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1. 发明公开

EP2812298A4 IMPROVED PROCESS FOR THE MANUFACTURE OF 2,3,3,3-TETRAFLUOROPROPENE 审中-公开
标题翻译：改进工艺用于生产2,3,3,3-四氟丙烯
公开(公告)号：EP2812298A4
公开(公告)日：2015-09-16
申请号：EP13746215
申请日：2013-02-08
申请人： WANG HAIYOU , TUNG HSUEH SUNG , KOPKALLI HALUK , CHIU YUON , CERRI GUSTAVO , BALL JEFFREY , DA PRATO PHILIP L , SUN XUEHUI , NAPPA MARIO JOSEPH
发明人： WANG HAIYOU , TUNG HSUEH SUNG , KOPKALLI HALUK , CHIU YUON , CERRI GUSTAVO , BALL JEFFREY , DA PRATO PHILIP L , SUN XUEHUI , NAPPA MARIO JOSEPH
IPC分类号： C07C17/20 , B01J23/755 , B01J27/08 , C07C17/06 , C07C17/087 , C07C17/25 , C07C17/383 , C07C17/386 , C07C17/389 , C07C19/10 , C07C21/18
CPC分类号： C07C17/395 , B01J27/08 , C07C17/06 , C07C17/087 , C07C17/23 , C07C17/25 , C07C17/386 , C07C17/389 , Y02P20/582 , C07C19/10 , C07C21/18
摘要： A method for forming 2,3,3,3-tetrafluoropropene (HFO-1234yf) comprising providing a dehydrochlorination starting material having relatively low concentrations of 2-chloro-3,3,3-trifluoropropene (HCFO-1233xf), especially and preferable less than about 8.0% when the dehydrochlorination reaction utilizes no substantial amount of catalyst or catalyst comprising austenitic nickel-based materials.

2. 发明公开

EP2812298A1 IMPROVED PROCESS FOR THE MANUFACTURE OF 2,3,3,3-TETRAFLUOROPROPENE 审中-公开
标题翻译：改进工艺用于生产2,3,3,3-四氟丙烯
公开(公告)号：EP2812298A1
公开(公告)日：2014-12-17
申请号：EP13746215.6
申请日：2013-02-08
申请人： Wang, Haiyou , Tung, Hsueh Sung , Kopkalli, Haluk , Chiu, Yuon , Cerri, Gustavo , Ball, Jeffrey , Da Prato, Philip L. , Sun, Xuehui , Nappa, Mario Joseph
发明人： Wang, Haiyou , Tung, Hsueh Sung , Kopkalli, Haluk , Chiu, Yuon , Cerri, Gustavo , Ball, Jeffrey , Da Prato, Philip L. , Sun, Xuehui , Nappa, Mario Joseph
IPC分类号： C07C17/20 , C07C17/383 , C07C21/18 , B01J23/755
CPC分类号： C07C17/395 , B01J27/08 , C07C17/06 , C07C17/087 , C07C17/23 , C07C17/25 , C07C17/386 , C07C17/389 , Y02P20/582 , C07C19/10 , C07C21/18
摘要： A method for forming 2,3,3,3-tetrafluoropropene (HFO-1234yf) comprising providing a dehydrochlorination starting material having relatively low concentrations of 2-chloro-3,3,3-trifluoropropene (HCFO-1233xf), especially and preferable less than about 8.0% when the dehydrochlorination reaction utilizes no substantial amount of catalyst or catalyst comprising austenitic nickel-based materials.

