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1. 发明申请

WO2011028804A2 SULFUR-CARBON NANOCOMPOSITES AND THEIR APPLICATION AS CATHODE MATERIALS IN LITHIUM-SULFUR BATTERIES 审中-公开
标题翻译：硫 - 碳纳米复合材料及其在锂硫电池中的阴极材料应用
公开(公告)号：WO2011028804A2
公开(公告)日：2011-03-10
申请号：PCT/US2010/047535
申请日：2010-09-01
申请人： UT-BATTELLE, LLC , LIANG, Chengdu , DUDNEY, Nancy J. , HOWE, Jane Y.
发明人： LIANG, Chengdu , DUDNEY, Nancy J. , HOWE, Jane Y.
IPC分类号： H01M4/583 , H01M4/38 , H01M10/0525 , H01M10/0567 , H01M10/0569
CPC分类号： H01M4/5815 , C01B32/342 , H01M4/0402 , H01M4/0416 , H01M4/0471 , H01M4/133 , H01M4/136 , H01M4/1393 , H01M4/1397 , H01M4/362 , H01M4/364 , H01M4/581 , H01M4/587 , H01M4/625 , H01M10/052 , H01M10/0565 , H01M10/0566 , H01M10/0567 , H01M10/0569 , H01M2004/021 , Y02T10/7011
摘要： The invention is directed in a first aspect to a sulfur-carbon composite material comprising: (i) a bimodal porous carbon component containing therein a first mode of pores which are mesopores, and a second mode of pores which are micropores; and (ii) elemental sulfur contained in at least a portion of said micropores. The invention is also directed to the aforesaid sulfur-carbon composite as a layer on a current collector material; a lithium ion battery containing the sulfur-carbon composite in a cathode therein; as well as a method for preparing the sulfur-composite material.
摘要翻译：本发明的第一方面涉及一种硫 - 碳复合材料，其包含：（i）双峰多孔碳组分，其中包含第一模式的中孔孔隙和第二孔隙模式它们是微孔; 和（ii）包含在至少一部分所述微孔中的元素硫。本发明还涉及上述硫 - 碳复合物作为集流体材料上的层; 在其中的阴极中含有硫 - 碳复合物的锂离子电池; 以及制备硫磺复合材料的方法。

2. 发明申请

WO2011028804A3 SULFUR-CARBON NANOCOMPOSITES AND THEIR APPLICATION AS CATHODE MATERIALS IN LITHIUM-SULFUR BATTERIES 审中-公开
标题翻译：硫化碳纳米复合材料及其作为硫酸锂电池阴极材料的应用
公开(公告)号：WO2011028804A3
公开(公告)日：2011-07-21
申请号：PCT/US2010047535
申请日：2010-09-01
申请人： UT BATTELLE LLC , LIANG CHENGDU , DUDNEY NANCY J , HOWE JANE Y
发明人： LIANG CHENGDU , DUDNEY NANCY J , HOWE JANE Y
IPC分类号： H01M4/583 , H01M4/38 , H01M10/0525 , H01M10/0567 , H01M10/0569
CPC分类号： H01M4/5815 , C01B32/342 , H01M4/0402 , H01M4/0416 , H01M4/0471 , H01M4/133 , H01M4/136 , H01M4/1393 , H01M4/1397 , H01M4/362 , H01M4/364 , H01M4/581 , H01M4/587 , H01M4/625 , H01M10/052 , H01M10/0565 , H01M10/0566 , H01M10/0567 , H01M10/0569 , H01M2004/021 , Y02T10/7011
摘要： The invention is directed in a first aspect to a sulfur-carbon composite material comprising: (i) a bimodal porous carbon component containing therein a first mode of pores which are mesopores, and a second mode of pores which are micropores; and (ii) elemental sulfur contained in at least a portion of said micropores. The invention is also directed to the aforesaid sulfur-carbon composite as a layer on a current collector material; a lithium ion battery containing the sulfur-carbon composite in a cathode therein; as well as a method for preparing the sulfur-composite material.
摘要翻译：本发明的第一方面涉及一种硫 - 碳复合材料，包括：（i）双峰多孔碳组分，其中含有作为中孔的第一模式孔，和第二孔是微孔; 和（ii）至少部分所述微孔中所含的元素硫。本发明还涉及上述硫 - 碳复合材料作为集电体材料上的层; 在其中的阴极中含有硫 - 碳复合材料的锂离子电池; 以及制备硫 - 复合材料的方法。

