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    • 1. 发明申请
    • A PROCESS OF MANUFACTURING THICKENERS AND THE USE OF THUS PRODUCED THICKENERS IN HIGH-VISCOSITY UNSATURATED POLYESTER CONTAINING FORMULATIONS
    • 在高粘度不饱和聚酯制剂中制造增稠剂的方法和使用制造的增稠剂的方法
    • WO2017220506A1
    • 2017-12-28
    • PCT/EP2017/064964
    • 2017-06-19
    • BYK-CHEMIE GMBHBYK USA, INC.
    • DZIWOK, KlausNASH, TylerBRIELL, RobertCOUTELLE, Helmut
    • C01B33/44C08K3/34C08L67/06
    • The invention relates to the use of at least one mixed mineral organoclay rheology additive, which comprises or consists of a quaternary alkyl-ammonium salt treated mineral clay mixture prepared by forming an aqueous hormite clay slurry (a), forming an aqueous smectite clay slurry (b), combining the aqueous hormite clay slurry (a) with the aqueous smectite clay slurry (b) to form a combined clay slurry (c), treating the combined clay slurry (c) with one or more quaternary alkyl-ammonium salts, separating the thus produced quaternary alkyl-ammonium salt treated mineral clay mixture from the aqueous medium, in which the aqueous hormite clay slurry (a) being formed by (i.1) dispersing a fraction of one or more hormite clays selected from the group of sepiolites and palygorskites in an aqueous medium to form a dispersion, and the aqueous smectite clay slurry (b) being formed by (ii.1) dispersing a fraction of one or more smectite clays in an aqueous medium to form a dispersion, and in that the weight of the hormite clay content exceeds the weight of the smectite clay content in the combined clay slurry (c); and subjecting the dispersions formed in (i.1) and (ii.1) to high speed fluid shear before carrying out step iii. and/or after having carried out step iii; and wherein the fraction of one or more hormite clays employed in the formation of the aqueous hormite clay slurry (a) has an integral breadth B defined according of the reflection with Miller indices (110) of less than 0.800 scan units in an X-ray powder pattern recorded on an oriented glycolated sample of the hormite clay fraction using Cu-Kai-radiation, in a liquid composition comprising at least one unsaturated polyester. The invention also relates to a process for producing a mixed mineral organoclay rheology additive and the use of the thus produced additive as a thickening agent in liquid compositions.
    • 本发明涉及至少一种混合矿物有机粘土流变学添加剂的用途,其包含季化烷基铵盐处理的矿物粘土混合物或由其组成,所述季化烷基铵盐处理的矿物粘土混合物通过形成含水溶胶粘土浆料(a) ,形成含水蒙皂石粘土浆料(b),将含水蒙脱石粘土浆料(a)与含水蒙脱石粘土浆料(b)混合以形成合并的粘土浆料(c),用一种或 更多季铵烷基铵盐,将由此制得的季烷基铵盐处理的矿物粘土混合物与含水介质分离,其中通过(i.1)分散一种或多种 (b)由(ii.1)将一部分一种或多种蒙脱石粘土分散于含水介质中以形成分散体以形成分散体,以及(ii)将含水蒙脱石粘土分散于 形成一个分散 n,并且在该组合粘土浆料(c)中,该粘土含量超过该蒙脱石粘土含量的重量; 并且在进行步骤iii之前使(i.1)和(ii.1)中形成的分散体经受高速流体剪切。 和/或在执行步骤iii之后; 并且其中用于形成含水方酸铝粘土浆料(a)的一种或多种方沸石粘土的分数具有根据在X射线下小于0.800个扫描单位的密勒指数(110)的反射定义的整体宽度B 在包含至少一种不饱和聚酯的液体组合物中使用Cu-Kai-辐射记录在方沸石粘土部分的取向甘油化样品上的粉末图案。 本发明还涉及生产混合矿物有机粘土流变学添加剂的方法以及由此生产的添加剂作为增稠剂在液体组合物中的用途。
    • 2. 发明申请
    • A PROCESS OF MANUFACTURING THICKENERS AND THE USE OF THUS PRODUCED THICKENERS IN HIGH-VISCOSITY UNSATURATED POLYESTER CONTAINING FORMULATIONS
    • 在高粘度不饱和聚酯制剂中制造增稠剂的方法和使用制造的增稠剂的方法
    • WO2017220502A1
    • 2017-12-28
    • PCT/EP2017/064958
    • 2017-06-19
    • BYK-CHEMIE GMBHBYK USA, INC.
