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81. 发明公开

EP2103571A1 A method of removing fluoride impurities from trona and preparation of sodium bicarbonate 审中-公开
标题翻译：一种用于从Tronit去除碳酸氢钠的氟化物杂质和生产过程
公开(公告)号：EP2103571A1
公开(公告)日：2009-09-23
申请号：EP09155475.8
申请日：2009-03-18
申请人： Tata Chemicals Limited
发明人： Sensarma, Soumen , Phadtare, Sumant , Sastry, Murali
IPC分类号： C01D7/10 , C01D7/26
CPC分类号： C01D7/26 , C01D7/10 , C01P2004/61 , C01P2006/20 , C01P2006/80
摘要： The invention relates to a method of preparing sodium bicarbonate from trona containing sodium fluoride as an impurity comprising preparing a saturated solution of trona and filtering the trona solution to remove insoluble impurities; introducing carbon dioxide to the trona solution till the pH of the solution reaches the range of 7.5 to 8.75 and sodium carbonate in the trona solution is converted to sodium bicarbonate that precipitates; and recovering the precipitated sodium bicarbonate from the trona solution.
摘要翻译：本发明涉及一种制备由含有氟化钠为在包括杂质制备天然碱的饱和溶液天然碱碳酸氢钠和过滤所述天然碱溶液以除去不溶性杂质的方法; 引入二氧化碳于天然碱溶液直到溶液的pH达到7.5至8.75，并在天然碱溶液碳酸钠的范围被转换为碳酸氢钠那样的析出物; 并从该天然碱溶液沉淀的碳酸氢钠。

82. 发明公开

EP1030819A4 IMMUNOGENIC CONJUGATED POLYPEPTIDE FOR TREATMENT OF HERPES SIMPLEX VIRUS 审中-公开
标题翻译：免疫原性共轭多肽的单纯疱疹病毒的治疗
公开(公告)号：EP1030819A4
公开(公告)日：2001-11-21
申请号：EP98953226
申请日：1998-09-29
申请人： CEL SCI CORP , UNIV NORTHEASTERN OHIO
发明人： ZIMMERMAN DANIEL H , ROSENTHAL KENNETH S
IPC分类号： A61K38/00 , A61K39/00 , A61K39/245 , A61K39/385 , A61P31/22 , C07K14/035 , C07K14/47 , C07K14/74 , C07K19/00 , C01D1/32 , A61K39/12 , C01D3/16 , C01D7/26 , C07K14/705 , C22B26/10
CPC分类号： C07K14/70539 , A61K39/00 , C07K14/005 , C07K2319/00 , C12N2710/16622

83. 发明专利

JP6159527B2 炭酸水素ナトリウムの製造方法及び炭酸水素ナトリウムの製造装置有权
公开(公告)号：JP6159527B2
公开(公告)日：2017-07-05
申请号：JP2012287988
申请日：2012-12-28
申请人：オルガノ株式会社
发明人：清水和彦 , 鳥羽裕一郎 , 今村英二 , 志村光則 , 篠原雅世 , 今濱敏信 , 金賢兒
IPC分类号： C02F1/42 , C01D7/26
CPC分类号： C01D7/00 , C02F1/42 , C02F2001/422 , C02F2103/10 , C02F2209/06 , C02F2209/29 , C02F2303/16