3. 发明申请

WO2021025970A1 IONICALLY CONDUCTIVE POWDERS AND FILMS, AND METHODS OF PREPARATION 审中-公开
公开(公告)号：WO2021025970A1
公开(公告)日：2021-02-11
申请号：PCT/US2020/044382
申请日：2020-07-31
申请人： UT-BATTELLE, LLC , KERCHER, Andrew K. , WESTOVER, Andrew S. , ABDELMALAK, Michael Naguib , DUDNEY, Nancy J.
发明人： KERCHER, Andrew K. , WESTOVER, Andrew S. , ABDELMALAK, Michael Naguib , DUDNEY, Nancy J.
IPC分类号： H01M10/0525 , H01M4/36 , H01M10/052 , H01M10/0562
摘要： A solid ionically conductive composition (e.g., nanoparticles of less than 1 micron or a continuous film) comprising at least one element selected from alkali metal, alkaline earth metal, aluminum, zinc, copper, and silver in combination with at least two elements selected from oxygen, sulfur, silicon, phosphorus, nitrogen, boron, gallium, indium, tin, germanium, arsenic, antimony, bismuth, transition metals, and lanthanides. Also described is a battery comprising an anode, a cathode, and a solid electrolyte (corresponding to the above ionically conductive composition) in contact with or as part of the anode and/or cathode. Further described is a thermal (e.g., plasma-based) method of producing the ionically conductive composition. Further described is a method for using an additive manufacturing (AM) process to produce an object constructed of the ionically conductive composition by use of particles of the ionically conductive composition as a feed material in the AM process.

4. 发明申请

WO2012044678A2 A HIGH ENERGY DENSITY ALUMINUM BATTERY 审中-公开
标题翻译：高能量密度铝电池
公开(公告)号：WO2012044678A2
公开(公告)日：2012-04-05
申请号：PCT/US2011/053667
申请日：2011-09-28
申请人： UT-BATTELE, LLC , BROWN, Gilbert, M. , PARANTHAMAN, Mariappan, Parans , DAI, Sheng , DUDNEY, Nancy, J. , MANTHIRAM, Arumugan , MCINTYRE, Timothy , SUN, Xiago-guang , LIU, Hansan
发明人： BROWN, Gilbert, M. , PARANTHAMAN, Mariappan, Parans , DAI, Sheng , DUDNEY, Nancy, J. , MANTHIRAM, Arumugan , MCINTYRE, Timothy , SUN, Xiago-guang , LIU, Hansan
IPC分类号： H01M10/05 , H01M4/38 , H01M6/16 , H01M10/052 , H01M10/0564
CPC分类号： H01M10/054 , H01M4/38 , H01M4/463 , H01M4/483 , H01M4/502 , H01M4/582 , H01M6/14 , H01M6/164 , H01M10/056 , H01M10/0568 , H01M10/0569 , H01M2300/0045 , Y10T29/49108
摘要： Compositions and methods of making are provided for a high energy density aluminum battery. The battery comprises an anode comprising aluminum metal. The battery further comprises a cathode comprising a material capable of intercalating aluminum or lithium ions during a discharge cycle and deintercalating the aluminum or lithium ions during a charge cycle. The battery further comprises an electrolyte capable of supporting reversible deposition and stripping of aluminum at the anode, and reversible intercalation and deintercalation of aluminum or lithium at the cathode.
摘要翻译：为高能量密度铝电池提供组合物和制备方法。电池包括包含铝金属的阳极。电池还包括阴极，其包括能够在放电循环期间插入铝或锂离子的材料，并且在充电循环期间使铝或锂离子脱嵌。电池还包括能够支持在阳极处可逆沉积和剥离铝的电解质，以及在阴极处可逆地插入和脱嵌铝或锂。

