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1. 发明申请

WO2008002890A2 COMPOSITIONS AND METHODS FOR POLYMER COMPOSITES 审中-公开
标题翻译：聚合物复合材料的组合物和方法
公开(公告)号：WO2008002890A2
公开(公告)日：2008-01-03
申请号：PCT/US2007/072072
申请日：2007-06-26
申请人： GENERAL ELECTRIC COMPANY , CHAN, Kwok, Pong , CROLL, Joshua, McClellan , HAGBERG, Erik , MAXAM, John, Lester , MULLEN, Tara, J. , ODLE, Roy, Ray , SUFFIELD, Rachel, Marie , WHITE, James, Mitchell , YAMAGUCHI, Norimitsu
发明人： CHAN, Kwok, Pong , CROLL, Joshua, McClellan , HAGBERG, Erik , MAXAM, John, Lester , MULLEN, Tara, J. , ODLE, Roy, Ray , SUFFIELD, Rachel, Marie , WHITE, James, Mitchell , YAMAGUCHI, Norimitsu
CPC分类号： C08J5/18 , C08J3/201 , C08J5/10 , C08J2379/08 , C08K3/346 , C08K5/18 , C08K5/19 , C08K5/3432 , C08K5/50 , C08K9/04
摘要： This invention relates to organic salt compositions useful in the preparation of organoclay compositions, polymer-organoclay composite compositions, and methods for the preparation of polymer nanocomposites. In one embodiment, the present invention provides a method of making a polymer-organoclay composite composition, said method comprising melt mixing a quaternary organoclay composition comprising alternating inorganic silicate layers and organic layers, said organic layers comprising a quaternary organic cation with a polyetherimide composition; said melt mixing being carried out at a temperature in a range between about 300°C and about 450°C to provide a polymer-organoclay composite composition, said polymer-organoclay composite composition being characterized by a percent exfoliation of at least 10 percent.
摘要翻译：本发明涉及可用于制备有机粘土组合物，聚合物 - 有机粘土复合材料组合物和制备聚合物纳米复合材料的方法的有机盐组合物。在一个实施方案中，本发明提供了制备聚合物 - 有机粘土复合材料组合物的方法，所述方法包括熔融混合包含交替的无机硅酸盐层和有机层的季有机粘土组合物，所述有机层包含季铵有机阳离子与聚醚酰亚胺组合物; 所述熔体混合在约300℃至约450℃之间的温度下进行，以提供聚合物 - 有机粘土复合材料组合物，所述聚合物 - 有机粘土复合组合物的特征在于至少10％的剥离百分比。

2. 发明申请

WO2008002888A3 COMPOSITIONS AND METHODS FOR POLYMER COMPOSITES 审中-公开
公开(公告)号：WO2008002888A3
公开(公告)日：2008-01-03
申请号：PCT/US2007/072070
申请日：2007-06-26
申请人： GENERAL ELECTRIC COMPANY , CHAN, Kwok, Pong , CROLL, Joshua, McClellan , GANESAN, Balakrishnan , HAGBERG, Erik , HARRIGAN, Marcus , KHOURI, Farid, Fouad , KISHAN, Gurram , MATHUR, Ritesh , MAXAM, John, Lester , MULLEN, Tara, J. , ODLE, Roy, Ray , RANGANATHAN, Sathish, Kumar , SUFFIELD, Rachel, Marie , WANG, Wenhui , WHITE, James, Mitchell
发明人： CHAN, Kwok, Pong , CROLL, Joshua, McClellan , GANESAN, Balakrishnan , HAGBERG, Erik , HARRIGAN, Marcus , KHOURI, Farid, Fouad , KISHAN, Gurram , MATHUR, Ritesh , MAXAM, John, Lester , MULLEN, Tara, J. , ODLE, Roy, Ray , RANGANATHAN, Sathish, Kumar , SUFFIELD, Rachel, Marie , WANG, Wenhui , WHITE, James, Mitchell
IPC分类号： C08K3/34 , C08K5/50 , C08K9/04 , C08L79/08
摘要： This invention relates to organic salt compositions useful in the preparation of organoclay compositions, polymer-organoclay composite compositions, and methods for the preparation of polymer nanocomposites. In one embodiment, the present invention provides a polymer-organoclay composite composition comprising (a) a polymeric resin; and (b) an organoclay composition comprising alternating inorganic silicate layers and organic layers, said organic layers comprising a quaternary phosphonium cation having structure X wherein Ar 1 , Ar 2 , and Ar 3 are independently C 2 -C 50 aromatic radicals; Ar 4 is a bond or a C 2 -C 50 aromatic radical; "a" is a number from 1 to about 200; "c" is a number from 0 to 3; R 1 is independently at each occurrence a halogen atom, a C 1 -C 20 aliphatic radical, a C 5 -C 20 cycloaliphatic radical, or a C 2 -C 20 aromatic radical; and R 2 is a halogen atom, a C 1 -C 20 aliphatic radical, a C 5 -C 20 cycloaliphatic radical, a C 2 -C 50 aromatic radical, or a polymer chain.