3. 发明专利

IN6917DEN2014A IMPROVED PROCESS FOR THE MANUFACTURE OF 2 3 3 3 TETRAFLUOROPROPENE 未知
公开(公告)号：IN6917DEN2014A
公开(公告)日：2015-05-15
申请号：IN6917DEN2014
申请日：2014-08-18
申请人： WANG HAIYOU , TUNG HSUEH S , KOPKALLI HALUK , CHIU YUON , CERRI GUSTAVO , BALL JEFFREY , DA PRATO PHILIP L , SUN XUEHUI , NAPPA MARIO JOSEPH
发明人： WANG HAIYOU , TUNG HSUEH S , KOPKALLI HALUK , CHIU YUON , CERRI GUSTAVO , BALL JEFFREY , DA PRATO PHILIP L , SUN XUEHUI , NAPPA MARIO JOSEPH
IPC分类号： C07C17/20 , C07C17/383 , C07C21/18
摘要： A method for forming 2 3 3 3 tetrafluoropropene (HFO 1234yf) comprising providing a dehydrochlorination starting material having relatively low concentrations of 2 chloro 3 3 3 trifluoropropene (HCFO 1233xf) especially and preferable less than about 8.0% when the dehydrochlorination reaction utilizes no substantial amount of catalyst or catalyst comprising austenitic nickel based materials.

4. 发明申请

WO2013119919A1 IMPROVED PROCESS FOR THE MANUFACTURE OF 2,3,3,3-TETRAFLUOROPROPENE 审中-公开
标题翻译：制备2,3,3,3-四氯丙烯的改进方法
公开(公告)号：WO2013119919A1
公开(公告)日：2013-08-15
申请号：PCT/US2013/025299
申请日：2013-02-08
申请人： WANG, Haiyou , TUNG, Hsueh S. , KOPKALLI, Haluk , CHIU, Yuon , CERRI, Gustavo , BALL, Jeffrey , DA PRATO, Philip L. , SUN, Xuehui , NAPPA, Mario Joseph
发明人： WANG, Haiyou , TUNG, Hsueh S. , KOPKALLI, Haluk , CHIU, Yuon , CERRI, Gustavo , BALL, Jeffrey , DA PRATO, Philip L. , SUN, Xuehui , NAPPA, Mario Joseph
IPC分类号： C07C17/20 , C07C17/383 , C07C21/18 , B01J23/755
CPC分类号： C07C17/395 , B01J27/08 , C07C17/06 , C07C17/087 , C07C17/23 , C07C17/25 , C07C17/386 , C07C17/389 , Y02P20/582 , C07C19/10 , C07C21/18
摘要： A method for forming 2,3,3,3-tetrafluoropropene (HFO-1234yf) comprising providing a dehydrochlorination starting material having relatively low concentrations of 2-chloro-3,3,3-trifluoropropene (HCFO-1233xf), especially and preferable less than about 8.0% when the dehydrochlorination reaction utilizes no substantial amount of catalyst or catalyst comprising austenitic nickel-based materials.
摘要翻译：一种形成2,3,3,3-四氟丙烯（HFO-1234yf）的方法，包括提供具有较低浓度的2-氯-3,3,3-三氟丙烯（HCFO-1233xf）的脱氯化氢原料，特别优选较少当脱氯化氢反应不使用显着量的包含奥氏体镍基材料的催化剂或催化剂时，约为8.0％。

