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1. 发明专利

JP2010527352A The start of the high selectivity of the catalyst in olefin oxide plant 审中-公开
公开(公告)号：JP2010527352A
公开(公告)日：2010-08-12
申请号：JP2010508369
申请日：2008-05-07
申请人：カスタグノラ,ノーマ,ベアトリズCastagnola,Norma,Beatriz , グエケル,クリスチャン,ジェイ.Gueckel,Christian,J. , ビリッグ,バリー,ジェイ.Billig,Barry,J. , マン,ジェイムズMann,James , ロキキ,アンドルゼイRokicki,Andrzej
发明人：カスタグノラ，ノーマ，ベアトリズ , グエケル，クリスチャン，ジェイ． , ビリッグ，バリー，ジェイ． , マン，ジェイムズ , ロキキ，アンドルゼイ
IPC分类号： C07D301/10 , B01J23/50 , B01J35/10 , B01J37/08 , C07B61/00 , C07D303/04
CPC分类号： C07D301/10
摘要：【課題】外部熱源を用いた場合に対し、エポキシ化反応器の最大到達温度を超えた、エポキシ化プロセスの制御された開始温度を達成する方法。
【解決手段】
本発明の方法は、反応器の温度を高選択性触媒の調整に適した温度とする反応器内の酸化反応を使用する。本発明の方法は、反応器の設計制限内にとどまり設計割合の２５から１００％の間の反応器へのガス流量を維持している間、高選択性触媒を含む反応器を、反応器の外部熱源を用いた第１温度とする工程を含む。反応器が第１温度に到達すると、少なくともオレフィン、例えばエチレン、その上酸素が反応器の供給ガスへ導入される。オレフィン及び酸素の濃度は、反応器のガス流量が設計の１００％へ上昇することを許容する反応器熱を有するように、その上、反応器温度を第１温度より高く且つ外部熱源により到達可能な反応器の温度より高い第２温度へ上昇させるのに十分な反応器熱を有するように調整される。

2. 发明授权

EP2162446B1 START-UP OF HIGH SELECTIVITY CATALYSTS IN OLEFIN OXIDE PLANTS 有权转让
标题翻译： OLEFIN氧化物工厂高选择性催化剂的启动
公开(公告)号：EP2162446B1
公开(公告)日：2016-03-16
申请号：EP08754227.0
申请日：2008-05-07
申请人： Billig, Barry J. , Mann, James , Castagnola, Norma Beatriz , Rokicki, Andrzej , Gueckel, Christian J.
发明人： Billig, Barry J. , Mann, James , Castagnola, Norma Beatriz , Rokicki, Andrzej , Gueckel, Christian J.
IPC分类号： C07D301/03
CPC分类号： C07D301/10

3. 发明公开

EP2162446A4 START-UP OF HIGH SELECTIVITY CATALYSTS IN OLEFIN OXIDE PLANTS 有权转让
标题翻译：邻烯基氧化物高选择性催化剂的研究进展
公开(公告)号：EP2162446A4
公开(公告)日：2011-09-07
申请号：EP08754227
申请日：2008-05-07
申请人： BILLIG BARRY J , MANN JAMES , CASTAGNOLA NORMA BEATRIZ , ROKICKI ANDRZEJ , GUECKEL CHRISTIAN J
发明人： BILLIG BARRY J , MANN JAMES , CASTAGNOLA NORMA BEATRIZ , ROKICKI ANDRZEJ , GUECKEL CHRISTIAN J
IPC分类号： C07D301/03
CPC分类号： C07D301/10

