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1. 发明申请

WO2012107641A3 METHOD OF PURIFYING A GAS 审中-公开
标题翻译：净化气体的方法
公开(公告)号：WO2012107641A3
公开(公告)日：2012-11-15
申请号：PCT/FI2012050113
申请日：2012-02-08
申请人： NESTE OIL OYJ , KESKINEN KARI I , KOSKINEN JUKKA , AITTAMAA JUHANI , PETTERSSON MARIANNE
发明人： KESKINEN KARI I , KOSKINEN JUKKA , AITTAMAA JUHANI , PETTERSSON MARIANNE
IPC分类号： B01D53/14 , B01D53/52 , C01B17/05 , C10G2/00
CPC分类号： B01D53/526 , B01D53/1406 , B01D53/1462 , B01D2252/2021 , B01D2257/304 , B01D2257/504 , C01B17/20 , C01G3/06 , C10G2300/1011 , C10G2300/207 , C10G2300/44 , C10J3/00 , C10J2300/0916 , C10K1/004 , C10K1/005 , C10K1/085 , C10K1/108 , C10K1/165 , Y02C10/06 , Y02E20/18 , Y02E50/32 , Y02P20/145 , Y02P20/152 , Y02P30/20
摘要： A method of purifying gas obtained by gasification of a biomass feedstock. The gas which contains carbon monoxide, carbon dioxide, hydrogen, hydrocarbons and mixtures thereof can be freed from impurities, such as hydrogen sulphide, hydrogen chloride, ammonia, carbonyl sulphide, hydrogen cyanide and mixtures thereof, by contacting the gas with an acidic aqueous wash solution of transition metal ions capable of binding to sulphide ions, by binding a significant portion of the hydrogen sulphide impurities contained in the gas into practically insoluble transition metal sulphide compounds to remove hydrogen sulphide impurities from the gas; and by separating the thus obtained purified gas from the aqueous solution. The purified gas is suitable for production of hydrocarbon compositions by, for example the Fischer-Tropsch process.
摘要翻译：一种净化通过生物质原料气化获得的气体的方法。含有一氧化碳，二氧化碳，氢，烃及其混合物的气体可以通过使气体与酸性水洗液相接触来除去杂质，例如硫化氢，氯化氢，氨，硫化羰，氰化氢及其混合物能够结合硫化物离子的过渡金属离子的溶液，通过将气体中包含的大部分硫化氢杂质与几乎不溶的过渡金属硫化物化合物结合，以从气体中除去硫化氢杂质; 并通过从水溶液中分离由此获得的净化气体。纯化的气体适用于通过例如费 - 托方法生产烃组合物。

2. 发明申请

WO1993019032A1 PROCESS FOR PREPARING METHYL ETHERS 审中-公开
标题翻译：制备甲基醚的方法
公开(公告)号：WO1993019032A1
公开(公告)日：1993-09-30
申请号：PCT/FI1993000098
申请日：1993-03-18
申请人： NESTE OY , TAMMINEN, Esa , AITTAMAA, Juhani , JAKKULA, Juha
发明人： NESTE OY
IPC分类号： C07C41/06
CPC分类号： B01D3/009 , C07C41/06 , C07C41/42 , Y02P20/127 , C07C43/046
摘要： The invention relates to a process for preparing tertiary methyl ethers. According to the process the feedstock containing hydrocarbons is fed to a catalytic distillation reactor system, in which the isoolefines, in particular the C4 to C7 isoolefines, of the feed are reacted with methanol in the presence of a cation exchange resin in order to produce tertiary methyl ether products. The reaction product containing the ethers is removed from the distillation system as the bottoms product and, if necessary, it is subjected to an additional treatment for producing a gasoline component. The unreacted methanol is removed as the overhead product of the distillation. According to the invention, the distillate withdrawn mainly contains an azeotrope of C4 hydrocarbons and methanol, the C4 amount of which at least approximately corresponds to the C4 hydrocarbon concentration of the hydrocarbon feed, a substantial amount of the unreacted methanol being removed in the form of said azeotrope. By means of the invention the need for a separate methanol washing unit is eliminated in the apparatus which considerably diminishes apparatus investment costs.
摘要翻译：本发明涉及一种制备叔甲基醚的方法。根据该方法，将含有烃的原料进料到催化蒸馏反应器系统中，其中进料的异烯烃，特别是C4至C7异烯烃在阳离子交换树脂的存在下与甲醇反应，以产生叔甲醚产品。含有醚的反应产物作为塔底产物从蒸馏系统中除去，如果需要，将其进行额外处理以生产汽油组分。作为蒸馏塔顶产物除去未反应的甲醇。根据本发明，取出的馏出物主要含有C 4烃和甲醇的共沸物，其C4量至少大约对应于烃进料的C4烃浓度，大量未反应的甲醇以说共沸物。通过本发明，在装置中消除了对单独的甲醇洗涤单元的需求，这显着地减少了设备投资成本。