84. 发明专利

JP2009167050A Method for producing high purity alkali metal carbonate aqueous solution 审中-公开
标题翻译：生产高纯度碱金属碳酸盐水溶液的方法
公开(公告)号：JP2009167050A
公开(公告)日：2009-07-30
申请号：JP2008006221
申请日：2008-01-15
申请人： Toagosei Co Ltd , 東亞合成株式会社
发明人： IHARA TAKASHI , OSAKABE TSUGIKATSU
IPC分类号： C01D7/26 , B01J45/00 , C02F1/42
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a high purity alkali metal carbonate aqueous solution where a coarse alkali metal carbonate aqueous solution can be refined by removing a heavy metal contained in the coarse alkali metal carbonate aqueous solution. SOLUTION: In the method for producing the high purity alkali metal carbonate aqueous solution, the heavy metal in the coarse alkali metal carbonate aqueous solution is removed by using a chelate resin having an aminophosphate group as a functional group. At least one kind among iron, copper, nickel, lead, aluminum, manganese, titanium, cobalt, zinc and cadmium is quoted as the heavy metal. It is favorable that the concentration of an alkali metal carbonate contained in the coarse alkali metal carbonate aqueous solution is 15-60 mass% when the total amount of the coarse alkali metal carbonate aqueous solution is 100 mass% and that the heavy metal is 5,000 ng/g or less. The heavy metal contained in the high purity alkali metal carbonate aqueous solution can be 500 ng/g or less. The chelate resin having the aminophosphate group is 0.1-20 mass%. COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：要解决的问题：提供一种高纯度碱金属碳酸盐水溶液的制造方法，其中粗碱金属碳酸盐水溶液可以通过除去粗碱金属碳酸盐水溶液中所含的重金属来精制。解决方案：在高纯碱金属碳酸盐水溶液的制造方法中，通过使用具有氨基磷酸基作为官能团的螯合树脂，除去粗碱金属碳酸盐水溶液中的重金属。铁，铜，镍，铅，铝，锰，钛，钴，锌和镉中至少有一种称为重金属。当粗碱金属碳酸盐水溶液的总量为100质量％，重金属为5,000ng时，碱土金属碳酸盐水溶液中所含的碱金属碳酸盐的浓度为15〜60质量％ / g以下。高纯度碱金属碳酸盐水溶液中所含的重金属可以为500ng / g以下。具有氨基磷酸酯基的螯合树脂为0.1-20质量％。版权所有（C）2009，JPO＆INPIT

85. 发明专利

JP2009167036A Method for producing high purity alkali metal carbonate aqueous solution 审中-公开
标题翻译：生产高纯度碱金属碳酸盐水溶液的方法
公开(公告)号：JP2009167036A
公开(公告)日：2009-07-30
申请号：JP2008005010
申请日：2008-01-11
申请人： Toagosei Co Ltd , Tsurumi Soda Co Ltd , 東亞合成株式会社 , 鶴見曹達株式会社
发明人： IHARA TAKASHI , OSAKABE TSUGIKATSU
IPC分类号： C01D7/26 , B01J45/00 , C02F1/42
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a high purity alkali metal carbonate aqueous solution where a coarse alkali metal carbonate aqueous solution can be refined by removing a heavy metal contained in the coarse alkali metal carbonate aqueous solution. SOLUTION: In the method for producing the high purity alkali metal carbonate aqueous solution, the heavy metal in the coarse alkali metal carbonate aqueous solution is removed by using a chelate resin having an amidino group as a functional group. At least one kind among iron, copper, nickel, lead, aluminum, manganese, titanium, cobalt, zinc and cadmium is quoted as the heavy metal. It is favorable that the concentration of an alkali metal carbonate contained in the coarse alkali metal carbonate aqueous solution is 15-60 mass% when the total amount of the coarse alkali metal carbonate aqueous solution is 100 mass% and that the heavy metal is 5,000 ng/g or less. The heavy metal contained in the high purity alkali metal carbonate aqueous solution can be 500 ng/g or less. The chelate resin having the amidino group is 0.1-20 mass%. COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：要解决的问题：提供一种高纯度碱金属碳酸盐水溶液的制造方法，其中粗碱金属碳酸盐水溶液可以通过除去粗碱金属碳酸盐水溶液中所含的重金属来精制。解决方案：在高纯度碱金属碳酸盐水溶液的制造方法中，通过使用具有脒基作为官能团的螯合树脂，除去粗碱金属碳酸盐水溶液中的重金属。铁，铜，镍，铅，铝，锰，钛，钴，锌和镉中至少有一种称为重金属。当粗碱金属碳酸盐水溶液的总量为100质量％，重金属为5,000ng时，碱土金属碳酸盐水溶液中所含的碱金属碳酸盐的浓度为15〜60质量％ / g以下。高纯度碱金属碳酸盐水溶液中所含的重金属可以为500ng / g以下。具有脒基的螯合树脂为0.1-20质量％。版权所有（C）2009，JPO＆INPIT