4. 发明公开

EP2162446A1 START-UP OF HIGH SELECTIVITY CATALYSTS IN OLEFIN OXIDE PLANTS 有权转让
标题翻译： OLEFIN氧化物工厂高选择性催化剂的启动
公开(公告)号：EP2162446A1
公开(公告)日：2010-03-17
申请号：EP08754227.0
申请日：2008-05-07
申请人： Billig, Barry J. , Mann, James , Castagnola, Norma Beatriz , Rokicki, Andrzej , Gueckel, Christian J.
发明人： Billig, Barry J. , Mann, James , Castagnola, Norma Beatriz , Rokicki, Andrzej , Gueckel, Christian J.
IPC分类号： C07D301/03
CPC分类号： C07D301/10
摘要： A method to achieve a controlled start-up temperature of an expoxidation process which exceeds the maximum achievable temperature of the epoxidation reactor relative to using an external heat source. The method of the present invention employs an oxidation reaction within the reactor to bring the temperature of the reactor to a temperature that is suitable for conditioning a high selectivity catalyst. The method of the present invention includes first bringing a reactor including a high selectivity catalyst to a first temperature using the external heat source to the reactor, while staying within the reactor design limitations and maintaining a gas flow to the reactor that is within 25 to 100 % of the design rates. Once the reactor has achieved the first temperature, at least an olefin, e.g., ethylene, and then oxygen are introduced to the reactor feed gas. The olefin and oxygen concentrations are adjusted to have a heat of reaction that will allow raising the reactor gas flow to 100% of design and then have sufficient heat of reaction to raise the reactor temperature to a second temperature which is greater than the first temperature and greater than the temperature of the reactor achievable by the external heat source.
摘要翻译：一种获得超过环氧化反应器相对于使用外部热源的最大可实现温度的循环氧化过程的受控启动温度的方法。本发明的方法在反应器内采用氧化反应以使反应器的温度达到适合调节高选择性催化剂的温度。本发明的方法包括首先使用外部热源将包含高选择性催化剂的反应器带到第一温度到反应器，同时保持在反应器设计限制内并保持到反应器的气体流量在25到100之内设计费率的百分比。一旦反应器达到第一温度，至少将烯烃（例如乙烯），然后将氧气引入反应器原料气中。调节烯烃和氧气浓度以具有使反应器气体流量升高到设计的100％的反应热，然后具有足够的反应热以将反应器温度升高到大于第一温度的第二温度，并且大于外部热源可实现的反应器的温度。

5. 发明专利

BRPI0811260B1 partida de catalisadores de alta seletividade em plantas de óxido de olefina. 未知
公开(公告)号：BRPI0811260B1
公开(公告)日：2017-01-17
申请号：BRPI0811260
申请日：2008-05-07
申请人： ROKICKI ANDRZEJ , BILLIG BARRY J , GUECKEL CHRISTIAN J , MANN JAMES , CASTAGNOLA NORMA BEATRIZ
发明人： ROKICKI ANDRZEJ , BILLIG BARRY J , GUECKEL CHRISTIAN J , MANN JAMES , CASTAGNOLA NORMA BEATRIZ
IPC分类号： C07D301/03
摘要： abstract not avaible

6. 发明专利

MX2009012234A ACTIVACION DE CATALIZADORES DE ALTA SELECTIVIDAD EN PLANTAS DE OXIDO DE OLEFINA. 未知
公开(公告)号：MX2009012234A
公开(公告)日：2010-03-26
申请号：MX2009012234
申请日：2008-05-07
申请人： BILLIG BARRY J
发明人： MANN JAMES , BILLIG BARRY J , CASTAGNOLA NORMA BEATRIZ , ROKICKI ANDRZEJ , GUECKEL CHRISTIAN J
IPC分类号： C07D301/03
摘要： Un método para obtener una temperatura de inicio controlada de un proceso de epoxidación que excede la temperatura máxima que se puede alcanzar en un reactor de epoxidación con relación al uso de una fuerte de calor externa. El método de la presente invención utiliza una reacción de oxidación dentro del reactor para llevar la temperatura del reactor a una temperatura que es apropiada para acondicionar un catalizador de alta selectividad. El método de la presente invención incluye primeramente llevar el reactor que incluye un catalizador de alta selectividad a una primera temperatura utilizando la fuente de calor externa al reactor, el cual mientras está dentro del reactor designa limitaciones y mantiene en flujo de gas al reactor que está dentro de 25 a 100% del rango de diseño. Una vez que el reactor haya alcanzado la primera temperatura, al menos una olefina, por ejemplo, etileno y después oxígeno son introducidos al gas de alimentación del reactor. Las concentraciones y de olefina y oxígeno son ajustadas para tener un calor de reacción que permitirá el crecimiento del flujo de gas en el reactor a 100% del diseño y después suficiente calor de reacción para elevar la temperatura de reacción a una segunda temperatura la cual es mayor que la primera temperatura y mayor que la temperatura del reactor que se puede alcanzar por la fuente de calor externa.