    • DZIWOK, KlausCOUTELLE, HelmutBRIELL, Robert
    • C01B33/04C08K3/34C08K9/04C08K5/19C08J3/20
    • The invention relates to the use of at least one mixed mineral organoclay rheology additive, which comprises or consists of a quaternary alkyl-ammonium salt treated mineral clay mixture prepared by forming an aqueous hormite clay slurry (a), forming an aqueous smectite clay slurry (b), combining the aqueous hormite clay slurry (a) with the aqueous smectite clay slurry (b) to form a combined clay slurry (c), treating the combined clay slurry (c) with one or more quaternary alkyl-ammonium salts, separating the thus produced quaternary alkyl-ammonium salt treated mineral clay mixture from the aqueous medium, in which the aqueous hormite clay slurry (a) being formed by (i.1) dispersing a fraction of one or more hormite clays selected from the group of sepiolites and palygorskites in an aqueous medium to form a dispersion, and the aqueous smectite clay slurry (b) being formed by (ii.1) dispersing a fraction of one or more smectite clays in an aqueous medium to form a dispersion, and in that the weight of the hormite clay content exceeds the weight of the smectite clay content in the combined clay slurry (c); and subjecting the dispersions formed in (i.1) and (ii.1) to high speed fluid shear before carrying out step iii. and/or after having carried out step iii; and wherein the one or more hormite clays employed in the formation of the aqueous hormite clay slurry (a) exhibit a methylene blue exchange capacity below 20 mmol methylene blue per 100 g of the one or more hormite clays in dry state, the methylene blue exchange capacity being determined on the part of an aqueous hormite clay slurry that passes a 100 mesh U.S. standard screen, and the hormite clay slurry before passing the 100 mesh U.S. standard screen having a particle size distribution such that at least 90 % by weight of the hormite clay contained in the aqueous hormite clay slurry passes the 100 mesh U.S. standard screen, in a liquid composition comprising at least one unsaturated polyester. The invention also relates to a process for producing a mixed mineral organoclay rheology additive and the use of the thus produced additive as a thickening agent in liquid compositions.
    • 本发明涉及至少一种混合矿物有机粘土流变学添加剂的用途,其包含季化烷基铵盐处理的矿物粘土混合物或由其组成,所述季化烷基铵盐处理的矿物粘土混合物通过形成含水溶胶粘土浆料(a) ,形成含水蒙皂石粘土浆料(b),将含水蒙脱石粘土浆料(a)与含水蒙脱石粘土浆料(b)混合以形成合并的粘土浆料(c),用一种或 更多季铵烷基铵盐,将由此制得的季烷基铵盐处理的矿物粘土混合物与含水介质分离,其中通过(i.1)分散一种或多种 (b)由(ii.1)将一部分一种或多种蒙脱石粘土分散于含水介质中以形成分散体以形成分散体,以及(ii)将含水蒙脱石粘土分散于 形成一个分散 n,并且在该组合粘土浆料(c)中,该粘土含量超过该蒙脱石粘土含量的重量; 并且在进行步骤iii之前使(i.1)和(ii.1)中形成的分散体经受高速流体剪切。 和/或在执行步骤iii之后; 并且其中用于形成含水溶胶粘土浆料(a)的一种或多种方沸石粘土表现出低于20mmol亚甲基蓝的亚甲基蓝交换容量/ 100g干燥状态下的一种或多种粘土矿物粘土,亚甲基蓝交换 在通过100目美国标准筛的含水的方沸石粘土浆料部分上测定容量,并且在通过100目美国标准筛网之前的方酸钙粘土浆料的粒度分布使得至少90重量%的方酸铝 在包含至少一种不饱和聚酯的液体组合物中,包含在含水溶胶粘土浆料中的粘土通过100目美国标准筛网。 本发明还涉及生产混合矿物有机粘土流变学添加剂的方法以及由此生产的添加剂作为增稠剂在液体组合物中的用途。
    • 3. 发明申请
    • A PROCESS OF MANUFACTURING THICKENERS AND THE USE OF THUS PRODUCED THICKENERS IN HIGH-VISCOSITY NON AQUEOUS FORMULATIONS
    • 一种制造增稠剂的方法及其在高粘度非水性制剂中使用制造的增稠剂的用途
    • WO2017220507A1
    • 2017-12-28
    • PCT/EP2017/064967
    • 2017-06-19
    • BYK-CHEMIE GMBHBYK USA, INC.
