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1. 发明授权

US4565649A Graphite intercalation compounds 失效
标题翻译：石墨插层化合物
公开(公告)号：US4565649A
公开(公告)日：1986-01-21
申请号：US635940
申请日：1984-07-30
申请人： F. Lincoln Vogel
发明人： F. Lincoln Vogel
IPC分类号： D01F11/12 , H01B1/00 , H01B1/04
CPC分类号： D01F11/121 , D01F11/12 , H01B1/00 , H01B1/04
摘要： An electrically conductive composition is disclosed which comprises a graphite intercalation compound of graphite, a Bronsted acid such as hydrogen fluoride, chloride, or bromide, nitric, nitrous, sulfuric or perchloric acid, and a metal halide selected from boron trihalide, a pentahalide of a metal from Group V of the Periodic Table, a tetrahalide of a metal from Group IV of the Periodic Table and mixtures thereof.
摘要翻译：公开了一种导电组合物，其包括石墨的石墨插层化合物，诸如氟化氢，氯化物或溴化物的布朗斯台德酸，硝酸，亚硝酸，硫酸或高氯酸，以及金属卤化物，其选自三卤化硼，五卤化硼周期表第Ⅴ族金属，元素周期表第Ⅳ族金属的四卤化物及其混合物。

2. 发明授权

US4293450A Process for conducting electricity utilizing a specifically defined graphite intercalation compound 失效
标题翻译：使用特定石墨插层化合物进行电力的方法
公开(公告)号：US4293450A
公开(公告)日：1981-10-06
申请号：US897443
申请日：1978-04-18
申请人： F. Lincoln Vogel
发明人： F. Lincoln Vogel
IPC分类号： C01B31/00 , C04B35/536 , D01F11/12 , H01B1/04
CPC分类号： H01B1/04 , C01B31/0415 , C04B35/536 , D01F11/127
摘要： An electrically conductive composition is provided which comprises an intercalation compound of (1) graphite, (2) fluorosulfonic acid, chlorosulfonic acid, or mixtures thereof, and (3) a boron trihalide, a tetrahalide of a Group IV element, a pentahalide of a Group V element, or mixtures thereof. The graphite may be in any one of a variety of physical configurations, e.g. as particulate crystals or present in a carbonaceous fibrous material, at the time of the intercalation reaction. The resulting graphite intercalation compound possesses advantageous electrical conductivity characteristics not possessed by plain graphite and is capable of utilization as a light weight electrical conductor. The graphite intercalation compound may optionally be provided within a metal matrix (e.g. within elemental copper) to form an electrically conductive composite article.
摘要翻译：提供一种导电组合物，其包含（1）石墨，（2）氟磺酸，氯磺酸或其混合物的嵌入化合物，和（3）三卤化硼，IV族元素的四卤化物， V族元素或其混合物。石墨可以是各种物理构型中的任何一种，例如，作为颗粒状晶体或存在于碳质纤维材料中时，在插层反应时。所得到的石墨插层化合物具有普通石墨不具有的有利的导电特性，并且能够用作轻质电导体。石墨插层化合物可以任选地在金属基质（例如在元素铜内）提供以形成导电复合材料制品。

3. 发明授权

US4414142A Organic matrix composites reinforced with intercalated graphite 失效
标题翻译：有机基质复合材料用插层石墨增强
公开(公告)号：US4414142A
公开(公告)日：1983-11-08
申请号：US323560
申请日：1981-11-20
申请人： F. Lincoln Vogel , Claude Zeller
发明人： F. Lincoln Vogel , Claude Zeller
IPC分类号： C08K3/04 , C08K9/02 , H01B1/24 , H01B1/04
CPC分类号： C08K9/02 , C08K3/04 , H01B1/24
摘要： The incorporation of intercalated carbon/graphite in any of its forms such as powder, flake or fiber into an organic matrix results in a high strength, light weight composite with an electrical conductivity considerably higher than a similar product made with nonintercalated graphite. A great variety of organic polymers may be used, such as epoxy, thermoplastics and thermoset resins. Depending on the form of the intercalated graphite, fabrication techniques of extrusion, lay-up, injection molding and pressing can be employed to fabricate the parts from these composites. A wide spectrum of properties is available from this type of composite in terms of strength and conductivity which will be useful for such widely ranging applications as aircraft structures and shielding for electronic equipment.
摘要翻译：将其中任何形式（例如粉末，薄片或纤维）中的嵌入碳/石墨掺入有机基质中导致高强度，重量轻的复合材料，导电率显着高于用非插层石墨制成的类似产品。可以使用各种有机聚合物，例如环氧树脂，热塑性塑料和热固性树脂。取决于插层石墨的形式，可以采用挤出，铺层，注塑和压制的制造技术来制造这些复合材料的零件。从这种类型的复合材料在强度和导电性方面可以获得广泛的性能，这对于诸如飞机结构和用于电子设备的屏蔽的广泛应用是有用的。

