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1. 发明申请

WO2019123126A1 PROCESS FOR THE MANUFACTURING OF A 3-HALOPROPIONYL HALIDE IN A FLOW REACTOR 审中-公开
公开(公告)号：WO2019123126A1
公开(公告)日：2019-06-27
申请号：PCT/IB2018/059956
申请日：2018-12-12
申请人： 3M INNOVATIVE PROPERTIES COMPANY , DAMS, Rudolf J.
发明人： VAN CAMPENHOUT, Rudy W. , CONRADI, Matthias , MOVSISYAN, Marine , STEVENS, Christian
IPC分类号： C07C51/60 , C07C51/62 , C07C53/50
CPC分类号： C07C51/58 , C07C53/50
摘要： The present disclosure relates to a process for the manufacturing of a 3-5 halopropionylhalide, wherein the process comprises the steps of: a) providing a flow reactor comprising a reaction chamber; b) providing reactants comprising: i. acrylic acid; ii. a reaction co-agent selected from the group consisting of N,N-0 disubstituted amides; and iii. a halogenating agent; and c) incorporating the reactants into the reaction chamber of the flow reactor, thereby forming a reaction product stream comprising a 3-halopropionylhalide; wherein the molar ratio of acrylic acid to the halogenating agent is 1 to at least 5 0.8; wherein the temperature of the reaction chamber of the flow reactor is greater than 60°C; and wherein the residence time of the reaction product stream comprising the 3-halopropionylhalide in the reaction chamber of the flow reactor is greater than 10 minutes.

2. 发明申请

WO2011044093A3 TRIAZINE CONTAINING FLUOROPOLYETHER ELASTOMERS HAVING VERY LOW GLASS TRANSITION TERMPERATURES, COMPOSITIONS CONTAINING THEM AND METHODS OF MAKING THEM 审中-公开
标题翻译：含有极低玻璃转变温度的含氟聚合物弹性体，含有它们的组合物及其制备方法
公开(公告)号：WO2011044093A3
公开(公告)日：2011-08-18
申请号：PCT/US2010051422
申请日：2010-10-05
申请人： 3M INNOVATIVE PROPERTIES CO , CORVELEYN STEVEN G , DAMS RUDOLF J , GROOTAERT WERNER M A , DAHLKE GREGG D , GUERRA MIGUEL A
发明人： CORVELEYN STEVEN G , DAMS RUDOLF J , GROOTAERT WERNER M A , DAHLKE GREGG D , GUERRA MIGUEL A
IPC分类号： C08G65/32 , C08G65/323 , C08G65/333 , C08J5/00 , C08L71/00
CPC分类号： C08G65/007
摘要： A method of making a fluoropolyether elastomer containing triazine groups and having a glass transition temperature of less than -40 °C, including providing (i) one or more saturated fluoropolyethers containing repeating moieties selected from (-C4F8O-), (-C3F6O-), (-C2F4O-), (-CF2O-) and combinations thereof and further containing at least one functional group at a terminal carbon atom of the backbone chain, or of a side chain if present, wherein the terminal carbon atom may be a primary or secondary carbon atom and wherein the functional group is capable of reacting with a functional group of the fluorinated compound according to (ii) below to form a triazine ring, (ii) one or more fluorinated compound containing at least one perfluorinated alkyl or perfluorinated alkylene moiety wherein the carbon atoms of the perfluorinated alkyl or alkylene moiety may be interrupted by one or more oxygen atoms and wherein the fluorinated compound further contains at least one functional group capable of reacting with the functional group of the one or more fluoropolyethers to form a triazine; curing the components according to (i) and (ii) to form triazines. Further provided are cured compositions, articles comprising the cured compositions and methods of making articles.
摘要翻译：一种制备含三嗪基团且玻璃化转变温度低于-40℃的含氟聚醚弹性体的方法，包括提供（i）一种或多种含有选自（-C 4 F 8 O - ），（ - C 3 F 6 O - ） - ，（ - C 2 F 4 O-），（ - CF 2 O-）及其组合，并且在主链的末端碳原子或侧链（如果存在）还包含至少一个官能团，其中末端碳原子可以是伯或仲碳原子，并且其中所述官能团能够与根据以下（ii）的氟化化合物的官能团反应以形成三嗪环，（ii）一种或多种含有至少一种全氟化烷基或全氟化亚烷基的氟化化合物其中全氟化烷基或亚烷基部分的碳原子可以被一个或多个氧原子间隔，并且其中氟化化合物还包含至少一个官能团帽能够与一种或多种含氟聚醚的官能团反应形成三嗪; 根据（i）和（ii）固化组分以形成三嗪。进一步提供了固化组合物，包含固化组合物的制品和制造制品的方法。

