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1. 发明授权

US08435400B2 Systems and methods for producing a crude product 有权
标题翻译：用于生产粗产品的系统和方法
公开(公告)号：US08435400B2
公开(公告)日：2013-05-07
申请号：US13103790
申请日：2011-05-09
申请人： Bo Kou , Shuwu Yang , Bruce Reynolds , Julie Chabot
发明人： Bo Kou , Shuwu Yang , Bruce Reynolds , Julie Chabot
IPC分类号： C10G65/10
CPC分类号： C10G47/02 , C10G47/26 , C10G47/32 , C10G65/02 , C10G65/10 , C10G65/18 , C10G2300/1044 , C10G2300/107 , C10G2300/1074 , C10G2300/1077 , C10G2300/4081 , C10G2300/44 , C10G2300/80 , C10G2300/805
摘要： Systems and methods for hydroprocessing heavy oil feedstock is disclosed. The process employs a plurality of contacting zones and at least a separation zone to convert at least a portion of the heavy oil feedstock to lower boiling hydrocarbons, forming upgraded products. In one embodiment, water and/or steam being injected into at least a contacting zone. The contacting zones operate under hydrocracking conditions, employing at least a slurry catalyst. In one embodiment, at least a portion of the non-volatile fractions recovered from at least one of the separation zones is recycled back to at least a contacting zone (“recycled mode”). In one embodiment, the number of separation zones is less than the number of contacting zones in the system. In the separation zones, upgraded products are removed overhead and optionally treated in an in-line hydrotreater; and the bottom stream is optionally further treated in a fractionator.
摘要翻译：公开了用于加氢处理重油原料的系统和方法。该方法采用多个接触区和至少一个分离区，将至少一部分重油原料转化成低沸点烃，形成升级产物。在一个实施方案中，将水和/或蒸汽注入至少一个接触区。接触区在加氢裂化条件下运行，至少使用浆料催化剂。在一个实施方案中，从至少一个分离区回收的至少一部分非挥发性馏分被再循环回至少一个接触区（“再循环模式”）。在一个实施例中，分离区的数量小于系统中接触区的数量。在分离区中，升级后的产品被顶部除去并任选地在直列加氢处理器中处理; 并且底部物流任选地在分馏器中进一步处理。

2. 发明申请

US20120315202A1 APPARATUS AND METHOD FOR HYDROCONVERSION 审中-公开
标题翻译：装置和方法
公开(公告)号：US20120315202A1
公开(公告)日：2012-12-13
申请号：US13162742
申请日：2011-06-17
申请人： Steven X. Song , Donald L. Kuehne , Abdenour Kemoun , Bruce Reynolds
发明人： Steven X. Song , Donald L. Kuehne , Abdenour Kemoun , Bruce Reynolds
IPC分类号： B01J8/44
CPC分类号： B01J8/06 , B01J8/005 , B01J8/007 , B01J8/1827 , B01J8/22 , B01J8/226 , B01J8/44 , B01J2208/00176 , B01J2208/00929 , B01J2208/025 , B01J2208/026 , B01J2219/0004 , C10G45/02 , C10G45/16 , C10G45/22 , C10G47/26 , C10G49/12
摘要： An apparatus is disclosed for the hydroconversion of hydrocarbon feedstock with a hydrogen gas at elevated temperature and pressure with the use of a catalyst. The apparatus is a reactor vessel with a grid plate distributor for improved gas liquid distribution. The distributor comprises a grid plate and a bubble cap assembly with a plurality of tubular risers extending through the grid plate. Each tubular riser has an upper section above the grid plate and a lower section below the grid plate, the lower section terminated with an open bottom end for ingress of the hydrogen gas and hydrocarbon feedstock, the upper section having a closed top terminated with a housing cap. Each tubular riser has at least a vertical slot and a least a side hole sufficiently sized such that in operation, the liquid level in the zone below the grid plate is above the vertical slot and below the side hole opening.
摘要翻译：公开了一种使用催化剂在升高的温度和压力下用氢气加氢转化烃原料的装置。该装置是具有用于改善气体液体分布的格栅分配器的反应器容器。分配器包括格栅板和气泡盖组件，其具有延伸穿过格栅板的多个管状立管。每个管状提升管具有在格栅板上方的上部部分和在格栅板下方的下部分，下部部分终止于用于进入氢气和烃原料的开口底端，上部部分具有封闭的顶部，其与壳体帽。每个管状提升管具有至少一个垂直狭槽和至少一个足够大小的侧孔，使得在操作中，格栅板下方的区域中的液位高于垂直槽并在侧孔开口下方。