3. 发明申请

WO1997030960A1 PROCESS FOR PREPARING ALKYL ETHERS AND MIXTURES THEREOF 审中-公开
标题翻译：制备烷基醚及其混合物的方法
公开(公告)号：WO1997030960A1
公开(公告)日：1997-08-28
申请号：PCT/FI1997000120
申请日：1997-02-21
申请人： NESTE OY , KOSKINEN, Matti , LINDQVIST, Petri , JÄRVELIN, Harri , AITTAMAA, Juhani
发明人： NESTE OY
IPC分类号： C07C41/06
CPC分类号： C07C41/42 , C07C41/06 , C07C43/046
摘要： The invention concerns a process for preparing a tertiary alkyl ether product. The process comprises reacting the isoolefins of an olefinic hydrocarbon feedstock in a reaction zone (1 - 3) with an alkanol to form a reaction mixture, which is subjected to distillation in a first distillation zone (4). The bottoms product of the first distillation contains the ether(s), whereas the overhead stream contains unreacted alkanol and a mixture of light hydrocarbons. The overhead stream is subjected to a second distillation in a second distillation zone (15). The overhead product of the second distillation mainly contains the lightest hydrocarbons and a small amount of alkanol, and the bottoms product contains an essentially oxygenate-free hydrocarbon stream which can be used as such for alkylation. In order to increase the conversion of the process, a side drawoff is withdrawn from the second distillation zone (15) and recirculated to the reaction zone (1 - 3).
摘要翻译：本发明涉及一种制备叔烷基醚产物的方法。该方法包括使反应区（1-3）中的烯烃原料的异烯烃与烷醇反应以形成反应混合物，其在第一蒸馏区（4）中进行蒸馏。第一次蒸馏的塔底产物含有醚，而顶部物流含有未反应的链烷醇和轻烃的混合物。塔顶流在第二蒸馏区（15）中进行第二次蒸馏。第二次蒸馏的塔顶产物主要含有最轻的烃和少量的链烷醇，底部产物含有基本上不含氧的烃流，可用于烷基化。为了增加该方法的转化率，从第二蒸馏区（15）中取出侧抽出物并再循环至反应区（1-3）。

4. 发明申请

WO1994000411A1 PROCESS AND APPARATUS FOR PRODUCING TERTIARY ETHERS 审中-公开
标题翻译：生产其他食品的方法和设备
公开(公告)号：WO1994000411A1
公开(公告)日：1994-01-06
申请号：PCT/FI1993000266
申请日：1993-06-22
申请人： NESTE OY , EILOS, Isto , AITTAMAA, Juhani , JAKKULA, Juha
发明人： NESTE OY
IPC分类号： C07C41/06
CPC分类号： C07C41/06 , B01J8/20 , B01J8/26 , C07C43/046
摘要： The present invention relates to a process and an apparatus for producing tertiary alkyl ethers from isoolefins and alcohols. According to the process, the isoolefins and alcohols are reacted with each other in a reaction space (31) in the presence of a cation exchange resin for forming the ethers. The process is carried out in an reactor vessel comprising a lower section in which a fluidized-bed section (35) can be formed, and an upper section in which a fixed-bed section (36) can be formed, respectively. The inlet nozzle (30A) for initial reactant mixture feed is adapted to the reactor vessel lower section and the outlet nozzle (30B) for removal of reaction products is adapted to the reactor vessel upper section, respectively. According to the invention the fixed reaction bed (36) is advantageously achieved by using a reactor equipped with an expansion section (37) above which the reactor cross-sectional area is increased sufficiently to reduce the superficial velocity of the liquid upflow from the reactor lower section to the upper section below the minimum fluidization velocity. By virtue of the invention, the catalyst contained in the fixed bed can be changed even during run by temporarily reducing the superficial liquid velocity so much as to allow the catalyst particles contained in the fixed bed to fall by gravity to the lower section of the reactor, wherefrom the spent catalyst can be unloaded as necessary and replaced by new catalyst.
摘要翻译：本发明涉及从异烯烃和醇生产叔烷基醚的方法和设备。根据该方法，异氰酸酯和醇在反应空间（31）中在形成醚的阳离子交换树脂的存在下反应。该方法在包括其中可以形成流化床部分（35）的下部分的反应器容器中，以及分别可以形成固定床部分（36）的上部分。用于初始反应物混合物进料的入口喷嘴（30A）适于反应器容器下部，并且用于除去反应产物的出口喷嘴（30B）分别适应于反应器容器上部。根据本发明，固定反应床（36）有利地通过使用装备有膨胀段（37）的反应器来实现，在该反应器上方，反应器的横截面面积被充分地增加以降低来自反应器的液体向上流的表面速度截面到最低流化速度以下的上部。根据本发明，即使在运行期间，包含在固定床中的催化剂也可以通过暂时降低表面液体速度来改变，使得包含在固定床中的催化剂颗粒通过重力下降到反应器的下部，从而可以根据需要卸载废催化剂，并用新的催化剂代替。

