vinyl ether copolymers, thermoplastic polyurethanes, thermoplastic olefins, and polyvinylidene fluoride homopolymers; and (c) drying the coated cathode current collector obtained from step (b) to provide a cathode, in which the cathode contains no more than 0.5% by volume of the first solvent and is capable of being bent to 180°. This disclosure also relates to methods of making a lithium battery.
摘要翻译：本公开涉及制备用于锂电池的阴极的方法。方法包括：（a）用火焰或电晕处理阴极集电器; （b）将含有二硫化铁，第一溶剂和粘合剂的浆料涂布到从步骤（a）获得的阴极集流体上，以形成涂覆的阴极集电器，其中浆料含有约73-75重量％的固体，粘合剂含有选自直链二嵌段和三嵌段共聚物，与三聚氰胺树脂交联的直链三嵌段共聚物，乙烯 - 丙烯共聚物，乙烯 - 丙烯 - 二烯三元共聚物，三嵌段氟化热塑性塑料，氢化丁腈橡胶，氟乙烯 - 乙烯基醚共聚物，热塑性聚氨酯，热塑性烯烃和聚偏氟乙烯均聚物; 和（c）将由步骤（b）获得的涂覆的阴极集电体干燥以提供阴极，其中阴极含有不超过0.5体积％的第一溶剂并且能够弯曲至180°。本公开还涉及制造锂电池的方法。

3. 发明授权

US5948464A Process of manufacturing porous separator for electrochemical power supply 失效
标题翻译：制造电化学电源多孔隔板的工艺
公开(公告)号：US5948464A
公开(公告)日：1999-09-07
申请号：US767468
申请日：1996-06-19
申请人： Frank M. Delnick
发明人： Frank M. Delnick
IPC分类号： B32B5/32 , C25B9/10 , H01G9/02 , H01M2/14 , H01M2/16 , H01M2/18 , H01M6/16 , H01M10/04 , B05D5/12
CPC分类号： H01M2/145 , C25B9/10 , H01G9/02 , H01M10/0436 , H01M2/1673 , H01M2/1646 , H01M2/1653 , H01M6/16
摘要： A method of forming a porous composite separator layer for an electrochemical cell comprising the steps of printing a thin layer of a separator precursor solution on the surface of one of the electrochemical cell electrodes, drying and curing the thin layer of separator precursor solution so that it transforms into a microporous composite separator structure. In the preferred embodiment, the separator precursor solution is formulated as an ink comprising a silica aerogel filler material dispersed in a solution of polymer binder which is dissolved in a suitable solvent. The process allows the manufacture of thin and flexible composite separators which are conformally bonded to the underlying electrodes.
摘要翻译：一种形成用于电化学电池的多孔复合隔离层的方法，包括以下步骤：在一个电化学电池电极的表面上印刷隔板前体溶液的薄层，干燥并固化隔膜前体溶液的薄层，使得其转化成微孔复合分离器结构。在优选的实施方案中，分离器前体溶液配制成包含分散在溶解在合适溶剂中的聚合物粘合剂溶液中的二氧化硅气凝胶填料的油墨。该方法允许制造薄且柔性的复合分离器，其被共形结合到下面的电极。