3. 发明授权

US07943036B2 Systems and methods for producing a crude product 有权
标题翻译：用于生产粗产品的系统和方法
公开(公告)号：US07943036B2
公开(公告)日：2011-05-17
申请号：US12506885
申请日：2009-07-21
申请人： Darush Farshid , Bruce Reynolds
发明人： Darush Farshid , Bruce Reynolds
IPC分类号： C10G47/00
CPC分类号： C10G65/18 , C10G47/02 , C10G47/26 , C10G47/32 , C10G65/02 , C10G65/10
摘要： A flexible once-through process for hydroprocessing heavy oil feedstock is disclosed. The process employs a plurality of contacting zones and at least a separation zone to convert at least a portion of the heavy oil feedstock to lower boiling hydrocarbons, forming upgraded products. The contacting zones operate under hydrocracking conditions, employing a slurry catalyst for upgrading the heavy oil feedstock. The plurality of contacting zones and separation zones are configured in a permutable fashion allowing the once-through process to be flexible operating in various modes: a sequential mode; a parallel mode; a combination of parallel and sequential mode; all online; some online and some on stand-by; some online and some off-line; a parallel mode with the effluent stream from the contacting zone being sent to at least a separation zone in series with the contacting zone; a parallel mode with the effluent stream from the contacting zone being combined with an effluent stream from at least another contacting zone and sent to the separation zone; and combinations thereof.
摘要翻译：公开了用于加氢处理重油原料的灵活的一次性方法。该方法采用多个接触区和至少一个分离区，将至少一部分重油原料转化成低沸点烃，形成升级产物。接触区在加氢裂化条件下运行，使用用于升级重油原料的浆料催化剂。多个接触区域和分离区域被配置成可替换的方式，使得直通过程能够以各种模式灵活地操作：顺序模式; 并行模式; 并行和顺序模式的组合; 所有在线一些在线和一些待机; 一些在线和一些离线; 与来自接触区的流出物流的并行模式被传送到与接触区串联的至少一个分离区; 来自接触区域的流出物流与来自至少另一个接触区域的流出物流的并行模式组合并被送至分离区域; 及其组合。

4. 发明申请

US20110017638A1 Systems and Methods for Producing a Crude Product 有权
标题翻译：生产原油产品的系统和方法
公开(公告)号：US20110017638A1
公开(公告)日：2011-01-27
申请号：US12506885
申请日：2009-07-21
申请人： Darush Farshid , Bruce Reynolds
发明人： Darush Farshid , Bruce Reynolds
IPC分类号： C10G47/00
CPC分类号： C10G65/18 , C10G47/02 , C10G47/26 , C10G47/32 , C10G65/02 , C10G65/10
摘要： A flexible once-through process for hydroprocessing heavy oil feedstock is disclosed. The process employs a plurality of contacting zones and at least a separation zone to convert at least a portion of the heavy oil feedstock to lower boiling hydrocarbons, forming upgraded products. The contacting zones operate under hydrocracking conditions, employing a slurry catalyst for upgrading the heavy oil feedstock. The plurality of contacting zones and separation zones are configured in a permutable fashion allowing the once-through process to be flexible operating in various modes: a sequential mode; a parallel mode; a combination of parallel and sequential mode; all online; some online and some on stand-by; some online and some off-line; a parallel mode with the effluent stream from the contacting zone being sent to at least a separation zone in series with the contacting zone; a parallel mode with the effluent stream from the contacting zone being combined with an effluent stream from at least another contacting zone and sent to the separation zone; and combinations thereof.
摘要翻译：公开了用于加氢处理重油原料的灵活的一次性方法。该方法采用多个接触区和至少一个分离区，将至少一部分重油原料转化成低沸点烃，形成升级产物。接触区在加氢裂化条件下运行，使用用于升级重油原料的浆料催化剂。多个接触区域和分离区域被配置成可替换的方式，使得直通过程能够以各种模式灵活地操作：顺序模式; 并行模式; 并行和顺序模式的组合; 所有在线一些在线和一些待机; 一些在线和一些离线; 与来自接触区的流出物流的并行模式被传送到与接触区串联的至少一个分离区; 来自接触区域的流出物流与来自至少另一个接触区域的流出物流的并行模式组合并被送至分离区域; 及其组合。