5. 发明申请

WO2013030448A3 A TWO-STAGE GAS WASHING METHOD APPLYING SULFIDE PRECIPITATION AND ALKALINE ABSORPTION 审中-公开
标题翻译：应用硫化物降解和碱吸收的两阶段气体洗涤方法
公开(公告)号：WO2013030448A3
公开(公告)日：2013-07-18
申请号：PCT/FI2012050816
申请日：2012-08-28
申请人： NESTE OIL OYJ , WAHLSTROEM JAN , AITTAMAA JUHANI , EILOS ISTO , KESKINEN KARI I , KOSKINEN JUKKA , TIITTA MARJA , VUORI HELI
发明人： WAHLSTROEM JAN , AITTAMAA JUHANI , EILOS ISTO , KESKINEN KARI I , KOSKINEN JUKKA , TIITTA MARJA , VUORI HELI
IPC分类号： B01D53/52 , C10G2/00 , C10K1/00 , C10K1/10 , C10K1/12 , C10K3/00 , C10K3/04
CPC分类号： B01D53/526 , B01D2251/404 , B01D2257/304 , B01D2257/504 , C10G2/30 , C10G2300/1011 , C10G2300/1022 , C10G2300/207 , C10J2300/0916 , C10K1/004 , C10K1/005 , C10K1/08 , C10K1/105 , C10K1/106 , C10K1/108 , C10K1/12 , C10K1/122 , C10K3/006 , C10K3/04 , Y02E50/32 , Y02P20/145 , Y02P20/152 , Y02P30/20
摘要： The present description is related to the field of hydrocarbon production by gasification of carbonaceous material. It provides a two-stage gas washing method as a part of gas refining. More specifically it discloses a method for hydrogen sulfide and carbon dioxide removal from synthesis gas produced by gasification. It introduces a use of a novel combination of two chemical wash approaches for this application. As a specific application, this process is utilized as a part of biomass to liquid (BTL) process.
摘要翻译：本说明书涉及通过碳质材料的气化生产烃类的领域。它作为气体精炼的一部分提供了两阶段的气体清洗方法。更具体地，其公开了从气化产生的合成气中除去硫化氢和二氧化碳的方法。它引入了两种化学洗涤方法的新颖组合在本申请中的应用。作为具体应用，该方法被用作生物质与液体（BTL）过程的一部分。

