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1. 发明申请

US20060079682A1 Method for producing phenothiazinium compounds 失效
公开(公告)号：US20060079682A1
公开(公告)日：2006-04-13
申请号：US10960811
申请日：2004-10-07
申请人： Suzanne Wassmann-Wilken , Reinhard Knieps , Thomas Potrawa , Andreas Kanschik-Conradsen , Joachim Schulz , Christian Werner
发明人： Suzanne Wassmann-Wilken , Reinhard Knieps , Thomas Potrawa , Andreas Kanschik-Conradsen , Joachim Schulz , Christian Werner
IPC分类号： C07D279/18
CPC分类号： C07D279/28 , C07D279/18
摘要： A process for producing a phenothiazinium compound comprising the step of: reacting phenothiazine, in the presence of a halogen, with at least one amine selected from the group consisting of: wherein Z is CH2, O, S, SO2, NH, NCH3, NC2H5, NCH2CH2OH or NCOCH3, and R1 and R2 are each independently linear or branched CnH2nY.

2. 发明申请

US20050090596A1 Organic composition 审中-公开
标题翻译：有机成分
公开(公告)号：US20050090596A1
公开(公告)日：2005-04-28
申请号：US10404676
申请日：2003-04-02
申请人： Paul Apen , Kreisler Lau , Boris Korolev , Bo Li , Ruslan Zherebin , Edward Sullivan , Christian Werner , Sonja Demel , Bernd Kellermeier , Andreas Kanschik-Conradsen
发明人： Paul Apen , Kreisler Lau , Boris Korolev , Bo Li , Ruslan Zherebin , Edward Sullivan , Christian Werner , Sonja Demel , Bernd Kellermeier , Andreas Kanschik-Conradsen
IPC分类号： C08G61/02 , C08G61/12 , C08K5/01
CPC分类号： C08G61/02 , C08G61/12
摘要： The present invention provides adamantane or diamantane compositions that are useful as a dielectric material in microelectronic applications such as microchips.
摘要翻译：本发明提供金刚烷或二金刚烷组合物，其可用作微电子应用如微芯片中的电介质材料。

3. 发明授权

US07601871B2 Method for purifying quaternary onium salts 有权
标题翻译：季铵盐的纯化方法
公开(公告)号：US07601871B2
公开(公告)日：2009-10-13
申请号：US11368168
申请日：2006-03-03
申请人： Alfred Siggel , Michael Fooken , Michael Theissen , Andreas Kanschik-Conradsen , Sonja Demel , Frank Nerenz
发明人： Alfred Siggel , Michael Fooken , Michael Theissen , Andreas Kanschik-Conradsen , Sonja Demel , Frank Nerenz
IPC分类号： C07C213/00
CPC分类号： C07C209/84 , C07C211/63 , C07F9/025 , C07F9/54 , C07F9/5407 , C07F9/65688
摘要： Provided are methods of purifying quaternary onium salts having the steps of (a) providing an quaternary onium salt solution having a first ionic impurity concentration; (b) providing an ion exchange material charged with electrochemically stable anions; and (c) contacting the salt solution with the ion exchange material to produce an quaternary onium salt solution having a second halide concentration is less than the first ionic impurity concentration.
摘要翻译：提供纯化季铵盐的方法，其具有以下步骤：（a）提供具有第一离子杂质浓度的季铵盐溶液; （b）提供带有电化学稳定阴离子的离子交换材料; 和（c）使盐溶液与离子交换材料接触以产生具有第二卤化物浓度的季铵盐溶液小于第一离子杂质浓度。