5. 发明申请

US20110017635A1 Systems and Methods for Producing a Crude Product 有权
标题翻译：生产原油产品的系统和方法
公开(公告)号：US20110017635A1
公开(公告)日：2011-01-27
申请号：US12506840
申请日：2009-07-21
申请人： Julie Chabot , Shuwu Yang , Bruce Reynolds
发明人： Julie Chabot , Shuwu Yang , Bruce Reynolds
IPC分类号： C10G65/10 , C10G47/02 , C10G65/18
CPC分类号： C10G47/32 , C10G47/02 , C10G47/26 , C10G65/00 , C10G65/10 , C10G65/18
摘要： A process for hydroprocessing heavy oil feedstock is disclosed. The process operates in once-through mode, employing a plurality of contacting zones and at least a separation zone to convert at least a portion of the heavy oil feedstock to lower boiling hydrocarbons, forming upgraded products. In the once-through upgrade system, little if any of the unconverted material and slurry catalyst mixture is recycled back to the system for further upgrading. The contacting zones operate under hydrocracking conditions, employing a slurry catalyst for upgrading the heavy oil feedstock. The slurry catalyst feed comprises an active metal catalyst having an average particle size of at least 1 micron in a hydrocarbon oil diluent, at a concentration of greater than 500 wppm of active metal catalyst to heavy oil feedstock.
摘要翻译：公开了一种加氢处理重油原料的方法。该方法以一次通过模式运行，采用多个接触区和至少一个分离区，将至少一部分重油原料转化成低沸点烃，形成升级产物。在一次性升级系统中，很少将未转化的材料和浆料催化剂混合物再循环回系统进行进一步升级。接触区在加氢裂化条件下运行，使用用于升级重油原料的浆料催化剂。浆料催化剂进料包含在烃油稀释剂中平均粒度至少为1微米的活性金属催化剂，其浓度大于500wppm的活性金属催化剂与重油原料。

6. 发明申请

US20100234212A1 HYDROPROCESSING BULK CATALYST AND USES THEREOF 有权
标题翻译：氢化聚合物催化剂及其用途
公开(公告)号：US20100234212A1
公开(公告)日：2010-09-16
申请号：US12787855
申请日：2010-05-26
申请人： Axel Brait , Alexander E. Kuperman , Jaime Lopez , Oleg Mironov , Bruce Reynolds , Kaidong Chen
发明人： Axel Brait , Alexander E. Kuperman , Jaime Lopez , Oleg Mironov , Bruce Reynolds , Kaidong Chen
IPC分类号： B01J31/02
CPC分类号： C10G47/04 , B01J23/24 , B01J23/28 , B01J23/85 , B01J23/882 , B01J23/883 , B01J23/8885 , B01J27/0515 , B01J35/002 , B01J35/023 , B01J35/1009 , B01J35/1014 , B01J35/1042 , B01J35/1047 , B01J37/0236 , B01J37/031 , B01J37/038 , B01J37/04 , B01J37/16 , B01J37/20 , B01J37/343 , C10G47/06 , C10G49/04 , C10G2300/107 , C10G2300/1077 , Y10S502/517
摘要： A hydroprocessing bulk catalyst is provided. A process to prepare hydroprocessing bulk catalysts is also provided. The hydroprocessing catalyst has the formula (Mt)a(Lu)b(Sv)d(Cw)e(Hx)f(Oy)g(Nz)h,, wherein M is at least one group VIII metal; promoter metal L is optional and if present, L is at least one Group VIII non-noble metal; t, u, v, w, x, y, z representing the total charge for each of the components (M, L, S, C, H, O and N, respectively); ta+ub+vd+we+xf+yg+zh=0; 0=
摘要翻译：提供加氢处理体积催化剂。还提供了制备加氢处理大量催化剂的方法。加氢处理催化剂具有式（Mt）a（Lu）b（Sv）d（Cw）e（Hx）f（Oy）g（Nz）h ,,其中M是至少一种VIII族金属; 促进剂金属L是任选的，如果存在，L是至少一种第VIII族非贵金属; 表示各组分（M，L，S，C，H，O和N分别）的总电荷的t，u，v，w，x，y，z; ta + ub + vd + we + xf + yg + zh = 0; 0 =