5. 发明申请

WO2007058836A8 1,1,1,3,3,3-HEXAFLUOROPROPANE PURIFICATION WITH PHOTOCHLORINATION EQUIPMENT 审中-公开
标题翻译： 1,1,1,3,3,3-HEXAFLORORROPANE用光电设备进行纯化
公开(公告)号：WO2007058836A8
公开(公告)日：2008-08-14
申请号：PCT/US2006043417
申请日：2006-11-08
申请人： HONEYWELL INT INC , CHIU YUON , MERKEL DAVID , TUNG HSUEH SUNG
发明人： CHIU YUON , MERKEL DAVID , TUNG HSUEH SUNG
IPC分类号： C07C17/395 , C07C19/08
CPC分类号： C07C17/38 , C07C17/395 , C07C19/08
摘要： A continuous, vapor phase method for purifying a crude mixture of 1,1,1,3,3,3-hexafluoropropane and one or more unsaturated fluorocarbon compounds, the process comprising: a) providing a photochlorinator vessel comprising : 1) a UV lamp unit comprising a UV lamp located in a transparent inner well, the transparent inner well being located within a transparent outer well, the outer well being provided with material for cooling walls of the inner and outer wells; the inner well and the outer well defining separate chambers isolated from each other; and 2) a reaction vessel into which the UV lamp unit has been inserted; b) introducing into the reaction vessel a gaseous mixture of Cb and a distillation inseparable mixture of 1,1,1,3,3,3-hexafluoropropane and one or more unsaturated fluorocarbon compdunds; c) reacting, in the gaseous state and in the presence of UV light from the photochlorinator, the mixture with CI 2 with the distillation inseparable mixture of 1,1,1,3,3,3-hexafluoropropane and one or more unsaturated compounds to saturate unsaturated fluorocarbons into a reacted mixture, and d) separating a purified 1, 1,1, 3,3, 3-hexafluoroporpane product containing less than 1000 ppm, most preferably less than 100 ppm unsaturated fluorocarbons.
摘要翻译：一种用于纯化1,1,1,3,3,3-六氟丙烷和一种或多种不饱和碳氟化合物的粗混合物的连续气相法，该方法包括：a）提供光氯化器容器，其包括：1）UV灯该单元包括位于透明内部井中的UV灯，所述透明内部井位于透明外部井内，所述外部井具有用于冷却所述内部和外部井的壁的材料; 所述内部井和所述外部井定义分离的彼此隔离的室; 和2）UV灯单元插入其中的反应容器; b）向反应容器中引入Cb的气态混合物和1,1,1,3,3,3-六氟丙烷与一种或多种不饱和氟碳化合物的蒸馏不可分离的混合物; c）以气态和在来自光氯提取器的紫外光的存在下，与CI 2的混合物与1,1,1,3,3,3-六氟丙烷的蒸馏不可分离的混合物反应和一种或多种使不饱和碳氟化合物饱和至反应混合物中的不饱和化合物，和d）分离含有小于1000ppm，最优选小于100ppm的不饱和碳氟化合物的纯化1,1,1,3,3,3-六氟丙烷产物。

6. 发明申请

WO2003002251A2 PROCESS FOR PREPARING FLUORINATION CATALYST 审中-公开
标题翻译：制备荧光催化剂的方法
公开(公告)号：WO2003002251A2
公开(公告)日：2003-01-09
申请号：PCT/US2002/020563
申请日：2002-06-28
申请人： HONEYWELL INTERNATIONAL, INC. , TUNG, Hsueh, Sung , STUCK, Jason, T. , CHIU, Yuon , CERRI, Gustavo
发明人： TUNG, Hsueh, Sung , STUCK, Jason, T. , CHIU, Yuon , CERRI, Gustavo
IPC分类号： B01J20/34
CPC分类号： C07C17/206 , B01J23/26 , B01J27/132 , B01J37/26 , C07B39/00 , C07C17/10 , C07C17/21 , C07C19/08
摘要： A process for preparing a fluorination catalyst using a low pressure activating step followed by a high pressure activating step.
摘要翻译：一种使用低压活化步骤随后进行高压活化步骤制备氟化催化剂的方法。