4. 发明授权

US07205414B2 Process for the Kumada coupling reaction 失效
标题翻译： Kumada偶联反应的方法
公开(公告)号：US07205414B2
公开(公告)日：2007-04-17
申请号：US11033573
申请日：2005-01-12
申请人： Christian Werner , Frauke Platz , Andreas Kanschik-Conradsen
发明人： Christian Werner , Frauke Platz , Andreas Kanschik-Conradsen
IPC分类号： C07D333/08 , C07D333/28
CPC分类号： C07D333/06
摘要： A method for the formation of 3-alkylthiophenes or 3-arylthiophenes from 3-halothiophenes. More particularly, improvements on the Kumada coupling reaction for the production of 3-alkylthiophenes or 3-arylthiophenes by reacting a 3-halothiophene with an alkylmagnesiumhalide or arylmagnesiumhalide Grignard reagent in the presence of a catalyst and a 2-methyl tetrahydrofuran solvent. The 2-methyl tetrahydrofuran solvent allows for higher concentrations of the Grignard reagent with minimal or no dithienyl side product generation, achieving higher product yields and at a lower cost than other known methods.
摘要翻译：从3-卤代噻吩形成3-烷基噻吩或3-芳基噻吩的方法。更具体地，通过在催化剂和2-甲基四氢呋喃溶剂的存在下使3-卤代噻吩与烷基镁卤化物或芳基镁卤化物格氏试剂反应制备3-烷基噻吩或3-芳基噻吩的Kumada偶联反应的改进。 2-甲基四氢呋喃溶剂允许较高浓度的格利雅试剂与最少或没有二噻吩基产物的产生相比，获得更高的产物产率并以比其它已知方法更低的成本。

5. 发明申请

US20060247472A1 Method for purifying quaternary onium salts 有权
公开(公告)号：US20060247472A1
公开(公告)日：2006-11-02
申请号：US11368168
申请日：2006-03-03
申请人： Alfred Siggel , Michael Fooken , Michael Theissen , Andreas Kanschik-Conradsen , Sonja Demel , Frank Nerenz
发明人： Alfred Siggel , Michael Fooken , Michael Theissen , Andreas Kanschik-Conradsen , Sonja Demel , Frank Nerenz
IPC分类号： C07C211/00
CPC分类号： C07C209/84 , C07C211/63 , C07F9/025 , C07F9/54 , C07F9/5407 , C07F9/65688
摘要： Provided are methods of purifying quaternary onium salts having the steps of (a) providing an quaternary onium salt solution having a first ionic impurity concentration; (b) providing an ion exchange material charged with electrochemically stable anions; and (c) contacting the salt solution with the ion exchange material to produce an quaternary onium salt solution having a second halide concentration is less than the first ionic impurity concentration.

6. 发明授权

US06894158B2 Methods of producing phosphitylated compounds 失效
标题翻译：磷酸化化合物的制备方法
公开(公告)号：US06894158B2
公开(公告)日：2005-05-17
申请号：US10373336
申请日：2003-02-24
申请人： Christian Werner , Frank Nerenz , Andreas Kanschik-Conradsen , Kalakota Reddy
发明人： Christian Werner , Frank Nerenz , Andreas Kanschik-Conradsen , Kalakota Reddy
IPC分类号： C12N15/09 , C07B61/00 , C07H19/073 , C07H19/10 , C07H19/173 , C07H19/20 , C07H21/00
CPC分类号： C07H19/10 , C07H19/20
摘要： Provided are methods of producing phosphitylated compounds, including 3′-O-phosphoramidites, comprising the step of reacting a hydroxyl-containing compound with a phosphitylating agent in the presence of a phosphitylation activator selected from the group consisting of: (1) acid-base complexes derived from an amine base of Formula I wherein R, R1, and R2 are independently C1-C10 alkyl, C3-C10 cycloalkyl, C6-C10 aryl, C7-C10 aralkyl, C1-C10 heteroalkyl, or C1-C10 heteroaryl, wherein any two adjacent R, R1, and R2 may be connected to form a heterocyclic ring; (2) acid-base complexes derived from a diazabicyclo amine base; and (3) combinations of two or more thereof.
摘要翻译：提供了生产磷酸化化合物（包括3'-O-亚磷酰胺）的方法，包括在磷酸化活化剂存在下使含羟基的化合物与磷酸化剂反应的步骤，所述磷化活化剂选自：（1）酸碱衍生自式I的胺碱的络合物，其中R 1，R 2和R 2独立地为C 1 -C 10烷基， C 1 -C 6烷基，C 3 -C 10环烷基，C 6 -C 10芳基，C