7. 发明授权

US07737072B2 Hydroprocessing bulk catalyst and uses thereof 有权
标题翻译：加氢处理本体催化剂及其用途
公开(公告)号：US07737072B2
公开(公告)日：2010-06-15
申请号：US11931972
申请日：2007-10-31
申请人： Oleg Mironov , Alexander E. Kuperman , Jaime Lopez , Axel Brait , Bruce Reynolds , Kaidong Chen
发明人： Oleg Mironov , Alexander E. Kuperman , Jaime Lopez , Axel Brait , Bruce Reynolds , Kaidong Chen
IPC分类号： B01J21/00 , B01J31/00 , B01J27/24 , B01J27/04
CPC分类号： B01J27/049 , B01J27/0515 , B01J35/002 , B01J35/023 , B01J37/03 , B01J37/20 , C10G45/04 , C10G45/08 , C10G45/50 , C10G49/02 , C10G49/04 , Y10S502/517
摘要： A hydroprocessing catalyst is provided. The hydroprocessing catalyst has the formula (Mt)a(Xu)b(Sv)d(Cw)e(Hx)f(Oy)g(Nz)h, wherein M is at least one group VIB metal; X is at least one Group VIII non-noble metal; t, u, v, w, x, y, z representing the total charge for each of the components (M, X, S, C, H, O and N, respectively); ta+ub+vd+we+xf+yg+zh=0; and 0=
摘要翻译：提供加氢处理催化剂。加氢处理催化剂具有式（Mt）a（Xu）b（Sv）d（Cw）e（Hx）f（Oy）g（Nz）h，其中M为至少一种VIB族金属; X是至少一种第VIII族非贵金属; 表示各组分（M，X，S，C，H，O和N分别）的总电荷的t，u，v，w，x，y，z; ta + ub + vd + we + xf + yg + zh = 0; 并且0 =

8. 发明申请

US20090159505A1 HEAVY OIL UPGRADE PROCESS INCLUDING RECOVERY OF SPENT CATALYST 有权
标题翻译：重油提升过程，包括回收催化剂
公开(公告)号：US20090159505A1
公开(公告)日：2009-06-25
申请号：US12346480
申请日：2008-12-30
申请人： Andre R. Da Costa , Bruce Reynolds , Christopher A. Powers , Seyi A. Odueyungbo
发明人： Andre R. Da Costa , Bruce Reynolds , Christopher A. Powers , Seyi A. Odueyungbo
IPC分类号： C10G31/09
CPC分类号： C10G31/09 , C10G67/02
摘要： A process to upgrade heavy oil and convert the heavy oil into lower boiling hydrocarbon products is provided. The process employs a catalyst slurry comprising catalyst particles with an average particle size ranging from 1 to 20 microns. In the upgrade process, spent slurry catalyst in heavy oil is generated as an effluent stream, which is subsequently recovered/separated from the heavy oil via a filtration assembly. The filtration assembly has a least a filtration unit employing at least a membrane for separating heavy oil from the catalyst particles. Valuable metals can be recovered from catalyst particles for subsequent re-use in a catalyst synthesis unit, generating a fresh slurry catalyst.
摘要翻译：提供了将重油升级并将重油转化为低沸点烃产品的方法。该方法采用包含平均粒度为1至20微米的催化剂颗粒的催化剂浆料。在升级过程中，将废液中的废浆催化剂作为流出物流产生，随后通过过滤组件从重油中回收/分离。过滤组件具有至少一个使用至少一个用于从催化剂颗粒分离重油的膜的过滤单元。可以从催化剂颗粒中回收有价值的金属，以便随后在催化剂合成装置中再次使用，产生新的浆料催化剂。

