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    • 1. 发明申请
    • RAPID SAMPLE EXCHANGE FOR MINIATURIZED NMR SPECTROMETER
    • 用于微型NMR光谱仪的快速样品交换器
    • US20110316536A1
    • 2011-12-29
    • US13171230
    • 2011-06-28
    • John C. PriceCharles MillerErick Winston
    • John C. PriceCharles MillerErick Winston
    • G01R33/44
    • G01R33/307G01R33/302G01R33/445
    • A method is provided for acquiring multiple NMR response signal data in rapid succession for averaging NMR spectral data from a sample. The fluid sample is placed in a capillary that extends through the magnetic field of the NMR spectrometer, including through the center of the magnetic field to place a segment of the sample in the magnetic center. After the sample fluid, initially magnetized by the magnetic field, is activated to emit an NMR pulse signal, the fluid in the capillary is advanced rapidly to put another pre-magnetized segment of the sample fluid in the fluid center, acquiring an NRM pulse signal, and continuing the cycle until a desired number of NMR response data signals from the sample have been acquired. Those response data from multiple acquisitions are then averaged.
    • 提供一种快速连续获取多个NMR响应信号数据的方法,用于对来自样品的NMR光谱数据进行平均。 将流体样品置于穿过NMR光谱仪的磁场的毛细管中,包括通过磁场的中心,将样品的一段放置在磁性中心。 在初始被磁场磁化的样品流体被激活以发射NMR脉冲信号之后,毛细管中的流体被快速前进,以将样品流体的另一个预先磁化的区段放在流体中心,获得NRM脉冲信号 并继续循环,直到获得了来自样品的所需数量的NMR响应数据信号。 然后对来自多次获取的响应数据进行平均。
    • 2. 发明授权
    • Rapid sample exchange for miniaturized NMR spectrometer
    • 用于小型化NMR光谱仪的快速样品交换
    • US08754646B2
    • 2014-06-17
    • US13171230
    • 2011-06-28
    • John C. PriceCharles MillerErick Winston
    • John C. PriceCharles MillerErick Winston
    • G01V3/00
    • G01R33/307G01R33/302G01R33/445
    • A method is provided for acquiring multiple NMR response signal data in rapid succession for averaging NMR spectral data from a sample. The fluid sample is placed in a capillary that extends through the magnetic field of the NMR spectrometer, including through the center of the magnetic field to place a segment of the sample in the magnetic center. After the sample fluid, initially magnetized by the magnetic field, is activated to emit an NMR pulse signal, the fluid in the capillary is advanced rapidly to put another pre-magnetized segment of the sample fluid in the fluid center, acquiring an NRM pulse signal, and continuing the cycle until a desired number of NMR response data signals from the sample have been acquired. Those response data from multiple acquisitions are then averaged.
    • 提供一种快速连续获取多个NMR响应信号数据的方法,用于对来自样品的NMR光谱数据进行平均。 将流体样品置于穿过NMR光谱仪的磁场的毛细管中,包括通过磁场的中心,将样品的一段放置在磁性中心。 在初始被磁场磁化的样品流体被激活以发射NMR脉冲信号之后,毛细管中的流体被快速前进,以将样品流体的另一个预先磁化的区段放在流体中心,获得NRM脉冲信号 并继续循环,直到获得了来自样品的所需数量的NMR响应数据信号。 然后对来自多次获取的响应数据进行平均。