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1. 发明申请

US20170368537A1 ITQ-49 MATERIAL, METHOD FOR THE PRODUCTION THEREOF AND USE OF SAME 审中-公开
公开(公告)号：US20170368537A1
公开(公告)日：2017-12-28
申请号：US15678636
申请日：2017-08-16
申请人： Avelino COMA CANOS , Fernando REY GARCIA , Manuel HERNANDEZ RODRIGUEZ , Jose Luis JORDA MORET
发明人： Avelino COMA CANOS , Fernando REY GARCIA , Manuel HERNANDEZ RODRIGUEZ , Jose Luis JORDA MORET
IPC分类号： B01J29/04 , C07C1/22 , C01B39/54 , C01B39/48 , B01D53/86 , B01J35/00 , B01D53/04 , B01J20/30 , B01J20/10 , B01J29/70 , C10G73/02 , C01B37/00
CPC分类号： B01J29/047 , B01D53/0407 , B01D53/8628 , B01D53/9418 , B01D2253/108 , B01D2255/50 , B01J20/10 , B01J20/3078 , B01J29/70 , B01J35/002 , C01B37/005 , C01B39/48 , C01B39/54 , C07C1/22 , C10G73/02
摘要： The present invention refers to a microporous crystalline material, to the method for the production thereof and to the use of same, the material having a composition: xX2O3:zZO2:yYO2 in which: X is a trivalent element such as Al, B, Fe, In, Ga, Cr, or mixtures thereof, where (y+z)/x can have values of between 9 and infinity; Z corresponds to a tetravalent element selected from Si, Ge or mixtures thereof; and Y corresponds to a tetravalent element such as Ti, Sn, Zr, V or mixtures thereof, where z/y can have values of between 10 and infinity.

2. 发明申请

US20160008753A1 Separation and Storage of Fluids Using ITQ-55 有权
标题翻译：使用ITQ-55分离和储存液体
公开(公告)号：US20160008753A1
公开(公告)日：2016-01-14
申请号：US14744485
申请日：2015-06-19
申请人： Edward W. Corcoran, JR. , Pavel Kortunov , Charanjit S. Paur , Peter I. Ravikovitch , Jade Yu Wang , Avelino Corma Canos , Fernando Rey Garcia , Susana Valencia Valencia , Angel Cantín Sanz , Miguel Palomino Roca
发明人： Edward W. Corcoran, JR. , Pavel Kortunov , Charanjit S. Paur , Peter I. Ravikovitch , Jade Yu Wang , Avelino Corma Canos , Fernando Rey Garcia , Susana Valencia Valencia , Angel Cantín Sanz , Miguel Palomino Roca
IPC分类号： B01D53/04 , B01D53/047 , B01J20/18
CPC分类号： C01B39/48 , B01D53/02 , B01D53/04 , B01D53/0407 , B01D53/0462 , B01D53/047 , B01D53/228 , B01D53/229 , B01D71/028 , B01D2253/108 , B01D2256/10 , B01D2256/12 , B01D2256/16 , B01D2256/18 , B01D2256/20 , B01D2256/22 , B01D2256/24 , B01D2256/245 , B01D2256/26 , B01D2257/302 , B01D2257/304 , B01D2257/40 , B01D2257/404 , B01D2257/406 , B01D2257/50 , B01D2257/504 , B01D2257/70 , B01D2257/702 , B01D2257/7022 , B01D2257/80 , B01J20/18 , B01J20/3078 , B01J29/70 , B01J29/86 , B01J29/89 , C01B3/508 , C01B17/167 , C01B21/0466 , C01B37/002 , C01B37/007 , C01B37/02 , C01B39/06 , C01B39/08 , C01B39/12 , C01B2203/0405 , C01B2210/0018 , C01C1/12 , C07C1/20 , C07C1/322 , C07C2/76 , C07C29/00 , C07C41/01 , C07C2529/70 , C07C2529/76 , C07C2529/78 , Y02C10/08
摘要： This invention refers to a microporous crystalline material of zeolitic nature that has, in its calcined state and in the absence of defects in its crystalline matrix manifested by the presence of silanols, the empirical formula x(M1/nXO2):yYO2:gGeO2:(1−g)SiO2 in which M is selected between H+, at least one inorganic cation of charge +n, and a mixture of both, X is at least one chemical element of oxidation state +3, Y is at least one chemical element with oxidation state +4 different from Si, x takes a value between 0 and 0.2, both included, y takes a value between 0 and 0.1, both included, g takes a value between 0 and 0.5, both included that has been denoted ITQ-55, as well as a method for its preparation. This invention also relates to uses of the crystalline material of zeolitic nature for adsorption of fluid components, membrane separation of fluid components, storage of fluid components, and catalysis of various conversion reactions.
摘要翻译：本发明涉及沸石性质的微孔结晶材料，其经煅烧状态并且在不存在硅烷醇存在下的结晶基质缺陷的情况下，经验式x（M1 / nXO2）：yYO2：gGeO2 :( 1-g）SiO 2，其中M选自H +，至少一种电荷无机阳离子+ n和两者的混合物，X是至少一种氧化态的化学元素+3，Y是至少一种具有氧化态+4不同于Si，x取值在0和0.2之间，均包括在内，y取0到0.1之间的值，均包括在内，g取0至0.5之间的值，这两者都包含在ITQ-55中，以及其制备方法。本发明还涉及沸石性质的结晶材料用于吸附流体组分，流体组分的膜分离，储存流体组分以及催化各种转化反应的用途。