9. 发明授权

US07431831B2 Integrated in-line pretreatment and heavy oil upgrading process 有权
标题翻译：综合在线预处理和重油升级过程
公开(公告)号：US07431831B2
公开(公告)日：2008-10-07
申请号：US11305378
申请日：2005-12-16
申请人： Darush Farshid , Bruce Reynolds
发明人： Darush Farshid , Bruce Reynolds
IPC分类号： C10B57/02 , C10G51/02
CPC分类号： C10G47/26 , C10G47/14 , C10G65/10 , C10G65/12
摘要： A new residuum full hydroconversion slurry reactor system has been developed that allows the catalyst, unconverted oil, products and hydrogen to circulate in a continuous mixture throughout an entire reactor with no confinement of the mixture. The mixture is partially separated in between the reactors to remove only the products and hydrogen while permitting the unconverted oil and the slurry catalyst to continue on into the next sequential reactor. In the next reactor, a portion of the unconverted oil is converted to lower boiling point hydrocarbons, once again creating a mixture of unconverted oil, products, hydrogen and slurry catalyst. Further hydroprocessing may occur in additional reactors, fully converting the oil. The oil may alternately be partially converted, leaving a highly concentrated catalyst in unconverted oil which can be recycled directly to the first reactor. The slurry reactor system is, in this invention, preceded by an in-line pretreating step, such as hydrotreating or deasphalting. Following the slurry reactor system, fully converted oil may be subsequently hydrofinished for the removal of hetoroatoms such as sulfur and nitrogen.
摘要翻译：已经开发了一种新的残渣全加氢转化淤浆反应器系统，其允许催化剂，未转化的油，产物和氢气在连续混合物中在整个反应器中循环，而不限制混合物。混合物在反应器之间部分分离，以仅去除产物和氢气，同时允许未转化的油和浆料催化剂继续进入下一个顺序的反应器。在下一个反应器中，未转化的油的一部分转化为低沸点烃，再次产生未转化的油，产物，氢气和浆料催化剂的混合物。进一步的加氢处理可能发生在额外的反应器中，完全转化油。油可以部分地转化，留下高度浓缩的催化剂在未转化的油中，其可以直接再循环到第一反应器。在本发明中，浆料反应器系统之前是在线预处理步骤，例如加氢处理或脱沥青。在浆料反应器系统之后，随后可以将完全转化的油加氢处理以除去诸如硫和氮的氢原子。

10. 发明授权

US07431823B2 Process for upgrading heavy oil using a highly active slurry catalyst composition 有权
标题翻译：使用高活性浆料催化剂组合物对重油进行改质的方法
公开(公告)号：US07431823B2
公开(公告)日：2008-10-07
申请号：US11305377
申请日：2005-12-16
申请人： Darush Farshid , Bruce Reynolds
发明人： Darush Farshid , Bruce Reynolds
IPC分类号： C10B57/02 , C10G51/02
CPC分类号： C10G49/12 , C10G65/02
摘要： The instant invention is directed to a new residuum full hydroconversion slurry reactor system that allows the catalyst, unconverted oil and converted oil to circulate in a continuous mixture throughout an entire reactor with no confinement of the mixture. The mixture is partially separated in between the reactors to remove only the products and hydrogen, while permitting the unconverted oil and the slurry catalyst to continue on into the next sequential reactor where a portion of the unconverted oil is converted to lower boiling point hydrocarbons, once again creating a mixture of unconverted oil, converted oil, and slurry catalyst. Further hydroprocessing may occur in additional reactors, fully converting the oil. The oil may alternately be partially converted, leaving a highly concentrated catalyst in unconverted oil which can be recycled directly to the first reactor.
摘要翻译：本发明涉及一种新的残渣全加氢转化淤浆反应器系统，其允许催化剂，未转化的油和转化油在连续混合物中在整个反应器中循环，而不限制混合物。混合物在反应器之间部分分离以除去产物和氢气，同时允许未转化的油和浆料催化剂继续进入下一个顺序的反应器，其中一部分未转化的油转化为低沸点烃，一次再次产生未转化的油，转化油和浆料催化剂的混合物。进一步的加氢处理可能发生在额外的反应器中，完全转化油。油可以部分地转化，留下高度浓缩的催化剂在未转化的油中，其可以直接再循环到第一反应器。

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