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1. 发明授权

US07396381B2 Storage and delivery systems for gases held in liquid medium 失效
标题翻译：保存在液体介质中的气体的储存和输送系统
公开(公告)号：US07396381B2
公开(公告)日：2008-07-08
申请号：US10887561
申请日：2004-07-08
申请人： David Ross Graham , Daniel Joseph Tempel , Bernard Allen Toseland , Philip Bruce Henderson , James Joseph Hart , John Bruce Appleby , Jeffrey Richard Brzozowski , Pushpinder Singh Puri
发明人： David Ross Graham , Daniel Joseph Tempel , Bernard Allen Toseland , Philip Bruce Henderson , James Joseph Hart , John Bruce Appleby , Jeffrey Richard Brzozowski , Pushpinder Singh Puri
IPC分类号： F17C11/00 , B01D19/00
CPC分类号： F17C11/00
摘要： The present invention is directed to improvements in storage and delivery systems that allow for rapid fill and delivery of gases reversibly stored in a nonvolatile liquid medium, improvements in delivery and purity of the delivered gas. The low pressure storage and delivery system for gas which comprises:a container having an interior portion containing a reactive Lewis basic or Lewis acidic reactive liquid medium that is reversibly reacted with a gas having opposing Lewis acidity or basicity; a system for transferring energy into or out of the reactive liquid medium; or, a product gas purifier (e.g. a gas/liquid separator); or both.
摘要翻译：本发明涉及储存和输送系统的改进，其允许可逆地储存在非挥发性液体介质中的气体的快速填充和输送，输送气体的输送和纯度的改善。用于气体的低压储存和输送系统包括：容器，其具有含有反应性路易斯碱性或路易斯酸性反应性液体介质的内部部分，其与具有相反路易斯酸度或碱度的气体可逆地反应; 用于将能量转移到或流出反应性液体介质的系统; 或产品气体净化器（例如气/液分离器）; 或两者。

2. 发明授权

US07485161B2 Dehydrogenation of liquid fuel in microchannel catalytic reactor 有权
标题翻译：微通道催化反应器中液体燃料的脱氢
公开(公告)号：US07485161B2
公开(公告)日：2009-02-03
申请号：US11029059
申请日：2005-01-04
申请人： Bernard Allen Toseland , Guido Peter Pez , Pushpinder Singh Puri
发明人： Bernard Allen Toseland , Guido Peter Pez , Pushpinder Singh Puri
IPC分类号： B01J7/00 , B01J8/04 , B01J19/00 , C01B6/00
CPC分类号： H01M8/065 , B01J19/0093 , B01J2219/00783 , B01J2219/00835 , B01J2219/0086 , B01J2219/00867 , B01J2219/00873 , B01J2219/00891 , B01J2219/00905 , B01J2219/00997 , C01B3/0015 , C07C5/32 , C07C5/327 , Y02E60/328 , Y02P20/129
摘要： The present invention is an improved process for the storage and delivery of hydrogen by the reversible hydrogenation/dehydrogenation of an organic compound wherein the organic compound is initially in its hydrogenated state. The improvement in the route to generating hydrogen is in the dehydrogenation step and recovery of the dehydrogenated organic compound resides in the following steps: introducing a hydrogenated organic compound to a microchannel reactor incorporating a dehydrogenation catalyst; effecting dehydrogenation of said hydrogenated organic compound under conditions whereby said hydrogenated organic compound is present as a liquid phase; generating a reaction product comprised of a liquid phase dehydrogenated organic compound and gaseous hydrogen; separating the liquid phase dehydrogenated organic compound from gaseous hydrogen; and, recovering the hydrogen and liquid phase dehydrogenated organic compound.
摘要翻译：本发明是通过可逆氢化/脱氢有机化合物的储存和输送氢的改进方法，其中有机化合物最初处于其氢化状态。生成氢气的途径的改进是脱氢步骤，脱氢有机化合物的回收步骤如下：将氢化有机化合物引入到包含脱氢催化剂的微通道反应器中; 所述氢化有机化合物在所述氢化有机化合物作为液相存在的条件下进行脱氢; 产生由液相脱氢有机化合物和气态氢组成的反应产物; 将液相脱氢有机化合物与气态氢分离; 并回收氢和液相脱氢的有机化合物。

3. 发明申请

US20090019768A1 Dehydrogenation of Liquid Fuel in Microchannel Catalytic Reactor 有权
标题翻译：液态燃料在微通道催化反应器中脱氢
公开(公告)号：US20090019768A1
公开(公告)日：2009-01-22
申请号：US12211585
申请日：2008-09-16
申请人： Bernard Allen Toseland , Guido Peter Pez , Pushpinder Singh Puri
发明人： Bernard Allen Toseland , Guido Peter Pez , Pushpinder Singh Puri
IPC分类号： C01B3/16
CPC分类号： H01M8/065 , B01J19/0093 , B01J2219/00783 , B01J2219/00835 , B01J2219/0086 , B01J2219/00867 , B01J2219/00873 , B01J2219/00891 , B01J2219/00905 , B01J2219/00997 , C01B3/0015 , C07C5/32 , C07C5/327 , Y02E60/328 , Y02P20/129
摘要： The present invention is an improved process for the storage and delivery of hydrogen by the reversible hydrogenation/dehydrogenation of an organic compound wherein the organic compound is initially in its hydrogenated state. The improvement in the route to generating hydrogen is in the dehydrogenation step and recovery of the dehydrogenated organic compound resides in the following steps: introducing a hydrogenated organic compound to a microchannel reactor incorporating a dehydrogenation catalyst; effecting dehydrogenation of said hydrogenated organic compound under conditions whereby said hydrogenated organic compound is present as a liquid phase; generating a reaction product comprised of a liquid phase dehydrogenated organic compound and gaseous hydrogen; separating the liquid phase dehydrogenated organic compound from gaseous hydrogen; and, recovering the hydrogen and liquid phase dehydrogenated organic compound.
摘要翻译：本发明是通过可逆氢化/脱氢有机化合物的储存和输送氢的改进方法，其中有机化合物最初处于其氢化状态。生成氢气的途径的改善是在脱氢步骤中，脱氢有机化合物的回收步骤如下：将氢化有机化合物引入到包含脱氢催化剂的微通道反应器中; 所述氢化有机化合物在所述氢化有机化合物作为液相存在的条件下进行脱氢; 产生由液相脱氢有机化合物和气态氢组成的反应产物; 将液相脱氢有机化合物与气态氢分离; 并回收氢和液相脱氢的有机化合物。