3. 发明申请

US20120067216A1 USE OF A MICROPOROUS CRYSTALLINE MATERIAL OF ZEOLITIC NATURE WITH RHO STRUCTURE IN NATURAL GAS PROCESSING 有权
标题翻译：在天然气加工中使用具有RHO结构的微生物自然材料的微波晶体材料
公开(公告)号：US20120067216A1
公开(公告)日：2012-03-22
申请号：US13272586
申请日：2011-10-13
申请人： Avelino CORMA CANOS , Miguel Palomino Roca , Fernando Rey Garcia , Susana Valencia Valencia
发明人： Avelino CORMA CANOS , Miguel Palomino Roca , Fernando Rey Garcia , Susana Valencia Valencia
IPC分类号： B01D53/02
CPC分类号： C10L3/10 , B01D53/04 , B01D2253/108 , B01D2256/24 , B01D2257/102 , B01D2257/504 , B01J20/18 , C01B39/48 , C10L3/102 , C10L3/104 , Y02C10/08 , Y02P20/152
摘要： The present invention describes the use of isostructural zeolites with rho zeolitic structure in processes of adsorption and separation of the various components of natural gas.
摘要翻译：本发明描述了在天然气各种成分的吸附和分离过程中使用具有rho沸石结构的异构沸石。

4. 发明申请

US20090202416A1 Separation of Fluids Using Zeolite Itq-32 失效
标题翻译：使用沸石Itq-32分离液体
公开(公告)号：US20090202416A1
公开(公告)日：2009-08-13
申请号：US11989330
申请日：2006-07-24
申请人： Avelino Corma Canos , Fernando Rey Garcia , Susana Valencia Valencia
发明人： Avelino Corma Canos , Fernando Rey Garcia , Susana Valencia Valencia
IPC分类号： B01D15/04 , C07C7/12 , B01D53/02 , C07C7/144 , C01B21/04
CPC分类号： C07C7/13 , B01D15/00 , B01D53/02 , B01D53/04 , B01D53/047 , B01D2253/108 , B01D2253/308 , B01D2256/10 , B01D2256/24 , B01D2257/702 , B01J20/18 , C01B39/48 , C10G25/03 , C10G53/08 , C10G2300/1081 , C10G2300/1092 , C10G2300/805 , C10G2400/20 , C10L3/10 , C10L3/102 , C10L3/12
摘要： The invention relates to a method of separating fluids from mixtures using a zeolite known as ITQ-32 consisting of a two-dimensional pore system comprising channels with openings formed by 8 tetrahedra which are interconnected by channels with openings formed by 12 tetrahedra. The inventive method comprises at least the following steps: a) the zeolite ITQ-32 material is brought into contact with the mixture of fluids, b) one or more of the components are adsorbed in the zeolite ITQ-32 material, c) the non-adsorbed components are extracted, and d) one or more of the components adsorbed in the zeolite ITQ-32 material are recovered.
摘要翻译：本发明涉及一种使用称为ITQ-32的沸石从混合物中分离流体的方法，所述沸石由二维孔隙系统组成，该二维孔隙系统包括由8面四面体形成的开口的通道，该通道由通过由12面四面体形成的开口的通道相互连接。本发明的方法至少包括以下步骤：a）使沸石ITQ-32材料与流体混合物接触，b）一种或多种组分被吸附在沸石ITQ-32材料中，c） - 吸附的组分被提取，并且d）吸收在沸石ITQ-32材料中的一种或多种组分被回收。