3. 发明申请

WO2011044093A2 TRIAZINE CONTAINING FLUOROPOLYETHER ELASTOMERS HAVING VERY LOW GLASS TRANSITION TERMPERATURES, COMPOSITIONS CONTAINING THEM AND METHODS OF MAKING THEM 审中-公开
标题翻译：含有非常低的玻璃化转变温度的含氟荧光体弹性体的TRIAZINE，包含它们的组合物及其制备方法
公开(公告)号：WO2011044093A2
公开(公告)日：2011-04-14
申请号：PCT/US2010/051422
申请日：2010-10-05
申请人： 3M INNOVATIVE PROPERTIES COMPANY , CORVELEYN, Steven, G. , DAMS, Rudolf, J. , GROOTAERT, Werner, M., A. , DAHLKE, Gregg, D. , GUERRA, Miguel, A.
发明人： CORVELEYN, Steven, G. , DAMS, Rudolf, J. , GROOTAERT, Werner, M., A. , DAHLKE, Gregg, D. , GUERRA, Miguel, A.
IPC分类号： C08G65/32 , C08G65/323 , C08G65/333 , C08L71/00 , C08J5/00
CPC分类号： C08G65/007
摘要： A method of making a fluoropolyether elastomer containing triazine groups and having a glass transition temperature of less than -40 °C, including providing (i) one or more saturated fluoropolyethers containing repeating moieties selected from (-C 4 F 8 O-), (-C 3 F 6 O-), (-C 2 F 4 O-), (-CF 2 O-) and combinations thereof and further containing at least one functional group at a terminal carbon atom of the backbone chain, or of a side chain if present, wherein the terminal carbon atom may be a primary or secondary carbon atom and wherein the functional group is capable of reacting with a functional group of the fluorinated compound according to (ii) below to form a triazine ring, (ii) one or more fluorinated compound containing at least one perfluorinated alkyl or perfluorinated alkylene moiety wherein the carbon atoms of the perfluorinated alkyl or alkylene moiety may be interrupted by one or more oxygen atoms and wherein the fluorinated compound further contains at least one functional group capable of reacting with the functional group of the one or more fluoropolyethers to form a triazine; curing the components according to (i) and (ii) to form triazines. Further provided are cured compositions, articles comprising the cured compositions and methods of making articles.
摘要翻译：制备含有三嗪基并具有小于-40℃的玻璃化转变温度的氟聚醚弹性体的方法，包括提供（i）一种或多种含有重复部分的饱和含氟聚醚，所述重复部分选自（-C 4 F 8 O-），（-C 3 F 6 O-），（-C 2 F 4 O-），（-CF 2 O-）及其组合，并且在主链的末端碳原子或侧链（如果存在）中还含有至少一个官能团，其中末端碳原子可以是伯或仲碳原子，并且其中所述官能团能够与下述（ii）的氟化化合物的官能团反应以形成三嗪环，（ii）一种或多种含有至少一个全氟化烷基或全氟化亚烷基的氟化化合物部分，其中全氟化烷基或亚烷基部分的碳原子可被一个或多个氧原子间隔，并且其中氟化化合物还含有至少一个官能团帽能够与一种或多种含氟聚醚的官能团反应形成三嗪; 根据（i）和（ii）固化组分以形成三嗪。还提供了固化组合物，包含固化组合物的制品和制造制品的方法。