4. 发明授权

US07766986B2 Dehydrogenation of liquid fuel in microchannel catalytic reactor 有权
标题翻译：微通道催化反应器中液体燃料的脱氢
公开(公告)号：US07766986B2
公开(公告)日：2010-08-03
申请号：US12211585
申请日：2008-09-16
申请人： Bernard Allen Toseland , Guido Peter Pez , Pushpinder Singh Puri
发明人： Bernard Allen Toseland , Guido Peter Pez , Pushpinder Singh Puri
IPC分类号： B01J7/00 , B01J8/04 , C01B3/02
CPC分类号： H01M8/065 , B01J19/0093 , B01J2219/00783 , B01J2219/00835 , B01J2219/0086 , B01J2219/00867 , B01J2219/00873 , B01J2219/00891 , B01J2219/00905 , B01J2219/00997 , C01B3/0015 , C07C5/32 , C07C5/327 , Y02E60/328 , Y02P20/129
摘要： The present invention is an improved process for the storage and delivery of hydrogen by the reversible hydrogenation/dehydrogenation of an organic compound wherein the organic compound is initially in its hydrogenated state. The improvement in the route to generating hydrogen is in the dehydrogenation step and recovery of the dehydrogenated organic compound resides in the following steps: introducing a hydrogenated organic compound to a microchannel reactor incorporating a dehydrogenation catalyst; effecting dehydrogenation of said hydrogenated organic compound under conditions whereby said hydrogenated organic compound is present as a liquid phase; generating a reaction product comprised of a liquid phase dehydrogenated organic compound and gaseous hydrogen; separating the liquid phase dehydrogenated organic compound from gaseous hydrogen; and, recovering the hydrogen and liquid phase dehydrogenated organic compound.
摘要翻译：本发明是通过可逆氢化/脱氢有机化合物的储存和输送氢的改进方法，其中有机化合物最初处于其氢化状态。生成氢气的途径的改进是脱氢步骤，脱氢有机化合物的回收步骤如下：将氢化有机化合物引入到包含脱氢催化剂的微通道反应器中; 所述氢化有机化合物在所述氢化有机化合物作为液相存在的条件下进行脱氢; 产生由液相脱氢有机化合物和气态氢组成的反应产物; 将液相脱氢有机化合物与气态氢分离; 并回收氢和液相脱氢的有机化合物。

5. 发明授权

US6069180A Single step synthesis gas-to-dimethyl ether process with methanol introduction 有权
标题翻译：用甲醇引入单步合成气 - 二甲醚工艺
公开(公告)号：US6069180A
公开(公告)日：2000-05-30
申请号：US213480
申请日：1998-12-17
申请人： Xiang-Dong Peng , Andrew Wilson Wang , Bernard Allen Toseland
发明人： Xiang-Dong Peng , Andrew Wilson Wang , Bernard Allen Toseland
IPC分类号： C07C41/01 , C07C27/00
CPC分类号： C07C41/01 , Y02P20/142
摘要： A process is set forth for converting synthesis gas into dimethyl ether (DME) in a single step comprising contacting the synthesis gas with a bifunctional catalyst system having a methanol synthesis functionality and a methanol dehydration functionality. In particular, the present invention is an improvement to said process for increasing the stability of the bifunctional catalyst system, particularly when the process is conducted in the liquid phase. The improvement comprises introducing a methanol containing stream into the DME reactor such that the methanol concentration throughout the DME reactor is maintained at a concentration greater than 1.0%, generally between 4.0% and 8.0%. In one embodiment of the present invention, the methanol containing stream comprises at least a portion of the byproduct methanol from the DME reactor such that said portion of byproduct methanol is introduced into the DME reactor as a recycle stream.
摘要翻译：阐述了在单步骤中将合成气转化为二甲醚（DME）的方法，包括使合成气与具有甲醇合成官能度和甲醇脱水官能团的双功能催化剂体系接触。特别地，本发明是提高双官能催化剂体系的稳定性的所述方法的改进，特别是当该方法在液相中进行时。改进之处在于将含甲醇的料流引入DME反应器，使得整个DME反应器中的甲醇浓度保持在大于1.0％，通常在4.0％和8.0％之间的浓度。在本发明的一个实施方案中，含甲醇的物流包含来自DME反应器的副产物甲醇的至少一部分，使得所述部分副产物甲醇作为循环物流引入DME反应器。

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