5. 发明申请

US20090068092A1 Microporous Crystalline Zeolite Material, Zeolite ITQ-32, Preparation Method Thereof and Use of Same 失效
标题翻译：微孔结晶沸石材料，沸石ITQ-32，其制备方法及其用途
公开(公告)号：US20090068092A1
公开(公告)日：2009-03-12
申请号：US11883354
申请日：2006-01-26
申请人： Avelino Corma Canos , Angel Cantin Sanz , Fernando Rey Garcia , Susana Valencia Valencia , Sandra Leiva Herrero
发明人： Avelino Corma Canos , Angel Cantin Sanz , Fernando Rey Garcia , Susana Valencia Valencia , Sandra Leiva Herrero
IPC分类号： C01B39/02 , C01B39/04
CPC分类号： C01B37/02 , B01J20/18 , B01J29/70 , C01B39/06 , C01B39/065 , C01B39/082 , C01B39/12 , C01B39/48
摘要： The invention relates to a microporous crystalline zeolite material which, in the calcined state and in the absence of defects in the crystalline lattice thereof, manifested by the presence of silanols, has empirical formula x(M1/nXO2):y YO2:SiO2, in which M is selected from among H+, at least one inorganic cation with charge +n and a mixture of both; X is at least one chemical element in oxidation state +3; Y is at least one chemical element in oxidation state +4, which is different from Si, x has a value of between 0 and 0.2 inclusive, and y has a value of between 0 and 0.1 inclusive. In addition, as it is synthesised, and in the calcined state, the material has a characteristic X-ray diffraction pattern known as ITQ-32. The invention also relates to the method of preparing said material and to the use thereof.
摘要翻译：本发明涉及一种微孔结晶沸石材料，其在煅烧状态下并且不存在其晶格缺陷的缺陷，通过硅烷醇的存在表现出具有经验式x（M1 / nXO2）：y YO2：SiO2，其中M选自H +，至少一种带电荷的无机阳离子和两者的混合物; X是至少一种氧化态的化学元素+3; Y是氧化态+4中的至少一种化学元素，其与Si不同，x具有在0和0.2之间的值，包括0和0.2之间，y的值在0和0.1之间。此外，如合成，并且在煅烧状态下，该材料具有称为ITQ-32的特征X射线衍射图。本发明还涉及制备所述材料的方法及其用途。

6. 发明授权

US10427140B2 ITQ-49 material, method for the production thereof and use of same 有权
公开(公告)号：US10427140B2
公开(公告)日：2019-10-01
申请号：US15678636
申请日：2017-08-16
申请人： Avelino Corma Canos , Fernando Rey Garcia , Manuel Hernandez Rodriguez , Jose Luis Jorda Moret
发明人： Avelino Corma Canos , Fernando Rey Garcia , Manuel Hernandez Rodriguez , Jose Luis Jorda Moret
IPC分类号： B01J20/10 , B01J29/70 , C01B39/48 , B01D53/86 , C07C1/22 , B01J29/04 , B01J35/00 , B01D53/04 , B01J20/30 , C10G73/02 , C01B37/00 , C01B39/54 , B01D53/94
摘要： The present invention refers to a microporous crystalline material, to the method for the production thereof and to the use of same, the material having a composition: xX2O3:zZO2:yYO2 in which: X is a trivalent element such as Al, B, Fe, In, Ga, Cr, or mixtures thereof, where (y+z)/x can have values of between 9 and infinity; Z corresponds to a tetravalent element selected from Si, Ge or mixtures thereof; and Y corresponds to a tetravalent element such as Ti, Sn, Zr, V or mixtures thereof, where z/y can have values of between 10 and infinity.