4. 发明申请

WO2010132362A3 METHOD FOR TREATING HYDROCARBON-BEARING FORMATIONS WITH FLUORINATED POLYURETHANES 审中-公开
标题翻译：用氟化聚氨酯处理碳氢化合物的方法
公开(公告)号：WO2010132362A3
公开(公告)日：2011-03-24
申请号：PCT/US2010034246
申请日：2010-05-10
申请人： UNIV TEXAS , 3M INNOVATIVE PROPERTIES CO , SHARMA MUKUL M , DAMS RUDOLF J , WU YONG K , FAN WAYNE W , MARTIN STEVE J
发明人： SHARMA MUKUL M , DAMS RUDOLF J , WU YONG K , FAN WAYNE W , MARTIN STEVE J
IPC分类号： C09K8/588 , C09K8/58
CPC分类号： C09K8/52 , C09K8/604 , C09K8/80
摘要： A method of treating a hydrocarbon-bearing formation including receiving data comprising a temperature and a brine composition of the hydrocarbon-bearing formation; selecting a treatment composition for the hydrocarbon-bearing formation comprising a fluorinated polyurethane and solvent, wherein, at the temperature, a mixture of an amount of the brine composition and the treatment composition is transparent and free of precipitated solid, and wherein the mixture does not separate into layers; and contacting the hydrocarbon-bearing formation with the treatment composition. Another method of treating a hydrocarbon-bearing formation includes contacting a limestone formation with a treatment composition comprising a fluorinated polyurethane and solvent. Hydrocarbon-bearing formations treated according to the method are also disclosed. A composition comprising a fluorinated polyurethane and a combination of solvents is also disclosed.
摘要翻译：一种处理含烃地层的方法，包括含有含烃地层的温度和盐水组成的接收数据; 选择包含氟化聚氨酯和溶剂的含烃地层的处理组合物，其中在该温度下，一定量的盐水组合物和处理组合物的混合物是透明的并且不含沉淀的固体，并且其中混合物不分成层并使含烃地层与处理组合物接触。处理含烃地层的另一种方法包括使石灰石地层与包含氟化聚氨酯和溶剂的处理组合物接触。还公开了根据该方法处理的含烃地层。还公开了包含氟化聚氨酯和溶剂组合的组合物。

5. 发明申请

WO2011005672A3 METHODS FOR TREATING CARBONATE HYDROCARBON-BEARING FORMATIONS WITH FLUORINATED AMPHOTERIC COMPOUNDS 审中-公开
公开(公告)号：WO2011005672A3
公开(公告)日：2011-01-13
申请号：PCT/US2010/040870
申请日：2010-07-02
申请人： 3M INNOVATIVE PROPERTIES COMPANY , DAMS, Rudolf, J. , MARTIN, Steven, J. , WU, Yong, K.
发明人： DAMS, Rudolf, J. , MARTIN, Steven, J. , WU, Yong, K.
IPC分类号： C09K8/60 , C09K8/80 , E21B43/26
摘要： Method of treating a carbonate hydrocarbon-bearing formation. The method includes contacting the hydrocarbon-bearing formation with a composition comprising solvent and a fluorinated amphoteric compound. Carbonate hydrocarbon-bearing formations treated according to the method are also disclosed.

6. 发明申请

WO2011005672A2 METHODS FOR TREATING CARBONATE HYDROCARBON-BEARING FORMATIONS WITH FLUORINATED AMPHOTERIC COMPOUNDS 审中-公开
标题翻译：用氟化两性化合物处理碳酸盐含烃地层的方法
公开(公告)号：WO2011005672A2
公开(公告)日：2011-01-13
申请号：PCT/US2010040870
申请日：2010-07-02
申请人： 3M INNOVATIVE PROPERTIES CO , DAMS RUDOLF J , MARTIN STEVEN J , WU YONG K
发明人： DAMS RUDOLF J , MARTIN STEVEN J , WU YONG K
IPC分类号： C09K8/60 , C09K8/80 , E21B43/26
CPC分类号： C09K8/68 , B01F17/0035 , C03C12/02 , C08F8/44 , C09K8/602 , C09K8/604 , C25C1/00
摘要： Method of treating a carbonate hydrocarbon-bearing formation. The method includes contacting the hydrocarbon-bearing formation with a composition comprising solvent and a fluorinated amphoteric compound. Carbonate hydrocarbon-bearing formations treated according to the method are also disclosed.
摘要翻译：处理碳酸盐含烃地层的方法。该方法包括使含烃地层与包含溶剂和氟化两性化合物的组合物接触。还公开了根据该方法处理的含碳氢化合物烃的地层。