6. 发明申请

WO2012107641A2 METHOD OF PURIFYING A GAS 审中-公开
标题翻译：净化气体的方法
公开(公告)号：WO2012107641A2
公开(公告)日：2012-08-16
申请号：PCT/FI2012/050113
申请日：2012-02-08
申请人： NESTE OIL OYJ , KESKINEN, Kari I , KOSKINEN, Jukka , AITTAMAA, Juhani , PETTERSSON, Marianne
发明人： KESKINEN, Kari I , KOSKINEN, Jukka , AITTAMAA, Juhani , PETTERSSON, Marianne
IPC分类号： B01D53/14 , B01D53/52 , C01B17/05 , C10G2/00
CPC分类号： B01D53/526 , B01D53/1406 , B01D53/1462 , B01D2252/2021 , B01D2257/304 , B01D2257/504 , C01B17/20 , C01G3/06 , C10G2300/1011 , C10G2300/207 , C10G2300/44 , C10J3/00 , C10J2300/0916 , C10K1/004 , C10K1/005 , C10K1/085 , C10K1/108 , C10K1/165 , Y02C10/06 , Y02E20/18 , Y02E50/32 , Y02P20/145 , Y02P20/152 , Y02P30/20
摘要： A method of purifying gas obtained by gasification of a biomass feedstock. The gas which contains carbon monoxide, carbon dioxide, hydrogen, hydrocarbons and mixtures thereof can be freed from impurities, such as hydrogen sulphide, hydrogen chloride, ammonia, carbonyl sulphide, hydrogen cyanide and mixtures thereof, by contacting the gas with an acidic aqueous wash solution of transition metal ions capable of binding to sulphide ions, by binding a significant portion of the hydrogen sulphide impurities contained in the gas into practically insoluble transition metal sulphide compounds to remove hydrogen sulphide impurities from the gas; and by separating the thus obtained purified gas from the aqueous solution. The purified gas is suitable for production of hydrocarbon compositions by, for example the Fischer-Tropsch process.
摘要翻译：净化通过气化生物质原料获得的气体的方法。含有一氧化碳，二氧化碳，氢气，烃及其混合物的气体可通过使气体与酸性含水洗涤液接触而除去诸如硫化氢，氯化氢，氨，硫化羰，氰化氢及其混合物的杂质通过将气体中含有的大部分硫化氢杂质结合到实际上不溶的过渡金属硫化物化合物中以从气体中除去硫化氢杂质，从而能够与硫化物离子结合的过渡金属离子溶液; 并从水溶液中分离这样获得的纯化气体。纯化的气体适用于通过例如费 - 托工艺生产烃组合物。

7. 发明申请

WO1993019031A1 PROCESS AND APPARATUS FOR PREPARING TERTIARY ALKYL ETHERS 审中-公开
标题翻译：制备碱性烷基醚的方法和装置
公开(公告)号：WO1993019031A1
公开(公告)日：1993-09-30
申请号：PCT/FI1993000097
申请日：1993-03-18
申请人： NESTE OY , AITTAMAA, Juhani , EILOS, Isto , JAKKULA, Juha , LINDQVIST, Petri
发明人： NESTE OY
IPC分类号： C07C41/06
CPC分类号： C07C41/42 , B01D3/009 , C07C41/06 , Y02P20/127 , Y10S203/06 , Y10S203/17 , Y10S203/20 , C07C43/046
摘要： The invention concerns a process and an apparatus for preparing tertiary ethers. According to the process, C4 to C6 isoolefins and possibly heavier olefins contained in the feedstock are reacted with lower aliphatic alcohols, in particular methanol or ethanol, in a catalytic distillation reactor system in order to produce the corresponding ethers. According to the invention, the reaction between the isoolefins and the alcohols is essentially carried out in at least one reactor (5-7) of the kind, which is combined with a distillation column (3) intended for product separation, by conducting at least a part of the liquid flow of the column through the reactor and returning it to a lower tray than the one from which it was taken. At least half of cation exchange resin is placed in the side reactor (5-7). In the process according to the invention, the catalyst can be rapidly changed without stopping the process. In order to improve conversion additional alcohol can be fed to at least one of the side reactors.
摘要翻译：本发明涉及一种制备叔醚的方法和装置。根据该方法，原料中所含的C4至C6异烯烃和可能较重的烯烃在催化蒸馏反应器系统中与低级脂族醇，特别是甲醇或乙醇反应，以产生相应的醚。根据本发明，异烯烃和醇之间的反应基本上在至少一个与用于产物分离的蒸馏塔（3）组合的反应器（5-7）中进行，至少通过至少柱的液体流的一部分通过反应器并将其返回到比从其取出的塔的下部托盘。将至少一半的阳离子交换树脂置于侧反应器（5-7）中。在根据本发明的方法中，可以快速改变催化剂而不停止该方法。为了改善转化率，另外的醇可以进料至至少一个侧反应器。