7. 发明授权

US08337594B2 Use of a microporous crystalline material of zeolitic nature with RHO structure in natural gas processing 有权
标题翻译：在天然气加工中使用具有RHO结构的沸石性质的微孔结晶材料
公开(公告)号：US08337594B2
公开(公告)日：2012-12-25
申请号：US13272586
申请日：2011-10-13
申请人： Avelino Corma Canos , Miguel Palomino Roca , Fernando Rey Garcia , Susana Valencia Valencia
发明人： Avelino Corma Canos , Miguel Palomino Roca , Fernando Rey Garcia , Susana Valencia Valencia
IPC分类号： B01D53/02
CPC分类号： C10L3/10 , B01D53/04 , B01D2253/108 , B01D2256/24 , B01D2257/102 , B01D2257/504 , B01J20/18 , C01B39/48 , C10L3/102 , C10L3/104 , Y02C10/08 , Y02P20/152
摘要： The present invention describes the use of isostructural zeolites with rho zeolitic structure in processes of adsorption and separation of the various components of natural gas.
摘要翻译：本发明描述了在天然气各种成分的吸附和分离过程中使用具有rho沸石结构的异构沸石。

8. 发明授权

US08226925B2 Microporous crystalline material of zeolitic nature, zeolite ITQ-39, method of preparation and uses 有权
标题翻译：沸石性质的微孔结晶材料，沸石ITQ-39，制备方法和用途
公开(公告)号：US08226925B2
公开(公告)日：2012-07-24
申请号：US12525506
申请日：2008-01-31
申请人： Avelino Corma Canos , Manuel Moliner Marin , Fernando Rey Garcia , Jorge Gonzalez Gonzalez
发明人： Avelino Corma Canos , Manuel Moliner Marin , Fernando Rey Garcia , Jorge Gonzalez Gonzalez
IPC分类号： C01B39/46 , C01B39/48
CPC分类号： B01J29/70 , B01J20/18 , C01B39/48
摘要： Described herein are zeolite microporous crystalline materials comprising, in the heated state and in the absence of defects in its crystalline framework manifested by the presence of silanols, the empirical formula: x(M1/nXO2):yYO2:SiO2, wherein M is selected from H+, an inorganic cation of charge +n, and mixtures thereof, X is at least one chemical element having an oxidation state of +3, Y is at least one second chemical element other than Si having an oxidation state +4, x has a value between 0 and about 0.3, y has a value between 0 and about 0.1, and wherein the synthesized material has an X-ray diffraction pattern having at least values of angle 2θ (degrees) and relative intensities (I/I0) described. Process of making the microporous crystalline materials are also disclosed.
摘要翻译：本文描述的是沸石微孔结晶材料，其包括在加热状态下，在不存在由硅烷醇存在的结晶框架中缺陷的情况下，经验式：x（M1 / nXO2）：yYO2：SiO2，其中M选自 H +，电荷无机阳离子+ n及其混合物，X是氧化态为+3的至少一种化学元素，Y是具有氧化态+4以外的除了Si以外的至少一种第二化学元素，x具有值在0和约0.3之间，y具有在0和约0.1之间的值，并且其中合成材料具有至少具有角度2的角度的X射线衍射图案; （度）和相对强度（I / I0）。还公开了制备微孔结晶材料的方法。