7. 发明授权

US5545768A Process for the preparation of chlorofluronitrobenzenes and difluoronitrobenzenes 失效
标题翻译：氯氟草硝和二氟硝基苯的制备方法
公开(公告)号：US5545768A
公开(公告)日：1996-08-13
申请号：US958107
申请日：1992-12-22
申请人： Theodor Papenfhus , Andreas Kanschik-Conradsen , Wilfried Pressler
发明人： Theodor Papenfhus , Andreas Kanschik-Conradsen , Wilfried Pressler
IPC分类号： B01J31/02 , C07B61/00 , C07C201/12 , C07C201/14 , C07C205/12
CPC分类号： C07C201/12
摘要： A process for the preparation of chlorofluoronitrobenzenes and difluoronitrobenzenes, which comprises heating dichloronitrobenzene to not more than 200.degree. C. in excess with an alkali metal fluoride having a total water content of about 0.2 to about 2.5% by weight in the presence of a quaternary ammonium and/or phosphonium salt, crown ether and/or polyethylene glycol dimethyl ether as catalyst in the absence of a solvent.
摘要翻译： PCT No.PCT / EP92 / 01079 Sec。 371日期1992年12月22日 102（e）日期1992年12月22日PCT Filed 1991年6月8日PCT公布。公开号WO91 / 00270 日期1992年1月9日一种氯氟硝基苯和二氟硝基苯的制备方法，其包括在二氯硝基苯与总含水量为约0.2至约2.5重量％的碱金属氟化物中将二氯硝基苯过量加热至不超过200℃ 在不存在溶剂的情况下存在季铵和/或鏻盐，冠醚和/或聚乙二醇二甲醚作为催化剂。

8. 发明授权

US07749483B2 Method for producing alkaline earth metal oxides 失效
标题翻译：碱土金属氧化物的制造方法
公开(公告)号：US07749483B2
公开(公告)日：2010-07-06
申请号：US11611707
申请日：2006-12-15
申请人： Thomas Scholten , Michael Fooken , Jessica Mauer , Andreas Kanschik-Conradsen , Michael Hau
发明人： Thomas Scholten , Michael Fooken , Jessica Mauer , Andreas Kanschik-Conradsen , Michael Hau
IPC分类号： C01F11/00
CPC分类号： C01F11/02 , C01F11/06 , C01F11/185 , C01F11/187 , C01P2004/61 , C01P2006/80 , C01P2006/82
摘要： Disclosed is a processes for the production of relatively high purity alkaline earth metal oxides, such as SrO, from relatively low purity forms of carbonated or other oxygenated forms of such metals, such as strontium carbonate. The relatively low purity material is exposed to conditions under which at least a portion of the metal contained therein is converted to a salt that is more readily solvated in a provided solvent than the starting material, while at the same time not substantially increasing the solubility of at least one or more of the impurities in such selected solvent. This step is then preferably followed by removal of solid or otherwise un-dissolved impurities from the solution. After the removal step, the solution is preferably exposed to conditions effective to form a relatively insoluble salt of the alkaline earth metal, such as a strontium salt. The insoluble salt is also preferably one that can be readily and effectively converted to the desired alkaline earth metal oxide, preferably SrO. A novel preferred thermal decomposition step disclosed.
摘要翻译：公开了一种生产相对较高纯度的碱土金属氧化物（如SrO）的方法，其来自相对低纯度形式的碳酸或其它氧化形式的这种金属如碳酸锶。将相对低纯度的材料暴露于其中含有的金属的至少一部分转化为在所提供的溶剂中比原料更容易溶剂化的盐的条件下，同时基本上不提高溶解度在这种选择的溶剂中的至少一种或多种杂质。然后优选该步骤从溶液中除去固体或其它未溶解的杂质。在除去步骤之后，溶液优选暴露于有效形成碱土金属的相对不溶性盐如锶盐的条件下。不溶性盐也优选可以容易且有效地转化为所需的碱土金属氧化物，优选SrO的那些。公开了一种新颖的热分解步骤。