8. 发明申请

WO2013030448A2 A TWO-STAGE GAS WASHING METHOD APPLYING SULFIDE PRECIPITATION AND ALKALINE ABSORPTION 审中-公开
标题翻译：应用硫化物沉淀和碱吸收的两段式气体洗涤方法
公开(公告)号：WO2013030448A2
公开(公告)日：2013-03-07
申请号：PCT/FI2012/050816
申请日：2012-08-28
申请人： NESTE OIL OYJ , WAHLSTRÖM, Jan , AITTAMAA, Juhani , EILOS, Isto , KESKINEN, Kari I. , KOSKINEN, Jukka , TIITTA, Marja , VUORI, Heli
发明人： WAHLSTRÖM, Jan , AITTAMAA, Juhani , EILOS, Isto , KESKINEN, Kari I. , KOSKINEN, Jukka , TIITTA, Marja , VUORI, Heli
IPC分类号： C10K1/10
CPC分类号： B01D53/526 , B01D2251/404 , B01D2257/304 , B01D2257/504 , C10G2/30 , C10G2300/1011 , C10G2300/1022 , C10G2300/207 , C10J2300/0916 , C10K1/004 , C10K1/005 , C10K1/08 , C10K1/105 , C10K1/106 , C10K1/108 , C10K1/12 , C10K1/122 , C10K3/006 , C10K3/04 , Y02E50/32 , Y02P20/145 , Y02P20/152 , Y02P30/20
摘要： The present description is related to the field of hydrocarbon production by gasification of carbonaceous material. It provides a two-stage gas washing method as a part of gas refining. More specifically it discloses a method for hydrogen sulfide and carbon dioxide removal from synthesis gas produced by gasification. It introduces a use of a novel combination of two chemical wash approaches for this application. As a specific application, this process is utilized as a part of biomass to liquid (BTL) process.
摘要翻译：本说明书涉及通过碳质材料的气化生产碳氢化合物的领域。它提供了一种两段式气体清洗方法作为气体精炼的一部分。更具体地说，它公开了一种从气化产生的合成气中除去硫化氢和二氧化碳的方法。它介绍了这种应用中两种化学清洗方式的新型组合的用法。作为具体应用，这个过程被用作生物质液化（BTL）过程的一部分。

9. 发明申请

WO2012107640A3 A TWO-STAGE GAS WASHING METHOD 审中-公开
公开(公告)号：WO2012107640A3
公开(公告)日：2012-08-16
申请号：PCT/FI2012/050112
申请日：2012-02-08
申请人： NESTE OIL OYJ , WAHLSTRÖM, Jan , AITTAMAA, Juhani , EILOS, Isto
发明人： WAHLSTRÖM, Jan , AITTAMAA, Juhani , EILOS, Isto
IPC分类号： B01D53/52 , C10K1/08 , C10J3/00
摘要： The present description is related to the field of hydrocarbon production by gasification of carbonaceous material. It provides a two-stage gas washing method as a part of gas refining. More specifically it discloses a method for hydrogen sulfide and carbon dioxide removal from synthesis gas produced by gasification. It introduces a use of a novel combination of wash approaches for this application. As a specific application, this process is utilizedas a part of biomass to liquid (BTL) process.

10. 发明申请

WO2012107640A2 A TWO-STAGE GAS WASHING METHOD 审中-公开
标题翻译：两级气体洗涤方法
公开(公告)号：WO2012107640A2
公开(公告)日：2012-08-16
申请号：PCT/FI2012050112
申请日：2012-02-08
申请人： NESTE OIL OYJ , WAHLSTROEM JAN , AITTAMAA JUHANI , EILOS ISTO
发明人： WAHLSTROEM JAN , AITTAMAA JUHANI , EILOS ISTO
CPC分类号： B01D53/526 , B01D53/1406 , B01D53/1462 , B01D2252/2021 , B01D2257/304 , B01D2257/504 , C01B17/20 , C01G3/06 , C10G2300/1011 , C10G2300/207 , C10G2300/44 , C10J3/00 , C10J2300/0916 , C10K1/004 , C10K1/005 , C10K1/085 , C10K1/108 , C10K1/165 , Y02C10/06 , Y02E20/18 , Y02E50/32 , Y02P20/145 , Y02P20/152 , Y02P30/20
摘要： The present description is related to the field of hydrocarbon production by gasification of carbonaceous material. It provides a two-stage gas washing method as a part of gas refining. More specifically it discloses a method for hydrogen sulfide and carbon dioxide removal from synthesis gas produced by gasification. It introduces a use of a novel combination of wash approaches for this application. As a specific application, this process is utilizedas a part of biomass to liquid (BTL) process.
摘要翻译：本说明书涉及通过碳质材料的气化生产烃类的领域。它作为气体精炼的一部分提供了两阶段的气体清洗方法。更具体地，其公开了从气化产生的合成气中除去硫化氢和二氧化碳的方法。它介绍了一种新的洗涤方法组合的应用。作为具体应用，该过程被用作生物量与液体（BTL）过程的一部分。

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