    • DZIWOK, KlausCOUTELLE, HelmutBRIELL, RobertNASH, Tyler
    • C01B33/44C08K3/34C08L67/06C08L63/00
    • The invention relates to the use of at least one mixed mineral organoclay rheology additive, which comprises or consists of a quaternary alkyl-ammonium salt treated mineral clay mixture prepared by forming an aqueous hormite clay slurry (a), forming an aqueous smectite clay slurry (b), combining the aqueous hormite clay slurry (a) with the aqueous smectite clay slurry (b) to form a combined clay slurry (c), treating the combined clay slurry (c) with one or more quaternary alkyl- ammonium salts, in which the aqueous hormite clay slurry (a) being formed by dispersing a fraction of one or more hormite clays selected from the group of sepiolites and palygorskites in an aqueous medium to form a dispersion, and whereby the hormite clay fraction employed contains less than 3.0 % by weight of AI 2 O 3 , less than 1.0 % by weight of Fe 2 O 3 , and less than 3.5 % by weight of the combination of AI 2 O 3 and Fe 2 O 3 ; and the aqueous smectite clay slurry (b) being formed by dispersing a fraction of one or more smectite clays in an aqueous medium to form a dispersion, and in that the weight of the hormite clay content exceeds the weight of the smectite clay content in the combined clay slurry (c); and subjecting the hormite clay slurry (a) and the smectite clay slurry (b) to high speed fluid shear before combining both slurries and/or after having both slurries combined and wherein the one or more hormite clays employed in the formation of the aqueous hormite clay slurry (a) exhibit a methylene blue exchange capacity below 20 mmol methylene blue per 100 g of the one or more hormite clays in dry state and whereby the hormite clay fraction employed in the formation of the aqueous hormite clay slurry (a) shows an integral breadth B = (net area of reflection)/(net height of reflection) of the (110) reflection in an X-ray powder pattern recorded on an oriented glycolated sample of the hormite clay fraction using CuKΡ α - radiation of less than 0.800 scan units, in a liquid composition. The invention also relates to a process for producing a mixed mineral organoclay rheology additive and the use of the thus produced additive as a thickening agent in liquid compositions.