4. 发明申请

US20100236056A1 Flexible Cathodes 有权
标题翻译：柔性阴极
公开(公告)号：US20100236056A1
公开(公告)日：2010-09-23
申请号：US12791221
申请日：2010-06-01
申请人： Christopher Boczer , Frank M. Delnick , Rosauro Del Rosario , Minkoo Kang , Lucyna M. Pawlowska , Michael Pozin , Dharmendra Rana , Maya Stevanovic , John J. Weckesser
发明人： Christopher Boczer , Frank M. Delnick , Rosauro Del Rosario , Minkoo Kang , Lucyna M. Pawlowska , Michael Pozin , Dharmendra Rana , Maya Stevanovic , John J. Weckesser
IPC分类号： H01M10/04
CPC分类号： H01M10/0569 , H01M4/0404 , H01M4/0411 , H01M4/131 , H01M4/1391 , H01M4/505 , H01M4/621 , H01M4/622 , H01M4/661 , H01M10/0525 , Y10T29/49108 , Y10T29/49115
摘要： This disclosure relates to methods of making a cathode for a lithium batter. The methods include: (a) treating a cathode current collector with flame or corona; (b) coating a slurry containing iron disulfide, a first solvent, and a binder onto the cathode current collector obtained from step (a) to form a coated cathode current collector, in which the slurry contains about 73-75% by weight solids and the binder contains a polymer selected from the group consisting of linear di- and tri-block copolymers, linear tri-block copolymers cross-linked with melamine resin, ethylene-propylene copolymers, ethylene-propylene-diene terpolymers, tri-block fluorinated thermoplastics, hydrogenated nitrile rubbers, fluoro-ethylene-vinyl ether copolymers, thermoplastic polyurethanes, thermoplastic olefins, and polyvinylidene fluoride homopolymers; and (c) drying the coated cathode current collector obtained from step (b) to provide a cathode, in which the cathode contains no more than 0.5% by volume of the first solvent and is capable of being bent to 180°. This disclosure also relates to methods of making a lithium battery.
摘要翻译：本公开涉及制备用于锂电池的阴极的方法。方法包括：（a）用火焰或电晕处理阴极集电器; （b）将含有二硫化铁，第一溶剂和粘合剂的浆料涂布到从步骤（a）获得的阴极集流体上，以形成涂覆的阴极集电器，其中浆料含有约73-75重量％的固体，粘合剂含有选自直链二嵌段和三嵌段共聚物，与三聚氰胺树脂交联的直链三嵌段共聚物，乙烯 - 丙烯共聚物，乙烯 - 丙烯 - 二烯三元共聚物，三嵌段氟化热塑性塑料，氢化丁腈橡胶，氟乙烯 - 乙烯基醚共聚物，热塑性聚氨酯，热塑性烯烃和聚偏氟乙烯均聚物; 和（c）将由步骤（b）获得的涂覆的阴极集电体干燥以提供阴极，其中阴极含有不超过0.5体积％的第一溶剂并且能够弯曲至180°。本公开还涉及制造锂电池的方法。

5. 发明授权

US5865860A Process for filling electrochemical cells with electrolyte 失效
标题翻译：用电解质填充电化学电池的工艺
公开(公告)号：US5865860A
公开(公告)日：1999-02-02
申请号：US879936
申请日：1997-06-20
申请人： Frank M. Delnick
发明人： Frank M. Delnick
IPC分类号： H01M6/48 , B41J2/01 , H01M2/36 , H01M4/04 , H01M6/00
CPC分类号： H01M2/361 , B41J2/01 , H01M4/04 , Y10T29/49115
摘要： A process for manufacturing an electrochemical cell comprising the steps of providing an electrode and applying electrolyte to the electrode using an ink-jet printer. In the preferred embodiment of the present invention, an ink-jet printing process is utilized to print the electrolyte onto the surface of the electrodes and separators or the electrode/separator bilayers. The ink-jet printing accurately meters and uniformly distributes the electrolyte throughout the pore structure of the separator and the electrode without contaminating the cell gasket. Preferably, a drop-on-demand ink-jet printing head is used to facilitate the electrolyte printing process. The ink-jet printing head is electronically pulsed to form and eject the electrolyte droplets from a nozzle of printing-head. The volume and the distribution of each electrolyte droplet are accurately determined and controlled by varying the pulse width and the pulse frequency of the printing head.
摘要翻译：一种用于制造电化学电池的方法，包括以下步骤：使用喷墨打印机提供电极和将电解质施加到电极。在本发明的优选实施例中，使用喷墨印刷方法将电解质印刷到电极和隔板或电极/分离器双层的表面上。喷墨打印精确地计量并均匀地分布电解液遍及分离器和电极的孔结构，而不会污染电池垫片。优选地，按需喷墨打印头用于促进电解质印刷过程。喷墨打印头被电子脉冲以形成并从打印头的喷嘴喷出电解质液滴。通过改变打印头的脉冲宽度和脉冲频率来精确地确定和控制每个电解质液滴的体积和分布。