3. 发明申请

WO2008002886A3 PHOSPHONIUM SALTS FOR POLYMER COMPOSITES AND THEIR PREPARATION 审中-公开
标题翻译：聚合物复合材料的磷酸盐盐及其制备方法
公开(公告)号：WO2008002886A3
公开(公告)日：2008-03-13
申请号：PCT/US2007072068
申请日：2007-06-26
申请人： GEN ELECTRIC , CHAN KWOK PONG , CROLL JOSHUA MCCLELLAN , HARRIGAN MARCUS , SUFFIELD RACHEL MARIE , WANG WENHUI , WHITE JAMES MITCHELL
发明人： CHAN KWOK PONG , CROLL JOSHUA MCCLELLAN , HARRIGAN MARCUS , SUFFIELD RACHEL MARIE , WANG WENHUI , WHITE JAMES MITCHELL
IPC分类号： C08K9/04 , C07F9/572 , C07F9/6558 , C08K3/34 , C08K5/50 , C08L71/00 , C08L79/08 , C08L81/06
CPC分类号： C07F9/5728 , C07F9/65583 , C08G65/48 , C08G73/1053 , C08G75/23
摘要： This invention relates to organic salt compositions useful in the preparation of organoclay compositions, polymer-organoclay composite compositions, and methods for the preparation of polymer nanocomposites. In one embodiment, the present invention provides novel organophosphonium salts having structure (I) wherein Ar 1 , Ar 2 , and Ar 3 are independently C 2 -C 50 aromatic radicals; Ar 4 is a bond or a C 2 -C 50 aromatic radical; "a" is a number from 1 to about 200; "c" is a number from 0 to 3; R 1 is independently at each occurrence a halogen atom, a C 1 -C 20 aliphatic radical, a C 5 -C 20 cycloaliphatic radical, or a C 2 -C 20 aromatic radical; R 2 is a halogen atom, a C 1 -C 20 aliphatic radical, a C 5 -C 20 cycloaliphatic radical, a C 2 -C 50 aromatic radical, or a polymer chain; and X - is a charge balancing counterion. In another embodiment, the present invention provides methodologies for the preparation of organophosphonium salts having structure (I).
摘要翻译：本发明涉及可用于制备有机粘土组合物，聚合物 - 有机粘土复合材料组合物和制备聚合物纳米复合材料的方法的有机盐组合物。在一个实施方案中，本发明提供了具有结构（I）的新型有机鏻盐，其中Ar 1，Ar 2和Ar 3独立地为C 芳香族基团; Ar 4是一个键或一个C 2 -C 50芳族基团; “a”是从1到大约200的数字; “c”是从0到3的数字; R 1在每次出现时独立地为卤素原子，C 1 -C 20脂族基团，C 5 H 12 -C 20脂环族基团或C 2 -C 20芳族基团; R 2是卤素原子，C 1 -C 20脂族基团，C 5 -C 5烷基， SUB 20脂环族基团，C 2 -C 20芳族基团或聚合物链; 而X - SUP是电荷平衡抗衡离子。在另一个实施方案中，本发明提供了具有结构（I）的有机鏻盐的制备方法。