7. 发明申请

WO2008140714A1 START-UP OF HIGH SELECTIVITY CATALYSTS IN OLEFIN OXIDE PLANTS 审中-公开
标题翻译：烯烃氧化物中高选择性催化剂的启动
公开(公告)号：WO2008140714A1
公开(公告)日：2008-11-20
申请号：PCT/US2008/005838
申请日：2008-05-07
申请人： BILLIG, Barry, J. , MANN, James , CASTAGNOLA, Norma, Beatriz , ROKICKI, Andrzej , GUECKEL, Christian, J.
发明人： BILLIG, Barry, J. , MANN, James , CASTAGNOLA, Norma, Beatriz , ROKICKI, Andrzej , GUECKEL, Christian, J.
IPC分类号： C07D301/03
CPC分类号： C07D301/10
摘要： A method to achieve a controlled start-up temperature of an expoxidation process which exceeds the maximum achievable temperature of the epoxidation reactor relative to using an external heat source. The method of the present invention employs an oxidation reaction within the reactor to bring the temperature of the reactor to a temperature that is suitable for conditioning a high selectivity catalyst. The method of the present invention includes first bringing a reactor including a high selectivity catalyst to a first temperature using the external heat source to the reactor, while staying within the reactor design limitations and maintaining a gas flow to the reactor that is within 25 to 100 % of the design rates. Once the reactor has achieved the first temperature, at least an olefin, e.g., ethylene, and then oxygen are introduced to the reactor feed gas. The olefin and oxygen concentrations are adjusted to have a heat of reaction that will allow raising the reactor gas flow to 100% of design and then have sufficient heat of reaction to raise the reactor temperature to a second temperature which is greater than the first temperature and greater than the temperature of the reactor achievable by the external heat source.
摘要翻译：实现超过环氧化反应器相对于使用外部热源的最大可实现温度的过氧化过程的控制启动温度的方法。本发明的方法在反应器内采用氧化反应使反应器的温度达到适于调节高选择性催化剂的温度。本发明的方法包括首先将包含高选择性催化剂的反应器使用外部热源引入反应器，同时保持在反应器设计限制范围内并保持气体流入反应器的温度在25至100℃ ％的设计率。一旦反应器达到第一个温度，至少将一种烯烃，如乙烯，然后将氧气引入到反应器进料气中。调节烯烃和氧浓度以具有反应热，其将使反应器气体流量提高到设计的100％，然后具有足够的反应热，将反应器温度升高到大于第一温度的第二温度，大于外部热源可实现的反应器的温度。

8. 发明专利

BRPI0811260A2 未知
公开(公告)号：BRPI0811260A2
公开(公告)日：2014-11-04
申请号：BRPI0811260
申请日：2008-05-07
申请人： BILLIG BARRY J , MANN JAMES , CASTAGNOLA NORMA BEATRIZ , ROKICKI ANDRZEJ , GUECKEL CHRISTIAN J
发明人： BILLIG BARRY J , MANN JAMES , CASTAGNOLA NORMA BEATRIZ , ROKICKI ANDRZEJ , GUECKEL CHRISTIAN J
IPC分类号： C07D301/03
摘要： A method to achieve a controlled start-up temperature of an expoxidation process which exceeds the maximum achievable temperature of the epoxidation reactor relative to using an external heat source. The method of the present invention employs an oxidation reaction within the reactor to bring the temperature of the reactor to a temperature that is suitable for conditioning a high selectivity catalyst. The method of the present invention includes first bringing a reactor including a high selectivity catalyst to a first temperature using the external heat source to the reactor, while staying within the reactor design limitations and maintaining a gas flow to the reactor that is within 25 to 100% of the design rates. Once the reactor has achieved the first temperature, at least an olefin, e.g., ethylene, and then oxygen are introduced to the reactor feed gas. The olefin and oxygen concentrations are adjusted to have a heat of reaction that will allow raising the reactor gas flow to 100% of design and then have sufficient heat of reaction to raise the reactor temperature to a second temperature which is greater than the first temperature and greater than the temperature of the reactor achievable by the external heat source.