6. 发明授权

US5202203A Chloromethyl chlorosulfate as a voltage delay inhibitor in lithium cells 失效
标题翻译：氯代氯甲烷作为锂电池中的电压延迟抑制剂
公开(公告)号：US5202203A
公开(公告)日：1993-04-13
申请号：US680973
申请日：1991-04-05
申请人： Frank M. Delnick
发明人： Frank M. Delnick
IPC分类号： H01M6/14 , H01M6/16
CPC分类号： H01M6/14 , H01M6/168
摘要： Chloromethyl chlorosulfate (CMCS) is used as a passive film growth inhibitor in electrochemical cells to minimize voltage delay and low-voltage discharge. Film growth on lithium anodes is significantly diminished when CMCS is added to SOCl.sub.2 and SO.sub.2 Cl.sub.2 electrolytes of lithium batteries. The CMCS also has the effect of extending the shelf-life of Li/SOCl.sub.2 and Li/SO.sub.2 Cl.sub.2 batteries.
摘要翻译：氯化甲基氯硫酸盐（CMCS）用作电化学电池中的钝态膜生长抑制剂，以最小化电压延迟和低电压放电。当将CMCS加入锂电池的SOCl 2和SO 2 Cl 2电解质中时，锂阳极上的膜生长显着减少。 CMCS还具有延长Li / SOCl2和Li / SO2Cl2电池的保质期的作用。

7. 发明授权

US07033698B2 Flexible cathodes 有权
标题翻译：柔性阴极
公开(公告)号：US07033698B2
公开(公告)日：2006-04-25
申请号：US10290832
申请日：2002-11-08
申请人： Christopher Boczer , Frank M. Delnick , Rosauro Del Rosario , Minkoo Kang , Lucyna M. Pawlowska , Michael Pozin , Dharmendra Rana , Maya Stevanovic , John J. Weckesser
发明人： Christopher Boczer , Frank M. Delnick , Rosauro Del Rosario , Minkoo Kang , Lucyna M. Pawlowska , Michael Pozin , Dharmendra Rana , Maya Stevanovic , John J. Weckesser
IPC分类号： H01M4/62 , H01M4/50 , H01M4/66 , B05D5/12
CPC分类号： H01M10/0569 , H01M4/0404 , H01M4/0411 , H01M4/131 , H01M4/1391 , H01M4/505 , H01M4/621 , H01M4/622 , H01M4/661 , H01M10/0525 , Y10T29/49108 , Y10T29/49115
摘要： A cathode for a lithium battery is described. The cathode includes: (a) a current collector including aluminum foil; and (b) an active cathode material including: (i) manganese dioxide; (ii) conductive materials; and (iii) a binder selected from the group consisting of linear di- and tri-block polymers, linear tri-block polymers cross-linked with melamine resin, ethylene-propylene copolymers, ethylene-propylene-diene terpolymers, tri-block fluorinated thermoplastics, hydrogenated nitrile rubbers, fluoro-ethylene-vinyl ether copolymers, thermoplastic polyurethanes, thermoplastic olefins, and polyvinylidine fluoride homopolymers.
摘要翻译：描述了用于锂电池的阴极。阴极包括：（a）集电体，包括铝箔; 和（b）活性阴极材料，包括：（i）二氧化锰; （ii）导电材料; 和（iii）选自线性二嵌段和三嵌段聚合物的粘合剂，与三聚氰胺树脂交联的直链三嵌段聚合物，乙烯 - 丙烯共聚物，乙烯 - 丙烯 - 二烯三元共聚物，三嵌段氟化热塑性塑料氢化丁腈橡胶，氟乙烯 - 乙烯基醚共聚物，热塑性聚氨酯，热塑性烯烃和聚偏二氟乙烯均聚物。

8. 发明授权

US06316142B1 Electrode containing a polymeric binder material, method of formation thereof and electrochemical cell 有权
标题翻译：含有聚合物粘合剂材料的电极，其形成方法和电化学电池
公开(公告)号：US06316142B1
公开(公告)日：2001-11-13
申请号：US09281922
申请日：1999-03-31
申请人： Frank M. Delnick , Alan Iwamoto , Zhendong Hu , Liya Wang
发明人： Frank M. Delnick , Alan Iwamoto , Zhendong Hu , Liya Wang
IPC分类号： H01M462
CPC分类号： H01M4/622 , H01M4/0404 , H01M4/0435 , H01M4/621 , H01M4/625 , H01M10/052 , H01M10/054 , Y10T29/49112 , Y10T29/49115
摘要： Provided are methods of forming an electrode suitable for use in an electrochemical cell, and novel electrodes which can be formed therefrom. The methods involve the steps of: (a) forming an electrode slurry from components comprising a solvent, a polymeric binder material and a solid electrode material, wherein the polymeric binder material is formed by modifying a polyolefin with at least one unsaturated polycarboxylic acid or an anhydride of the acid, chlorinating the modified polyolefin and partially crosslinking carboxyl groups or acid anhydride groups on the chlorinated, modified polyolefin with an epoxy group of a compound which has at least two epoxy groups per molecule; (b) coating the electrode slurry on a substrate; and (c) evaporating the solvent. Also provided are electrochemical cells which include the inventive electrodes. The invention has particular applicability to the manufacture of nonaqueous electrochemical power supplies.
摘要翻译：提供了形成适用于电化学电池的电极的方法，以及可由其形成的新型电极。所述方法包括以下步骤：（a）从包括溶剂，聚合物粘合剂材料和固体电极材料的组分形成电极浆料，其中所述聚合物粘合剂材料通过用至少一种不饱和多元羧酸或酸的酸酐，氯化改性聚烯烃和氯化改性聚烯烃部分交联的羧基或酸酐基团，其中每个分子具有至少两个环氧基团的化合物的环氧基团; （b）将电极浆料涂覆在基材上; 和（c）蒸发溶剂。还提供了包括本发明电极的电化学电池。本发明特别适用于非水电化学电源的制造。