4. 发明申请

WO2017189314A1 METHODS AND SYSTEMS FOR THE MANUFACTURE OF AN AROMATIC PHTHALIC BISIMIDE AND A POLYETHERIMIDE 审中-公开
标题翻译：用于制备芳族邻苯二酰亚胺和聚醚酰亚胺的方法和系统
公开(公告)号：WO2017189314A1
公开(公告)日：2017-11-02
申请号：PCT/US2017/028541
申请日：2017-04-20
申请人： SABIC GLOBAL TECHNOLOGIES B.V. , CROLL, Joshua McClellan
发明人： CROLL, Joshua McClellan , ALJARRAH, Mohannad , GUGGENHEIM, Thomas Link
IPC分类号： C07D209/48 , B01D11/04 , C08G73/10 , C08L79/08
摘要： A method for producing an aromatic bisimide includes reacting a dialkali metal salt of a dihydroxy aromatic compound with a reactive substituted phthalimide under conditions effective to form a product mixture, introducing the product mixture to a liquid-liquid extraction column including an aqueous alkali metal hydroxide solution, and recovering from the liquid-liquid extraction column a purified aromatic bisimide having less than 500 ppm of residual dialkali metal salt of the dihydroxy aromatic compound, the corresponding dihydroxy aromatic compound, the corresponding mono-substituted salt of the dihydroxy aromatic compound, or a combination including at least one of the foregoing. A method for the manufacture of a polyetherimide from an aromatic bisimide prepared by the above method is also disclosed. A polyetherimide having less than 100 ppb of residual bisphenol A and an article made therefrom are also described.
摘要翻译：生产芳族双酰亚胺的方法包括在有效形成产物混合物的条件下使二羟基芳族化合物的二碱金属盐与反应性取代的邻苯二甲酰亚胺反应，将产物混合物引入液 - 液萃取从液 - 液萃取柱回收具有小于500ppm的二羟基芳族化合物的残余二碱金属盐，相应的二羟基芳族化合物，相应的单取代的盐的纯化的芳族双酰亚胺的二羟基芳族化合物，或包含前述中的至少一种的组合。还公开了由上述方法制备的芳族双酰亚胺制备聚醚酰亚胺的方法。还描述了具有小于100ppb的残余双酚A的聚醚酰亚胺和由其制成的制品。