9. 发明申请

US20090156834A1 PROCESS FOR MAKING 2,2-BIS (3,4-DICARBOXYPHENYL) HEXAFLUOROPROPANE 审中-公开
标题翻译：制备2,2-BIS（3,4-二氧代苯基）十六烷基二胺的方法
公开(公告)号：US20090156834A1
公开(公告)日：2009-06-18
申请号：US12327466
申请日：2008-12-03
申请人： Andreas Kanschik-Conradsen , Bjoern Oliver Jackisch , Ralph Lonsky
发明人： Andreas Kanschik-Conradsen , Bjoern Oliver Jackisch , Ralph Lonsky
IPC分类号： C07D407/10 , C07C51/275
CPC分类号： C07C51/275 , C07C51/56 , C07C63/72
摘要： There is provided a continuous process for making 2,2-bis(3,4-dicarboxyphenyl)hexafluoropropane. The process has the following steps: a) continuously feeding 2,2-bis(3,4-dimethylphenyl)hexafluoropropane and aqueous nitric acid into a reactor cell and b) heating the mixture to a temperature sufficient to effect reaction between the 2,2-bis(3,4-dimethylphenyl)hexafluoropropane and the nitric acid.
摘要翻译：提供了制备2,2-双（3,4-二羧基苯基）六氟丙烷的连续方法。该方法具有以下步骤：a）将2,2-双（3,4-二甲基苯基）六氟丙烷和硝酸水溶液连续供入反应器中，b）将混合物加热至足以在2,2 双（3,4-二甲基苯基）六氟丙烷和硝酸。

10. 发明授权

US07217814B2 Methods of producing phosphitylated compounds 失效
标题翻译：磷酸化化合物的制备方法
公开(公告)号：US07217814B2
公开(公告)日：2007-05-15
申请号：US10990138
申请日：2004-11-16
申请人： Christian Werner , Frank Nerenz , Andreas Kanschik-Conradsen , Kalakota S. Reddy
发明人： Christian Werner , Frank Nerenz , Andreas Kanschik-Conradsen , Kalakota S. Reddy
IPC分类号： C07H21/00
CPC分类号： C07H19/10 , C07H19/20
摘要： Provided are methods of producing phosphitylated compounds, including 3′-O-phosphoramidites, comprising the step of reacting a hydroxyl-containing compound with a phosphitylating agent in the presence of a phosphitylation activator selected from the group consisting of: (1) acid-base complexes derived from an amine base of Formula II wherein R3, R4, R5, R6, and R7 are independently hydrogen, C1–C10 alkyl, C3–C10 cycloalkyl, C6–C10 aryl, C7–C10 aralkyl, C1–C10 heteroalkyl, or C1–C10 heteroaryl, and at least one of R3, R4, R5, R6, and R7 is not hydrogen; (2) zwitterionic amine complexes; and (3) combinations of two or more thereof, to produce a phosphitylated compound. Further provided are methods for purifying phosphitylated compounds comprising the steps of providing a phosphitylated compound in a solution solvent, contacting said phosphitylated compound with a precipitation solvent, and precipitating said phosphitylated compound.
摘要翻译：提供了生产磷酸化化合物（包括3'-O-亚磷酰胺）的方法，包括在含磷酸化活化剂存在下使含羟基的化合物与磷酸化剂反应的步骤，所述磷化活化剂选自：（1）酸碱衍生自式II的胺碱的络合物，其中R 3，R 4，R 5，R 6， R 7独立地是氢，C 1 -C 10烷基，C 3 -C 10烷基，C 1 -C 10烷基，C 3 -C 10烷基，环烷基，C 6 -C 10芳基，C 7 -C 10芳烷基，C 1 -C 10烷基，或者C 1 -C 10杂芳基，以及至少一个R 1，R 2，R 2， R 4，R 4，R 5，R 6和R 7不是氢; （2）两性离子胺络合物; 和（3）两种或更多种的组合，以产生磷酸化化合物。还提供了纯化磷酸化化合物的方法，包括以下步骤：在溶液中提供磷酸化化合物，使所述磷酸化化合物与沉淀溶剂接触，并使所述磷酸化化合物沉淀。

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