7. 发明申请

WO2010144398A3 METHOD FOR TREATING HYDROCARBON-BEARING FORMATIONS WITH POLYFLUOROPOLYETHER SILANES 审中-公开
公开(公告)号：WO2010144398A3
公开(公告)日：2010-12-16
申请号：PCT/US2010/037705
申请日：2010-06-08
申请人： 3M INNOVATIVE PROPERTIES COMPANY , DAMS, Rudolf, J. , MARTIN, Steven, J. , WU, Yong, K.
发明人： DAMS, Rudolf, J. , MARTIN, Steven, J. , WU, Yong, K.
IPC分类号： C09K8/588 , C09K8/58 , C08L83/00
摘要： Method comprising contacting a hydrocarbon-bearing formation with a treatment composition comprising solvent and a fluoropolyether silane. The fluoropolyether silane: is selected from the group consisting of: (a) Rf'-[Q-X'-(Si(Y') w (Y) 3-W ) m ] n ; (b) a compound comprising at least one first divalent unit represented by formula (I): and at least one of (i) a second divalent unit comprising a pendent -Si(Y') w (Y) 3-w group; or (ii) a monovalent unit comprising a thioether linkage and at least one terminal -Si(Y') w (Y) 3-w group; and (c) combinations thereof. Hydrocarbon-bearing formations treated according to this method are also disclosed.

8. 发明申请

WO2010144352A2 METHOD FOR TREATING HYDROCARBON-BEARING FORMATIONS WITH FLUOROALKYL SILANES 审中-公开
标题翻译：用氟代烷基硅烷处理碳氢化合物的方法
公开(公告)号：WO2010144352A2
公开(公告)日：2010-12-16
申请号：PCT/US2010/037601
申请日：2010-06-07
申请人： 3M INNOVATIVE PROPERTIES COMPANY , FAN, Wayne W. , ARCO, Manuel , DAMS, Rudolf J. , SAVU, Patricia M. , MARTIN, Steven J. , WU, Yong K.
发明人： FAN, Wayne W. , ARCO, Manuel , DAMS, Rudolf J. , SAVU, Patricia M. , MARTIN, Steven J. , WU, Yong K.
IPC分类号： C09K8/035 , C08L83/04 , C08K5/54
CPC分类号： C09K8/584
摘要： A method of treating a hydrocarbon-bearing formation, which includes contacting the hydrocarbon-bearing formation with a treatment composition, the treatment composition includes solvent and a fluorinated silane, wherein the fluorinated silane is selected from the group consisting of: a fluorinated silane represented by formula R 1 -SO 2 -N (R)(C n H 2n )-Si(Y')w(Y) 3-w ; a nonionic compound free of alkyleneoxy groups and comprising at least one first divalent unit represented by (formula I) and at least one of a second divalent unit comprising a pendent -Si(Y') w (Y) 3-w group; or a monovalent unit comprising a thioether linkage and at least one terminal -Si(Y') w (Y) 3-w group; and combinations thereof. Hydrocarbon-bearing formations treated with fluorinated silanes or siloxanes are also disclosed.
摘要翻译：一种处理含烃地层的方法，包括使含烃地层与处理组合物接触，所述处理组合物包括溶剂和氟化硅烷，其中所述氟化硅烷选自由以下组成的组：氟代硅烷，由式R 1 -SO 2 -N（R）（C n H 2n）-Si（Y'）w（Y）3-w; 包含至少一个由（式I）表示的至少一个第一二价单元和至少一个包含侧-Si（Y'）w（Y）3-w基团的第二二价单元的非离子化合物; 或包含硫醚键和至少一个末端-Si（Y'）w（Y）3-w基团的一价单元; 及其组合。还公开了用氟化硅烷或硅氧烷处理的含烃地层。