5. 发明申请

WO2008002888A2 COMPOSITIONS AND METHODS FOR POLYMER COMPOSITES 审中-公开
标题翻译：聚合物复合材料的组合物和方法
公开(公告)号：WO2008002888A2
公开(公告)日：2008-01-03
申请号：PCT/US2007072070
申请日：2007-06-26
申请人： GEN ELECTRIC , CHAN KWOK PONG , CROLL JOSHUA MCCLELLAN , GANESAN BALAKRISHNAN , HAGBERG ERIK , HARRIGAN MARCUS , KHOURI FARID FOUAD , KISHAN GURRAM , MATHUR RITESH , MAXAM JOHN LESTER , MULLEN TARA J , ODLE ROY RAY , RANGANATHAN SATHISH KUMAR , SUFFIELD RACHEL MARIE , WANG WENHUI , WHITE JAMES MITCHELL
发明人： CHAN KWOK PONG , CROLL JOSHUA MCCLELLAN , GANESAN BALAKRISHNAN , HAGBERG ERIK , HARRIGAN MARCUS , KHOURI FARID FOUAD , KISHAN GURRAM , MATHUR RITESH , MAXAM JOHN LESTER , MULLEN TARA J , ODLE ROY RAY , RANGANATHAN SATHISH KUMAR , SUFFIELD RACHEL MARIE , WANG WENHUI , WHITE JAMES MITCHELL
CPC分类号： C08K5/50
摘要： This invention relates to organic salt compositions useful in the preparation of organoclay compositions, polymer-organoclay composite compositions, and methods for the preparation of polymer nanocomposites. In one embodiment, the present invention provides a polymer-organoclay composite composition comprising (a) a polymeric resin; and (b) an organoclay composition comprising alternating inorganic silicate layers and organic layers, said organic layers comprising a quaternary phosphonium cation having structure X wherein Ar 1 , Ar 2 , and Ar 3 are independently C 2 -C 50 aromatic radicals; Ar 4 is a bond or a C 2 -C 50 aromatic radical; "a" is a number from 1 to about 200; "c" is a number from 0 to 3; R 1 is independently at each occurrence a halogen atom, a C 1 -C 20 aliphatic radical, a C 5 -C 20 cycloaliphatic radical, or a C 2 -C 20 aromatic radical; and R 2 is a halogen atom, a C 1 -C 20 aliphatic radical, a C 5 -C 20 cycloaliphatic radical, a C 2 -C 50 aromatic radical, or a polymer chain.
摘要翻译：本发明涉及可用于制备有机粘土组合物的有机盐组合物，聚合物 - 有机粘土复合组合物和用于制备聚合物纳米复合材料的方法。在一个实施方案中，本发明提供了一种聚合物 - 有机粘土复合组合物，其包含（a）聚合物树脂; 和（b）包含交替的无机硅酸盐层和有机层的有机粘土组合物，所述有机层包含具有结构X的季鏻阳离子，其中Ar 1，Ar 2，Ar和Ar 3独立地为C 2 -C 50芳族基团; Ar 4是一个键或一个C 2 -C 50芳族基团; “a”是从1到约200的数字; “c”是从0到3的数字; R 1在每次出现时独立地为卤素原子，C 1 -C 20脂肪族基团，C 5 SUB > - C _{20 脂环族基团或C _{<2> _{20 芳族基团; 和R 2是卤素原子，C 1 -C 20脂肪族基团，C 5 -C 5脂肪族基团 20脂环族基团，C 2 -C 50芳族基团或聚合物链。}}}

6. 发明申请

WO2008002886A2 COMPOSITIONS AND METHODS FOR POLYMER COMPOSITES 审中-公开
标题翻译：聚合物复合材料的组合物和方法
公开(公告)号：WO2008002886A2
公开(公告)日：2008-01-03
申请号：PCT/US2007/072068
申请日：2007-06-26
申请人： GENERAL ELECTRIC COMPANY , CHAN, Kwok, Pong , CROLL, Joshua, McClellan , HARRIGAN, Marcus , SUFFIELD, Rachel, Marie , WANG, Wenhui , WHITE, James, Mitchell
发明人： CHAN, Kwok, Pong , CROLL, Joshua, McClellan , HARRIGAN, Marcus , SUFFIELD, Rachel, Marie , WANG, Wenhui , WHITE, James, Mitchell
CPC分类号： C07F9/5728 , C07F9/65583 , C08G65/48 , C08G73/1053 , C08G75/23
摘要： This invention relates to organic salt compositions useful in the preparation of organoclay compositions, polymer-organoclay composite compositions, and methods for the preparation of polymer nanocomposites. In one embodiment, the present invention provides novel organophosphonium salts having structure (I) wherein Ar 1 , Ar 2 , and Ar 3 are independently C 2 -C 50 aromatic radicals; Ar 4 is a bond or a C 2 -C 50 aromatic radical; "a" is a number from 1 to about 200; "c" is a number from 0 to 3; R 1 is independently at each occurrence a halogen atom, a C 1 -C 20 aliphatic radical, a C 5 -C 20 cycloaliphatic radical, or a C 2 -C 20 aromatic radical; R 2 is a halogen atom, a C 1 -C 20 aliphatic radical, a C 5 -C 20 cycloaliphatic radical, a C 2 -C 50 aromatic radical, or a polymer chain; and X - is a charge balancing counterion. In another embodiment, the present invention provides methodologies for the preparation of organophosphonium salts having structure (I).
摘要翻译：本发明涉及可用于制备有机粘土组合物，聚合物 - 有机粘土复合材料组合物和制备聚合物纳米复合材料的方法的有机盐组合物。在一个实施方案中，本发明提供了具有结构（I）的新型有机鏻盐，其中Ar 1，Ar 2和Ar 3独立地为C 芳香族基团; Ar 4是一个键或一个C 2 -C 50芳族基团; “a”是从1到大约200的数字; “c”是从0到3的数字; R 1在每次出现时独立地为卤素原子，C 1 -C 20脂族基团，C 5 H 12 -C 20脂环族基团或C 2 -C 20芳族基团; R 2是卤素原子，C 1 -C 20脂族基团，C 5 -C 5烷基， SUB 20脂环族基团，C 2 -C 20芳族基团或聚合物链; 而X - SUP是电荷平衡抗衡离子。在另一个实施方案中，本发明提供了具有结构（I）的有机鏻盐的制备方法。