7. 发明申请

WO2012099776A1 METHODS OF MAKING 2,3,3,3-TETRAFLUORO-2-PROPENE 审中-公开
标题翻译：制备2,3,3,3-四氢-2-丙烯的方法
公开(公告)号：WO2012099776A1
公开(公告)日：2012-07-26
申请号：PCT/US2012/021158
申请日：2012-01-13
申请人： HONEYWELL INTERNATIONAL INC. , COTTRELL, Stephen A. , CHIU, Yuon , KOPKALLI, Haluk , TUNG, Hsueh Sung , UHRICH, Kevin D. , SCHEIDLE, Peter
发明人： COTTRELL, Stephen A. , CHIU, Yuon , TUNG, Hsueh Sung , UHRICH, Kevin D. , SCHEIDLE, Peter
IPC分类号： C07C17/25 , C07C21/18 , C07C17/38 , B01J23/18
CPC分类号： C07C17/21 , C07C17/087 , C07C17/206 , C07C17/25 , C07C17/38 , C07C17/383 , C07C19/10 , C07C21/18
摘要： Disclosed is a process for the manufacture of 1234yf from 1,1,2,3-tetrachloro-propene, abbreviated herein as "TCP," in three integrated steps: (a) the R-1 hydrofluorination of TCP to form 1233xf in the vapor phase; (b) the R-2 hydrofluorination of 1233xf to form 244bb in either the liquid phase or in the liquid phase followed by the vapor phase; and (c) the R-3 dehydrochlorination of the 244bb in either the liquid or the vapor phase to produce 1234yf; wherein the vapor phase hydrofluorination of TCP in step (a) is carried out at a lower pressure than the liquid phase hydrofluorination of 123xf; and wherein the HCl generated during these steps is scrubbed with water to form an acid solution and the organic components are scrubbed with a caustic solution and then dried before further processing.
摘要翻译：本发明公开了一种从1,1,2,3-四氯丙烯（本文缩写为“TCP”）制备1234yf的方法，三个一体化步骤：（a）TCP的R-1氢氟化在蒸气中形成1233xf 相; （b）1233xf的R-2氢氟化在液相或液相中形成244bb，随后是气相; 和（c）244bb在液相或气相中的R-3脱氯化氢以产生1234yf; 其中步骤（a）中TCP的气相氢氟化在比123xf的液相氢氟化更低的压力下进行; 并且其中在这些步骤期间产生的HCl用水洗涤以形成酸溶液，并且用苛性碱溶液洗涤有机组分，然后在进一步加工之前干燥。

8. 发明申请

WO2011056441A3 INTEGRATED PROCESS FOR FLUORO-OLEFIN PRODUCTION 审中-公开
标题翻译：氟 - 烯烃生产的集成工艺
公开(公告)号：WO2011056441A3
公开(公告)日：2011-09-15
申请号：PCT/US2010053486
申请日：2010-10-21
申请人： HONEYWELL INT INC , KOPKALLI HALUK , CHIU YUON , COTTRELL STEPHEN A , TUNG HSUEH SUNG , ULRICH KEVIN D
发明人： KOPKALLI HALUK , CHIU YUON , COTTRELL STEPHEN A , TUNG HSUEH SUNG , ULRICH KEVIN D
IPC分类号： C07C17/20 , C07C17/25 , C07C21/18 , C09K5/02
CPC分类号： C07C21/18 , C01B7/0718 , C01B7/0737 , C01B7/195 , C07C17/087 , C07C17/10 , C07C17/206 , C07C17/25 , Y02P20/125 , C07C19/10
摘要： Disclosed is a process for the manufacture of HFO-1234yf from TCP in three integrated steps that include hydrofluorination of TCP (tetrachloropropene) to HCFC-1233xf in the vapor phase followed by hydrofluorination of HCFC-1233xf to HCFC-244bb in the liquid phase which is then followed by dehydrochlorination in liquid or vapor phase to produce HFO-1234yf. The vapor phase hydrofluorination is carried out at a higher pressure than the liquid phase hydrofluorination, thereby eliminating the need for compression and/or intermediate recovery. Also, any HCl generated from this reaction is fed to the liquid phase hydrofluorination section to promote agitation and mixing. This results in a more economical process from an initial capital and operating cost versus conducting the 3-steps sequentially.
摘要翻译：公开了一种由TCP以三个整合步骤制造HFO-1234yf的方法，其包括在气相中将TCP（四氯丙烯）氢氟化为HCFC-1233xf，接着在液相中将HCFC-1233xf氢氟化为HCFC-244bb 然后在液相或汽相中进行脱氯化氢反应，生成HFO-1234yf。气相氢氟化在比液相氢氟化更高的压力下进行，由此消除了压缩和/或中间回收的需要。而且，由该反应产生的任何HCl被供给到液相氢氟化部分以促进搅拌和混合。这从最初的资本和运营成本中获得了更经济的过程，而不是依次进行3个步骤。