    • 本发明涉及至少一种混合矿物有机粘土流变学添加剂的用途,其包含季化烷基铵盐处理的矿物粘土混合物或由其组成,所述季化烷基铵盐处理的矿物粘土混合物通过形成含水溶胶粘土浆料(a) ,形成含水蒙皂石粘土浆料(b),将含水蒙脱石粘土浆料(a)与含水蒙脱石粘土浆料(b)混合以形成合并的粘土浆料(c),用一种或 更多季铵烷基铵盐,其中通过将一种或多种选自海泡石和坡缕石的一种或多种粘土粘土的一部分分散在含水介质中以形成分散体而形成含水溶胶粘土浆料(a),并且由此所述溶胶 使用的粘土部分含有小于3.0重量%的Al 2 O 3:小于1.0重量%的Fe 2 O 3: 3和低于3.5重量%的Al 2 O 3 O 3和Fe 2 O 3的组合, > 3 ; 和通过将一部分一种或多种蒙脱石粘土分散在含水介质中以形成分散体而形成的含水蒙脱石粘土浆料(b),并且所述粘土粘土含量的重量超过所述蒙脱石粘土的蒙脱石粘土含量 结合粘土泥浆(c); 并且在合并两种浆料之前和/或在两种浆料结合之后,使角质粘土浆料(a)和蒙脱石粘土浆料(b)经受高速流体剪切,并且其中在形成水溶胶中使用的一种或多种角铝石粘土 粘土浆料(a)在干燥状态下每100g一种或多种粘土矿物粘土表现出低于20mmol亚甲基蓝的亚甲基蓝交换容量,并且其中用于形成含水粘质土粘土浆料(a)的粘土矿物部分表现出 积分宽度B =(X射线粉末图案中的(110)反射的净积分面积(净反射面积)/(净反射高度),使用CuKPαα - 在液体组合物中小于0.800扫描单位的辐射。 本发明还涉及生产混合矿物有机粘土流变学添加剂的方法以及由此生产的添加剂作为增稠剂在液体组合物中的用途。
    • 4. 发明申请
    • A PROCESS OF MANUFACTURING THICKENERS AND THE USE OF THUS PRODUCED THICKENERS IN HIGH-VISCOSITY EPOXY RESIN FORMULATIONS
    • 在高粘度环氧树脂配方中制造增稠剂的过程和使用该产生的增稠剂的方法
    • WO2017220497A1
    • 2017-12-28
    • PCT/EP2017/064945
    • 2017-06-19
    • BYK-CHEMIE GMBHBYK USA, INC.
    • DZIWOK, KlausCOUTELLE, HelmutBRIELL, RobertNASH, Tyler
    • C01B33/44C08K3/34C08K9/04C09C1/42C08J3/20C08K5/19
    • The invention relates to the use of at least one mixed mineral organoclay rheology additive in a liquid composition comprising at least one epoxy resin, the additive comprises or consists of a quaternary alkyl-ammonium salt treated mineral clay mixture prepared by forming an aqueous hormite clay slurry (a), forming an aqueous smectite clay slurry (b) combining the aqueous hormite clay slurry (a) with the aqueous smectite clay slurry (b) to form a combined clay slurry (c), treating the combined clay slurry (c) with one or more quaternary alkyl-ammonium salts, in which the aqueous hormite clay slurry (a) being formed by (i.1) dispersing a fraction of one or more hormite clays selected from the group of sepiolites and palygorskites in an aqueous medium to form a dispersion, and wherein the hormite clay fraction employed contains less than 3.0 % by weight of AI 2 O 3 , less than 1.0 % by weight of Fe 2 O 3 , and less than 3.5 % by weight of the combination of AI 2 O 3 and Fe 2 O 3 , and the aqueous smectite clay slurry (b) being formed by (ii.1) dispersing a fraction of one or more smectite clays in an aqueous medium to form a dispersion, and in that the weight of the hormite clay content exceeds the weight of the smectite clay content in the combined clay slurry I; and subjecting the dispersions formed in (i.1) and (ii.1) to high speed fluid shear before carrying out step iii. and/or after having carried out step iii, in a liquid composition comprising at least one epoxy resin. The invention also relates to a process for producing a mixed mineral organoclay rheology additive and the use of the thus produced additive as a thickening agent in liquid compositions.