5. 发明申请

WO2012071203A3 REAL SPACE MAPPING OF IONIC DIFFUSION AND ELECTROCHMICAL ACTIVITY IN ENERGY STORAGE AND CONVERSION MATERIALS 审中-公开
标题翻译：能量储存和转换材料中离子扩散和电化学活性的实际空间映射
公开(公告)号：WO2012071203A3
公开(公告)日：2012-07-19
申请号：PCT/US2011060547
申请日：2011-11-14
申请人： UT BATTELLE LLC , KALININ SERGEI V , BALKE NINA , KUMAR AMIT , DUDNEY NANCY J , JESSE STEPHEN
发明人： KALININ SERGEI V , BALKE NINA , KUMAR AMIT , DUDNEY NANCY J , JESSE STEPHEN
IPC分类号： G01N27/00 , G01R31/00 , G01R31/26
CPC分类号： G01Q60/60 , G01Q60/02 , G01Q60/30
摘要： A method and system for probing mobile ion diffusivity and electrochemical reactivity on a nanometer length scale of a free electrochemically active surface includes a control module that biases the surface of the material. An electrical excitation signal is applied to the material and induces the movement of mobile ions. An SPM probe in contact with the surface of the material detects the displacement of mobile ions at the surface of the material. A detector measures an electromechanical strain response at the surface of the material based on the movement and reactions of the mobile ions. The use of an SPM tip to detect local deformations allows highly reproducible measurements in an ambient environment without visible changes in surface structure. The measurements illustrate effective spatial resolution comparable with defect spacing and well below characteristic grain sizes of the material.
摘要翻译：用于在自由电化学活性表面的纳米长度尺度上探测移动离子扩散性和电化学反应性的方法和系统包括偏置材料表面的控制模块。电激励信号被施加到材料并诱导移动离子的移动。与材料表面接触的SPM探针检测材料表面上的移动离子的位移。检测器基于移动离子的移动和反应来测量材料表面处的机电应变响应。使用SPM尖端检测局部变形允许在周围环境中进行高度可重现的测量，而不会在表面结构中发生可见的变化。测量结果表明有效的空间分辨率与缺陷间距相当，并远低于材料的特征晶粒尺寸。

6. 发明申请

WO2012044678A3 A HIGH ENERGY DENSITY ALUMINUM BATTERY 审中-公开
标题翻译：高能量密度铝电池
公开(公告)号：WO2012044678A3
公开(公告)日：2012-07-12
申请号：PCT/US2011053667
申请日：2011-09-28
申请人： UT BATTELE LLC , BROWN GILBERT M , PARANTHAMAN MARIAPPAN PARANS , DAI SHENG , DUDNEY NANCY J , MANTHIRAM ARUMUGAN , MCINTYRE TIMOTHY , SUN XIAGO-GUANG , LIU HANSAN
发明人： BROWN GILBERT M , PARANTHAMAN MARIAPPAN PARANS , DAI SHENG , DUDNEY NANCY J , MANTHIRAM ARUMUGAN , MCINTYRE TIMOTHY , SUN XIAGO-GUANG , LIU HANSAN
IPC分类号： H01M10/05 , H01M4/38 , H01M6/16 , H01M10/052 , H01M10/0564
CPC分类号： H01M10/054 , H01M4/38 , H01M4/463 , H01M4/483 , H01M4/502 , H01M4/582 , H01M6/14 , H01M6/164 , H01M10/056 , H01M10/0568 , H01M10/0569 , H01M2300/0045 , Y10T29/49108
摘要： Compositions and methods of making are provided for a high energy density aluminum battery. The battery comprises an anode comprising aluminum metal. The battery further comprises a cathode comprising a material capable of intercalating aluminum or lithium ions during a discharge cycle and deintercalating the aluminum or lithium ions during a charge cycle. The battery further comprises an electrolyte capable of supporting reversible deposition and stripping of aluminum at the anode, and reversible intercalation and deintercalation of aluminum or lithium at the cathode.
摘要翻译：提供用于高能量密度铝电池的组合物和制造方法。该电池包含含有铝金属的阳极。电池进一步包括阴极，阴极包含在放电循环期间能够嵌入铝或锂离子的材料并且在充电循环期间使铝或锂离子脱嵌。该电池进一步包含能够支持阳极处铝的可逆沉积和剥离的电解质，并且在阴极处可逆地嵌入和解嵌铝或锂。