9. 发明授权

US5882721A Process of manufacturing porous separator for electrochemical power supply 失效
标题翻译：制造电化学电源多孔隔板的工艺
公开(公告)号：US5882721A
公开(公告)日：1999-03-16
申请号：US847098
申请日：1997-05-01
申请人： Frank M. Delnick
发明人： Frank M. Delnick
IPC分类号： H01G9/02 , H01M2/16 , H01M4/02 , H01M6/02 , H01M8/02 , H01M10/40 , B05D5/12 , H01M6/14
CPC分类号： H01M8/0293 , H01G11/52 , H01G11/84 , H01M2/164 , H01M2/1646 , H01M2/1673 , Y02E60/13 , Y02P70/54 , Y02P70/56
摘要： A method of forming a porous composite separator layer for an electrochemical cell comprising the steps of printing a thin layer of a separator precursor solution on the surface of one of the electrochemical cell electrodes, curing the thin layer of separator precursor solution so that it transforms into a microporous composite separator structure. In the preferred embodiment, the separator precursor solution is formulated as an ink comprising a silica aerogel filler material dispersed in a solution of polymer binder which is dissolved in a suitable solvent. The process allows the manufacture of thin and flexible composite separators which are conformally bonded to the underlying electrodes.
摘要翻译：一种形成用于电化学电池的多孔复合隔离层的方法，包括以下步骤：在一个电化学电池电极的表面上印刷隔板前体溶液的薄层，固化隔膜前体溶液的薄层，使其转变成微孔复合隔板结构。在优选的实施方案中，分离器前体溶液配制成包含分散在溶解在合适溶剂中的聚合物粘合剂溶液中的二氧化硅气凝胶填料的油墨。该方法允许制造薄且柔性的复合分离器，其被共形结合到下面的电极。

10. 发明授权

US5510212A Structural micro-porous carbon anode for rechargeable lithium ion batteries 失效
标题翻译：可再充电锂离子电池的结构微孔碳阳极
公开(公告)号：US5510212A
公开(公告)日：1996-04-23
申请号：US350281
申请日：1994-12-02
申请人： Frank M. Delnick , Narayan Doddapaneni , Robert R. Lagasse , Ronald F. Simandl , D. Gerald Glasgow , Alan Sylwester
发明人： Frank M. Delnick , Narayan Doddapaneni , Robert R. Lagasse , Ronald F. Simandl , D. Gerald Glasgow , Alan Sylwester
IPC分类号： H01M4/58 , H01M6/16 , H01M4/36
CPC分类号： H01M10/05 , H01M4/587 , H01M6/164 , H01M6/166
摘要： A secondary battery having a rechargeable lithium-containing anode, a cathode, and a separator positioned between the cathode and anode with an organic electrolyte solution absorbed therein is provided. The anode comprises three-dimensional microporous carbon structures synthesized by the controlled pyrolysis of gel derived polymer foam precursors. The gradual heating process in the carbonization of pretreated foam precursors stabilizes the pore structures in the pretreated foam.
摘要翻译：提供了具有可再充电的含锂阳极，阴极和位于阴极和阳极之间并且吸收有机电解质溶液的隔膜的二次电池。阳极包括通过凝胶衍生的聚合物泡沫前体的受控热解合成的三维微孔碳结构。预处理的泡沫前体的碳化中的逐渐加热过程稳定了预处理泡沫体中的孔结构。

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