9. 发明申请

WO2010009191A3 FLUORINATED ETHER COMPOUNDS AND METHODS OF USING THE SAME 审中-公开
标题翻译：氟化醚化合物及其使用方法
公开(公告)号：WO2010009191A3
公开(公告)日：2010-07-22
申请号：PCT/US2009050627
申请日：2009-07-15
申请人： 3M INNOVATIVE PROPERTIES CO , DAMS RUDOLF J , TERRAZAS MICHAEL S , HINTZER KLAUS , QIU ZAI-MING , GUERRA MIGUEL A , MAURER ANDREAS R , KASPAR HARALD , LOCHHAAS KAI H , JUERGENS MICHAEL , ZIPPLIES TILMAN C , SCHWERTFEGER WERNER
发明人： DAMS RUDOLF J , TERRAZAS MICHAEL S , HINTZER KLAUS , QIU ZAI-MING , GUERRA MIGUEL A , MAURER ANDREAS R , KASPAR HARALD , LOCHHAAS KAI H , JUERGENS MICHAEL , ZIPPLIES TILMAN C , SCHWERTFEGER WERNER
IPC分类号： C07C235/10 , C07C217/28 , C07C219/06
CPC分类号： C07C235/10 , C07C69/708 , C07C211/11 , C07C211/14 , C07C291/04 , C07C309/14 , C07F9/091 , C07F9/3808 , C08G65/007
摘要： Compounds represented by formula (Rf-Q-X)s-Z. Each Rf is independently a partially fluorinated or fully fluorinated group selected from Rfa-(O)r-CHF-(CF2)n-; [Rfb-(O)t-C(L)H-CF2-O]m-W-; CF3CFH-O-(CF2)p-; CF3-(O-CF2)z-; and CF3-O-(CF2)3-O-CF2-. Methods of reducing surface tension of a liquid, making foams, and treating a surface using the compounds are also disclosed.
摘要翻译：由式（Rf-Q-X）s-Z表示的化合物。每个Rf独立地为选自Rfa-（O）r-CHF-（CF 2）n - 的部分氟化或完全氟化的基团; [Rfb-（O）T-C（L）H-CF 2 -O] M-W-; CF 3 CFH-O-（CF 2）p - ; CF 3 - （O-CF 2）z - ; 和CF 3 -O-（CF 2）3 -O-CF 2 - 。还公开了降低液体表面张力，制造泡沫和使用该化合物处理表面的方法。

10. 发明申请

WO2010080353A2 METHOD OF CONTACTING HYDROCARBON-BEARING FORMATIONS WITH FLUORINATED PHOSPHATE AND PHOSPHONATE COMPOSITIONS 审中-公开
标题翻译：含氟化磷酸盐和磷酸盐组合物与含油层接触的方法
公开(公告)号：WO2010080353A2
公开(公告)日：2010-07-15
申请号：PCT/US2009/067829
申请日：2009-12-14
申请人： 3M INNOVATIVE PROPERTIES COMPANY , DAMS, Rudolf J. , BARAN, Jimmie R., , WU, Yong K.
发明人： DAMS, Rudolf J. , BARAN, Jimmie R., , WU, Yong K.
IPC分类号： C09K8/58 , C09K8/584
CPC分类号： C09K8/584 , C08F20/24 , C09K8/602 , C09K8/80 , C09K8/88
摘要： Method comprising contacting a hydrocarbon-bearing formation with a composition comprising solvent and a fluoropolyether compound. The fluoropolyether compound: is represented by formula Rf-[C(0)-NR 1 -X'-(Z) m ] n ; or comprises at least one first divalent unit represented by formula (I) and, at least one of, a second divalent unit comprising a pendant Z group; or a monovalent unit comprising a thioether linkage and at least one terminal Z group. Each Rf is independently a fluoropolyether group. Rf is a monovalent or divalent fluoropolyether group, and each Z group is independently -P(O)(OY) 2 or -O-P(O)(OY) 2 . Hydrocarbon-bearing formations treated according to this method are also disclosed.
摘要翻译：方法包括使含烃地层与包含溶剂和含氟聚醚化合物的组合物接触。含氟聚醚化合物：由式Rf- [C（O）-NR 1 -X' - （Z）m] n -n表示; 或包含至少一个由式（I）表示的第一二价单元和至少一个包含侧基Z基团的第二二价单元; 或包含硫醚键和至少一个末端Z基团的单价单元。每个Rf独立地是含氟聚醚基团。 R f是一价或二价含氟聚醚基团，并且每个Z基团独立地是-P（O）（OY）2或-O-P（O）（OY）2。也公开了根据该方法处理的含烃地层。

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