9. 发明申请

WO2009042300A1 PROCESS FOR INITIATING A HIGHLY SELECTIVE ETHYLENE OXIDE CATALYST 审中-公开
标题翻译：开发高选择性乙烯氧化物催化剂的方法
公开(公告)号：WO2009042300A1
公开(公告)日：2009-04-02
申请号：PCT/US2008/072945
申请日：2008-08-13
申请人： SD LIZENZVERWERTUNGSGESELLSCHAFT MBH & CO. KG , RIZKALLA, Nabil , BILLIG, Barry J. , CASTAGNOLA, Norma B.
发明人： RIZKALLA, Nabil , BILLIG, Barry J. , CASTAGNOLA, Norma B.
IPC分类号： C07D301/10
CPC分类号： C07D301/10 , Y02P20/52
摘要： A process for initiating a highly selective ethylene oxide catalyst is provided in which the highly selective ethylene oxide catalyst is operated first as a 'standard' Ag-based catalyst (e.g., a catalyst that contains only silver and alkali metal, especially cesium). Moreover, the inventive initiation procedure is more efficient when the concentration of carbon dioxide in the feed is higher than 6 vol. %, and even more efficient when the concentration of carbon dioxide in the feed is higher than 10 vol. %, of the feed mixture during the initiation period.
摘要翻译：提供了一种引发高选择性环氧乙烷催化剂的方法，其中高选择性环氧乙烷催化剂首先作为“标准”Ag基催化剂（例如仅含有银和碱金属，特别是铯的催化剂）。此外，当进料中二氧化碳的浓度高于6体积时，本发明的引发程序更有效。％，并且当进料中二氧化碳的浓度高于10体积时甚至更有效。％的进料混合物。

10. 发明申请

WO2009035807A1 CHEMICAL PROCESS OPTIMIZATION METHOD THAT CONSIDERS CHEMICAL PROCESS PLANT SAFETY 审中-公开
标题翻译：化学过程优化方法考虑化学过程植物安全
公开(公告)号：WO2009035807A1
公开(公告)日：2009-03-19
申请号：PCT/US2008/072880
申请日：2008-08-12
申请人： SD LIZENZVERWERTUNGSGESELLSCHAFT MBH & CO. KG. , BILLIG, Barry J. , SULLIVAN, John James
发明人： BILLIG, Barry J. , SULLIVAN, John James
IPC分类号： C08F2/00
CPC分类号： G05B9/02 , B01J8/025 , B01J2208/00274 , B01J2208/00539 , B01J2219/00259 , B01J2219/00263 , B01J2219/0027
摘要： A method for assuring safety of a particular chemical process plant includes measuring, for each of a plurality of sets of proposed process conditions for a chemical process within the chemical process plant, a pressure rise rate following a deliberate contained ignition of at least one material used within the chemical process. A particular pressure rise rate that allows for a safe operation of the chemical reaction within the chemical process plant may be selected from the resulting pressure rise rates that correspond with the plurality of sets of proposed process conditions. The chemical process may be implemented within the process plant while using a set of process conditions from the plurality of sets of process conditions that corresponds with the selected pressure rise rate. In addition, the particular chemical reaction may also be optimized with respect to an ancillary parameter, such as product yield or feedstock utilization.
摘要翻译：用于确保特定化学工艺设备的安全性的方法包括针对化学工艺设备中的化学过程的多组提出的工艺条件中的每一个测量所使用的至少一种材料的故意包含点燃的压力上升速率在化学过程中。允许化学处理设备内的化学反应的安全操作的特定压力升高速率可以从与多组所提出的工艺条件相对应的所得压力升高速率中选择。化学过程可以在处理工厂内实施，同时使用与所选择的压力上升率对应的多组工艺条件的一组工艺条件。此外，特定的化学反应也可以相对于辅助参数如产物收率或原料利用进行优化。

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