9. 发明申请

WO03002251A3 PROCESS FOR PREPARING FLUORINATION CATALYST 审中-公开
标题翻译：制备氟化催化剂的方法
公开(公告)号：WO03002251A3
公开(公告)日：2003-02-27
申请号：PCT/US0220563
申请日：2002-06-28
申请人： HONEYWELL INT INC , TUNG HSUEH SUNG , STUCK JASON T , CHIU YUON , CERRI GUSTAVO
发明人： TUNG HSUEH SUNG , STUCK JASON T , CHIU YUON , CERRI GUSTAVO
IPC分类号： B01J38/46 , B01J23/26 , B01J27/132 , B01J37/26 , C07B39/00 , C07B61/00 , C07C17/087 , C07C17/10 , C07C17/20 , C07C17/21 , C07C19/08 , B01J20/34 , B01J23/00 , B01J23/40 , B01J23/42 , B01J23/70 , B01J23/74
CPC分类号： C07C17/206 , B01J23/26 , B01J27/132 , B01J37/26 , C07B39/00 , C07C17/10 , C07C17/21 , C07C19/08
摘要： A process for preparing a fluorination catalyst using a low pressure activating step followed by a high pressure activating step.
摘要翻译：一种使用低压活化步骤然后进行高压活化步骤来制备氟化催化剂的方法。

10. 发明申请

WO2011056441A2 INTEGRATED PROCESS FOR FLUORO-OLEFIN PRODUCTION 审中-公开
标题翻译：氟油生产的综合工艺
公开(公告)号：WO2011056441A2
公开(公告)日：2011-05-12
申请号：PCT/US2010/053486
申请日：2010-10-21
申请人： HONEYWELL INTERNATIONAL INC. , KOPKALLI, Haluk , CHIU, Yuon , COTTRELL, Stephen, A. , TUNG, Hsueh Sung , ULRICH, Kevin D.
发明人： KOPKALLI, Haluk , CHIU, Yuon , COTTRELL, Stephen, A. , TUNG, Hsueh Sung , ULRICH, Kevin D.
IPC分类号： C07C17/20 , C07C17/25 , C07C21/18 , C09K5/02
CPC分类号： C07C21/18 , C01B7/0718 , C01B7/0737 , C01B7/195 , C07C17/087 , C07C17/10 , C07C17/206 , C07C17/25 , Y02P20/125 , C07C19/10
摘要： Disclosed is a process for the manufacture of HFO-1234yf from TCP in three integrated steps that include hydrofluorination of TCP (tetrachloropropene) to HCFC-1233xf in the vapor phase followed by hydrofluorination of HCFC-1233xf to HCFC-244bb in the liquid phase which is then followed by dehydrochlorination in liquid or vapor phase to produce HFO-1234yf. The vapor phase hydrofluorination is carried out at a higher pressure than the liquid phase hydrofluorination, thereby eliminating the need for compression and/or intermediate recovery. Also, any HCl generated from this reaction is fed to the liquid phase hydrofluorination section to promote agitation and mixing. This results in a more economical process from an initial capital and operating cost versus conducting the 3-steps sequentially.
摘要翻译：公开了一种从TCP制造HFO-1234yf的方法，其包括在气相中将TCP（四氯丙烯）氢氟化为HCFC-1233xf，然后在液相中HCFC-1233xf氢氟化为HCFC-244bb的三个整合步骤然后在液相或汽相中进行脱氯化氢以产生HFO-1234yf。气相氢氟化在比液相氢氟化更高的压力下进行，从而不需要压缩和/或中间回收。此外，将由该反应生成的任何HCl进料到液相氢氟化部分以促进搅拌和混合。这导致了从初始资本和运营成本的更经济的过程，而不是依次执行3个步骤。

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