7. 发明申请

WO2008002890A3 COMPOSITIONS AND METHODS FOR POLYMER COMPOSITES 审中-公开
标题翻译：聚合物复合材料的组合物和方法
公开(公告)号：WO2008002890A3
公开(公告)日：2008-03-27
申请号：PCT/US2007072072
申请日：2007-06-26
申请人： GEN ELECTRIC , CHAN KWOK PONG , CROLL JOSHUA MCCLELLAN , HAGBERG ERIK , MAXAM JOHN LESTER , MULLEN TARA J , ODLE ROY RAY , SUFFIELD RACHEL MARIE , WHITE JAMES MITCHELL , YAMAGUCHI NORIMITSU
发明人： CHAN KWOK PONG , CROLL JOSHUA MCCLELLAN , HAGBERG ERIK , MAXAM JOHN LESTER , MULLEN TARA J , ODLE ROY RAY , SUFFIELD RACHEL MARIE , WHITE JAMES MITCHELL , YAMAGUCHI NORIMITSU
IPC分类号： C08J3/20 , C08J5/10 , C08J5/18 , C08K3/34 , C08K5/18 , C08K5/19 , C08K5/3432 , C08K5/50 , C08K9/04 , C08L79/08
CPC分类号： C08J5/18 , C08J3/201 , C08J5/10 , C08J2379/08 , C08K3/346 , C08K5/18 , C08K5/19 , C08K5/3432 , C08K5/50 , C08K9/04
摘要： This invention relates to organic salt compositions useful in the preparation of organoclay compositions, polymer-organoclay composite compositions, and methods for the preparation of polymer nanocomposites. In one embodiment, the present invention provides a method of making a polymer-organoclay composite composition, said method comprising melt mixing a quaternary organoclay composition comprising alternating inorganic silicate layers and organic layers, said organic layers comprising a quaternary organic cation with a polyetherimide composition; said melt mixing being carried out at a temperature in a range between about 300°C and about 450°C to provide a polymer-organoclay composite composition, said polymer-organoclay composite composition being characterized by a percent exfoliation of at least 10 percent.
摘要翻译：本发明涉及可用于制备有机粘土组合物的有机盐组合物，聚合物 - 有机粘土复合组合物和用于制备聚合物纳米复合材料的方法。在一个实施方案中，本发明提供制备聚合物 - 有机粘土复合组合物的方法，所述方法包括熔融混合包含交替的无机硅酸盐层和有机层的季有机粘土组合物，所述有机层包含季聚有机阳离子和聚醚酰亚胺组合物; 所述熔融混合在约300℃至约450℃范围内的温度下进行以提供聚合物 - 有机粘土复合组合物，所述聚合物 - 有机粘土复合组合物的特征在于至少10％的百分比剥落。

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