    • 本发明涉及至少一种混合矿物有机粘土流变学添加剂在包含至少一种环氧树脂的液体组合物中的用途,所述添加剂包含季烷基铵盐处理的矿物粘土混合物或由季烷基铵盐处理的矿物粘土混合物 通过形成含水的方沸石粘土浆料(a),形成含水的蒙脱石粘土浆料(b),将含水的方沸石粘土浆料(a)与含水蒙脱石粘土浆料(b)合并以形成合并的粘土浆料(c) (c)与一种或多种季烷基铵盐的混合粘土浆料,其中通过(i.1)分散一种或多种选自海泡石族组的一种或多种粘土粘土形成含水的角砾陶土浆料(a) 和坡缕石在含水介质中反应以形成分散体,并且其中所使用的所述方沸石粘土组分包含小于3.0重量%的Al 2 O 3:小于1.0重量% Fe 2 O 3的重量以及按重量计小于3.5% Al 2 O 3和Fe 2 O 3 3的组合以及含水蒙脱石粘土浆料(b) (ii.1)将一部分一种或多种蒙脱石粘土分散在含水介质中以形成分散体,并且其中粘土粘土含量的重量超过组合粘土浆液I中蒙脱石粘土含量的重量 ; 并且在进行步骤iii之前使(i.1)和(ii.1)中形成的分散体经受高速流体剪切。 和/或在进行步骤iii之后,在包含至少一种环氧树脂的液体组合物中进行。 本发明还涉及生产混合矿物有机粘土流变学添加剂的方法以及由此生产的添加剂作为增稠剂在液体组合物中的用途。
    • 5. 发明申请
    • EMULSION, VERFAHREN ZU IHRER HERSTELLUNG UND IHRE VERWENDUNG
    • 乳化,生产过程及其使用
    • WO2017211748A1
    • 2017-12-14
    • PCT/EP2017/063571
    • 2017-06-02
    • BYK-CHEMIE GMBH
    • NAGELSDIEK, RenéBÜHNE, SylviaKLEIN, AgnethaSAUERLÄNDER, ChristianLENZ, Jan
    • C09K8/28
    • Die Erfindung betrifft eine Emulsion enthaltend oder bestehend aus (A) 40,00 bis 97,98 Gew.-% mindestens eines Kohlenwasserstoffs, (B) 2,00 bis 59,98 Gew.-% Wasser oder einer wässrigen Lösung eines Salzes, das nicht unter die folgende Definition gemäß (C) fällt und (C) 0,02 bis 8,00 Gew.-% eines Salzes aus einem Aminoamid einer Fettsäure, das mindestens eine primäre, sekundäre oder tertiäre Aminogruppe enthält, und einer sauren Komponente der allgemeinen Formel (I), in der R 1 ein linearer oder verzweigter, gesättigter oder einfach oder mehrfach ungesättigter Kohlenwasserstoffrest mit 1 bis 40 C-Atomen ist, R 2 ein Alkylen- oder Arylalkylenrest mit 2 bis 20 C-Atomen ist und X ein Rest ist, der mindestens eine saure Gruppe enthält, m = 0 oder 1 ist, n = 1 bis 30 ist, wobei die Gewichtsanteile der Komponenten (A), (B) und (C) auf die Summe der Massen dieser Komponenten bezogen sind und diese 100 Gew.-% beträgt. Die Erfindung betrifft auch ein Verfahren zur Herstellung der Emulsion, eine ölbasierte Bohrflüssigkeit und ein Verfahren zur Erstellung und Stabilisierung eines Bohrlochs.
    • 本发明涉及含有或由以下组分组成的乳液:(A)40.00至97.98重量%的至少一种烃,(B)2.00至59.98重量%的水 或不属于以下定义的盐的水溶液。 (C)和(C)0.02-8.00重量%的含有至少一个伯氨基,仲氨基或叔氨基的脂肪酸的氨基酰胺的盐, 和通式(I)的酸性组分,其中R 1是具有1-40个碳原子的直链或支链,饱和或单不饱和或多不饱和烃基,R