9. 发明授权

US08187469B2 Separation of fluids using zeolite ITQ-32 失效
标题翻译：使用沸石ITQ-32分离流体
公开(公告)号：US08187469B2
公开(公告)日：2012-05-29
申请号：US11989330
申请日：2006-07-24
申请人： Avelino Corma Canos , Fernando Rey Garcia , Susana Valencia Valencia
发明人： Avelino Corma Canos , Fernando Rey Garcia , Susana Valencia Valencia
IPC分类号： B01D15/00 , B01D15/04 , B01D53/22 , B01D59/12 , B01D53/02 , B01D59/26 , B01D47/00 , B01D53/14 , B01J39/00 , B01J49/00 , C02F1/42 , C02F1/28 , C07C7/144 , C01B33/36 , C07C7/12 , C01B39/00 , C01B21/00 , C01F7/00
CPC分类号： C07C7/13 , B01D15/00 , B01D53/02 , B01D53/04 , B01D53/047 , B01D2253/108 , B01D2253/308 , B01D2256/10 , B01D2256/24 , B01D2257/702 , B01J20/18 , C01B39/48 , C10G25/03 , C10G53/08 , C10G2300/1081 , C10G2300/1092 , C10G2300/805 , C10G2400/20 , C10L3/10 , C10L3/102 , C10L3/12
摘要： The invention relates to a method of separating fluids from mixtures using a zeolite known as ITQ-32 consisting of a two-dimensional pore system comprising channels with openings formed by 8 tetrahedra which are interconnected by channels with openings formed by 12 tetrahedra. The inventive method comprises at least the following steps: a) the zeolite ITQ-32 material is brought into contact with the mixture of fluids, b) one or more of the components are adsorbed in the zeolite ITQ-32 material, c) the non-adsorbed components are extracted, and d) one or more of the components adsorbed in the zeolite ITQ-32 material are recovered.
摘要翻译：本发明涉及一种使用称为ITQ-32的沸石从混合物中分离流体的方法，所述沸石由二维孔隙系统组成，该二维孔隙系统包括由8面四面体形成的开口的通道，该通道由通过由12面四面体形成的开口的通道相互连接。本发明的方法至少包括以下步骤：a）使沸石ITQ-32材料与流体混合物接触，b）一种或多种组分被吸附在沸石ITQ-32材料中，c） - 吸附的组分被提取，并且d）吸收在沸石ITQ-32材料中的一种或多种组分被回收。

10. 发明授权

US06211388B1 Method for producing propylene oxide 失效
标题翻译：生产环氧丙烷的方法
公开(公告)号：US06211388B1
公开(公告)日：2001-04-03
申请号：US09414555
申请日：1999-10-08
申请人： Junpei Tsuji , Jun Yamamoto , Avelino Corma Canos , Fernando Rey Garcia
发明人： Junpei Tsuji , Jun Yamamoto , Avelino Corma Canos , Fernando Rey Garcia
IPC分类号： C07D30112
CPC分类号： C07D301/19 , B01J29/89 , B01J35/002 , B01J35/1038 , B01J35/1042 , B01J35/1047 , B01J35/1057 , B01J35/1061 , B01J35/1076 , B01J35/108 , Y02P20/52
摘要： A method for producing propylene oxide by reacting propylene with ethylbenzene hydroperoxide, wherein the reaction is conducted in the presence of a catalyst comprising a titanium-containing silicon oxide and satisfying all of the following conditions (1) to (6): (1) there is at least one peak showing a interplanar spacing (d) larger than 18 Å in X-ray diffraction; (2) an average pore size is 10 Å or more; (3) a pore size of 90% or more of the total pore volume is 5 to 200 Å; (4) a specific pore volume is 0.2 cm3/g or more; (5) a quaternary ammonium ion represented by the following general formula (I) is used as a template and then said template is removed by calcination operation: [NR1R2R3R4]+ (I) wherein R1 represents a linear or branched hydrocarbon chain having 2 to 36 carbon atoms, and R2 to R4 represent an alkyl group having 1 to 6 carbon atoms; and (6) The catalyst has been subjected to silylation treatment.
摘要翻译：一种通过丙烯与氢过氧化苯反应生产环氧丙烷的方法，其中反应在包含含钛氧化硅的催化剂存在下进行，并满足以下所有条件（1）至（6）：（1）是在X射线衍射中显示出大于18的晶面间距（d）的至少一个峰;（2）平均孔径为10埃以上;（3）总孔径的90％以上的孔径体积为5〜200;（4）比孔体积为0.2cm 3 / g以上;（5）以下述通式（I）表示的季铵离子作为模板，将所述模板用煅烧操作：其中R1表示具有2至36个碳原子的直链或支链烃链，R 2至R 4表示具有1至6个碳原子的烷基; 和（6）催化剂已进行甲硅烷基化处理。

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