7. 发明申请

WO2012071203A2 REAL SPACE MAPPING OF IONIC DIFFUSION AND ELECTROCHMICAL ACTIVITY IN ENERGY STORAGE AND CONVERSION MATERIALS 审中-公开
标题翻译：能量储存和转化材料中离子扩散和电化学活动的实际空间映射
公开(公告)号：WO2012071203A2
公开(公告)日：2012-05-31
申请号：PCT/US2011/060547
申请日：2011-11-14
申请人： UT-BATTELLE, LLC , KALININ, Sergei, V. , BALKE, Nina , KUMAR, Amit , DUDNEY, Nancy, J. , JESSE, Stephen
发明人： KALININ, Sergei, V. , BALKE, Nina , KUMAR, Amit , DUDNEY, Nancy, J. , JESSE, Stephen
IPC分类号： G01N27/00 , G01R31/26 , G01R31/00
CPC分类号： G01Q60/60 , G01Q60/02 , G01Q60/30
摘要： A method and system for probing mobile ion diffusivity and electrochemical reactivity on a nanometer length scale of a free electrochemically active surface includes a control module that biases the surface of the material. An electrical excitation signal is applied to the material and induces the movement of mobile ions. An SPM probe in contact with the surface of the material detects the displacement of mobile ions at the surface of the material. A detector measures an electromechanical strain response at the surface of the material based on the movement and reactions of the mobile ions. The use of an SPM tip to detect local deformations allows highly reproducible measurements in an ambient environment without visible changes in surface structure. The measurements illustrate effective spatial resolution comparable with defect spacing and well below characteristic grain sizes of the material.
摘要翻译：用于探测自由电化学活性表面的纳米尺度上的移动离子扩散率和电化学反应性的方法和系统包括偏压材料表面的控制模块。电激励信号被施加到材料并引起移动离子的移动。与材料表面接触的SPM探针检测到材料表面上的移动离子的位移。检测器基于移动离子的运动和反应来测量材料表面处的机电应变响应。使用SPM尖端来检测局部变形允许在周围环境中进行高度可重复的测量，而没有表面结构的可见变化。测量结果说明了有效的空间分辨率与缺陷间距相当，远远低于材料的特征晶粒尺寸。

8. 发明申请

WO2006015328A3 PULSE THERMAL PROCESSING OF FUNCTIONAL MATERIALS USING DIRECTED PLASMA ARC 审中-公开
标题翻译：使用方向等离子体弧的功能材料的脉冲热处理
公开(公告)号：WO2006015328A3
公开(公告)日：2006-08-03
申请号：PCT/US2005027301
申请日：2005-08-01
申请人： UT BATTELLE LLC , OTT RONALD D , BLUE CRAIG A , DUDNEY NANCY J , HARPER DAVID C
发明人： OTT RONALD D , BLUE CRAIG A , DUDNEY NANCY J , HARPER DAVID C
IPC分类号： C23C4/18 , B05D3/14 , C23C2/26 , G11B5/84 , H01L21/263 , H01L21/268 , H01L31/00
CPC分类号： H01L21/324 , B05D3/148 , B82Y30/00 , C23C2/26 , C23C4/18 , C23C26/00 , G11B5/84 , H01L31/0322 , H01L31/1864 , Y02E10/541 , Y02P70/521
摘要： A method of thermally processing a material includes the steps of providing an article having a surface film disposed on a substrate, and exposing the thin film to at least one incident pulse of infrared comprising radiation at a power density of at least 0.1 kW/cm 2 emitted from a directed plasma arc to thermally process the thin film. The at least one pulse has a duration of no more than 10 s. The method provides a radiation intensity and spectrum of radiation capable of heating the surface film to the desired temperature while allowing the substrate to remain at a lower temperature. This feature permits use of substrates that generally are not high temperature tolerant, such as certain polymer substrates.
摘要翻译：一种热处理材料的方法包括以下步骤：提供具有设置在基底上的表面膜的制品，并将薄膜暴露于至少一个红外线的入射脉冲，其中包括以至少0.1kW / cm 2的功率密度的辐射， SUP> 2 从定向等离子体电弧发射，以热处理薄膜。该至少一个脉冲的持续时间不超过10秒。该方法提供辐射强度和能够将表面膜加热至所需温度的辐射光谱，同时允许基底保持在较低的温度。该特征允许使用通常不耐高温的基底，例如某些聚合物基底。