4. 发明授权

US5352430A Method of manufacturing intercalation compounds 失效
标题翻译：插层化合物的制备方法
公开(公告)号：US5352430A
公开(公告)日：1994-10-04
申请号：US914513
申请日：1992-07-17
申请人： Timothy J. McCulfor , F. Lincoln Vogel
发明人： Timothy J. McCulfor , F. Lincoln Vogel
IPC分类号： B01J8/24 , C01B21/064 , C01B31/00 , C01B31/04 , C01G39/06
CPC分类号： C01B21/064 , C01B31/0415
摘要： A method of manufacturing an intercalation compound, such as a graphite intercalation compound, in a fluidized bed reactor. The intercalation compound comprises a host material, like graphite, and an intercalant and is essentially free of excess intercalant.
摘要翻译：在流化床反应器中制造插层化合物如石墨插层化合物的方法。嵌入化合物包括主体材料，如石墨和插入剂，并且基本上不含过量的插入剂。

5. 发明授权

US4461719A Lamellar carbon-nitrosyl or nitronium salt compositions 失效
标题翻译：层状碳 - 亚硝酰基或硝酸盐组合物
公开(公告)号：US4461719A
公开(公告)日：1984-07-24
申请号：US475368
申请日：1983-03-14
申请人： F. Lincoln Vogel , William C. Forsman
发明人： F. Lincoln Vogel , William C. Forsman
IPC分类号： D01F11/12 , H01B1/04 , H01B1/18 , H01B1/24
CPC分类号： D01F11/12 , H01B1/04 , H01B1/18 , H01B1/24
摘要： Electrically conductive carbon compositions are disclosed which are formed from carbon having a graphite-like structure and a nitrosyl or nitronium salt or salts. The nitrosyl or nitronium salt reacts with the carbon to intercalate it with charge-exchange atoms or molecules. Binary, ternary and multi-intercalated lamellar compositions are produced according to the particular reaction process selected. The compositions may be used alone as electrical conductors or may be combined in a matrix to form composite conductors.
摘要翻译：公开了导电碳组合物，其由具有石墨状结构的碳和亚硝酰基或硝鎓盐或盐形成。亚硝酰基或硝酸盐与碳反应以将其与电荷交换原子或分子嵌入其中。根据所选择的特定反应过程制备二元，三元和多嵌层的层状组合物。组合物可以单独用作电导体，或者可以组合在基质中以形成复合导体。

6. 发明授权

US4382882A Lamellar carbon-nitrosyl or nitronium salt compositions 失效
标题翻译：层状碳 - 亚硝酰基或硝酸盐组合物
公开(公告)号：US4382882A
公开(公告)日：1983-05-10
申请号：US221013
申请日：1980-12-29
申请人： F. Lincoln Vogel , William C. Forsman
发明人： F. Lincoln Vogel , William C. Forsman
IPC分类号： D01F11/12 , H01B1/04 , H01B1/18 , H01B1/24
CPC分类号： D01F11/12 , H01B1/04 , H01B1/18 , H01B1/24
摘要： Electrically conductive carbon compositions are disclosed which are formed from carbon having a graphite-like structure and a nitrosyl or nitronium salt or salts. The nitrosyl or nitronium salt reacts with the carbon to intercalate it with charge-exchange atoms or molecules. Binary, ternary and multi-intercalated lamellar compositions are produced according to the particular reaction process selected. The compositions may be used alone as electrical conductors or may be combined in a matrix to form composite conductors.
摘要翻译：公开了导电碳组合物，其由具有石墨状结构的碳和亚硝酰基或硝鎓盐或盐形成。亚硝酰基或硝酸盐与碳反应以将其与电荷交换原子或分子嵌入其中。根据所选择的特定反应过程制备二元，三元和多嵌层的层状组合物。组合物可以单独用作电导体，或者可以组合在基质中以形成复合导体。

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