9. 发明申请

WO2006015328A2 PULSE THERMAL PROCESSING OF FUNCTIONAL MATERIALS USING DIRECTED PLASMA ARC 审中-公开
标题翻译：用等离子弧进行脉冲热处理功能材料
公开(公告)号：WO2006015328A2
公开(公告)日：2006-02-09
申请号：PCT/US2005/027301
申请日：2005-08-01
申请人： UT-BATTELLE, LLC. , OTT, Ronald, D. , BLUE, Craig, A. , DUDNEY, Nancy, J. , HARPER, David, C.
发明人： OTT, Ronald, D. , BLUE, Craig, A. , DUDNEY, Nancy, J. , HARPER, David, C.
IPC分类号： H01J61/00
CPC分类号： H01L21/324 , B05D3/148 , B82Y30/00 , C23C2/26 , C23C4/18 , C23C26/00 , G11B5/84 , H01L31/0322 , H01L31/1864 , Y02E10/541 , Y02P70/521
摘要： A method of thermally processing a material includes the steps of providing an article having a surface film disposed on a substrate, and exposing the thin film to at least one incident pulse of infrared comprising radiation at a power density of at least 0.1 kW/cm 2 emitted from a directed plasma arc to thermally process the thin film. The at least one pulse has a duration of no more than 10 s. The method provides a radiation intensity and spectrum of radiation capable of heating the surface film to the desired temperature while allowing the substrate to remain at a lower temperature. This feature permits use of substrates that generally are not high temperature tolerant, such as certain polymer substrates.
摘要翻译：对材料进行热处理的方法包括以下步骤：提供具有设置在衬底上的表面膜的制品;以及将所述薄膜暴露于至少一个红外入射脉冲，所述红外入射脉冲包括功率密度从定向等离子弧发射的至少0.1kW / cm 2的热量来热处理薄膜。至少一个脉冲具有不超过10秒的持续时间。该方法提供辐射强度和辐射光谱，该辐射强度和辐射光谱能够将表面薄膜加热到期望的温度，同时允许基底保持在较低的温度。此功能允许使用通常不耐高温的基材，如某些聚合物基材。

10. 发明申请

WO0060689A9 BATTERY WITH AN IN-SITU ACTIVATION PLATED LITHIUM ANODE 审中-公开
标题翻译：具有原位激活的锂离子阳极的电池
公开(公告)号：WO0060689A9
公开(公告)日：2002-03-14
申请号：PCT/US0006997
申请日：2000-03-17
申请人： UT BATELLE L L C , NEUDECKER BERND J , DUDNEY NANCY J , BATES JOHN B
发明人： NEUDECKER BERND J , DUDNEY NANCY J , BATES JOHN B
IPC分类号： H01M4/02 , H01M4/04 , H01M4/66 , H01M6/18 , H01M6/40 , H01M10/36
CPC分类号： H01M10/0436 , H01M4/0447 , H01M4/661 , H01M6/185 , H01M6/188 , H01M6/40 , H01M10/052 , H01M10/056 , H01M2004/027
摘要： A thin-film rechargeable battery includes a cathode film (3); including a lithium transition metal oxide, an electrolyte film (4) coupled to the cathode film, the electrolyte film being substantially nonreactive with oxidizing materials and with metallic lithium, an anode current collector (5) coupled to the electrolyte film; and an overlying layer (6) coupled to the anode current collector. The thin-film rechargeable battery is activated during an initial charge by electrochemical plating of a metallic lithium anode (7) between the anode current collector and the electrolyte film. The plating of the anode during charging and the stripping of the anode layer during discharging are essentially reversible. Therefore, almost no diminishment of discharge capacity occurs, even after many discharge and charge cycles. Other advantages include no need for special packaging for shipping and handling. The battery eliminates the main drawbacks of the thin-film Li-ion battery (high capacity loss during the initial charge) and of the thin-film lithium battery (high air-sensitivity at all times, temperature limited to SIMILAR 100 DEG C, expensive preparation of the lithium anode). The battery survives processing conditions that exceed those of a solder reflow process without any signs of degradation.
摘要翻译：薄膜可再充电电池包括阴极膜（3）; 包括锂过渡金属氧化物，耦合到阴极膜的电解质膜（4），所述电解质膜与氧化材料和金属锂基本上非反应性，耦合到所述电解质膜的阳极集电器（5）; 以及耦合到阳极集电器的上覆层（6）。在初始充电期间，通过在阳极集电器和电解质膜之间的金属锂阳极（7）的电化学电镀来激活薄膜可再充电电池。在充电期间阳极的电镀和在放电期间阳极层的剥离基本上是可逆的。因此，即使在许多放电和充电循环之后，也几乎不会发生放电容量的减小。其他优点包括不需要特殊的包装运输和处理。电池消除了薄膜锂离子电池的主要缺点（初始充电期间的高容量损耗）和薄膜锂电池（高度空气灵敏度始终保持在100℃，温度极限，昂贵锂阳极的制备）。电池的处理条件超过了焊料回流工艺，而没有任何退化的迹象。

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