86. 发明专利

JPH11310413A PRODUCTION OF HIGHLY PURE LITHIUM CARBONATE 失效
公开(公告)号：JPH11310413A
公开(公告)日：1999-11-09
申请号：JP13271398
申请日：1998-04-27
申请人： MITSUI CHEMICALS INC
发明人： IWASAKI HIROSHI , TAN HIROAKI , FURUYA KATSUAKI
IPC分类号： C01D7/26 , C01D15/08
摘要： PROBLEM TO BE SOLVED: To provide a method for producing highly pure lithium carbonate, capable of supplying the highly pure, singly crystalline lithium carbonate having a large primary particle diameter and not containing secondary aggregates in a high yield. SOLUTION: This method for producing highly pure lithium carbonate comprises (i) a dissolution process for introducing carbon dioxide into a pure lithium carbonate aqueous slurry under pressurization to dissolve the lithium carbonate, (ii) a degasification crystallization process for subjecting the aqueous solution containing the carbon dioxide and the lithium carbonate to a pressure- reducing treatment to vaporize the carbon dioxide and simultaneously precipitate the lithium carbonate crystals, and (iii) a separative recovery process for separating and recovering the precipitated lithium carbonate crystals from the solution.

87. 发明专利

JPS6445715A PRODUCTION OF HIGH-PURITY METALLIC COMPOUND 失效
公开(公告)号：JPS6445715A
公开(公告)日：1989-02-20
申请号：JP7207888
申请日：1988-03-28
申请人： CENTRAL GLASS CO LTD
发明人： YAMASHITA HIDEFUMI , KAWAMOTO HIROMI , NISHIMURA NATSUYA
IPC分类号： C01B9/00 , C01B17/96 , C01B21/48 , C01D3/16 , C01D7/26 , C01D13/00 , C01F7/48 , C01F11/20 , C01F17/00 , C01G15/00 , C01G25/00 , C09K3/00
摘要： PURPOSE:To obtain a high-purity metallic soluble salt and to obtain various high-purity metallic compounds from the soluble salt as a raw material, by using a relatively inexpensive and readily obtainable metallic soluble salt, adding a specific chelating agent to an aqueous solution of the soluble salt and removing formed precipitate. CONSTITUTION:An aqueous solution of at least one soluble salt of a metal selected from alkali metals, alkaline earth metals, lanthanide metals, zirconium, yttrium, indium and aluminum is maintained at pH 1.0-11 and incorporated with >=0.005wt.% based on the raw material compound of ammonium diethyldithiocarbamate or ammonium pyrrolidinedithiocarbamate. Then formed precipitated is filtered and removed to give a high-purity metallic soluble salt. The high-purity metallic salt is directly used in the aqueous solution as it is or crystallized and can be converted into high-purity oxide, halide, sulfate, carbonate or nitrate by a proper treatment. The high-purity metallic compound obtained by the above-mentioned method has impurities of transition metal reduced to order of ppb.

88. 发明专利

JPS6127326B2 JPS6127326B2 - 失效
公开(公告)号：JPS6127326B2
公开(公告)日：1986-06-25
申请号：JP770778
申请日：1978-01-26
申请人： Tokuyama Sooda Kk , Sumitomo Kinzoku Kogyo Kk
发明人： YAMADA KAZUNARI , IBA MASAHISA , MARUKAWA JUJO , OKAMOTO SETSUO
IPC分类号： C01D7/00 , C01D7/26 , C22B1/00 , C22B7/04
CPC分类号： C22B7/04 , Y02P10/212

89. 发明专利

JPS5788022A REMOVING METHOD FOR PHOSPHOROUS, SULFUR AND SILICON IN REFINING SLAG CONTAINING ALKALI METALLIC COMPOUND 失效
公开(公告)号：JPS5788022A
公开(公告)日：1982-06-01
申请号：JP16464980
申请日：1980-11-25
申请人： NIPPON KOKAN KK
发明人： YAMASHITA YUU , TAJIMA KAZUO
IPC分类号： C22B26/10 , C01D7/00 , C01D7/26 , C01D13/00 , C22B7/04
摘要： PURPOSE:To efficiently conduct the titled removal and to recover a high quality alkali metal by adding calcined dolomite limestone or the like to a soln. extracted from refining slag contg. an alkali metallic compound to make P, S and Si difficultly soluble and by filtering them off. CONSTITUTION:Molten iron is refined with an alkali metallic compound to remove S and P, and produced slag is crushed to a prescribed grain size. The crushed slag (a) is fed to an extraction vessel 1, and a satd. soln. of sodium hydrogencarbonate (b) and part of a filtrate separated from a filter 3 as a refluxing soln. (c) are supplied. By blowing a synthetic gas (d) consisting of CO2, O2 and N2, the pH of an extracted soln. in the vessel 1 is kept at a prescribed value. A slurry prepared by extraction is fed from the vessel 1 to a vessel 4 for removing P, S and Si, calcined dolomite limestone, calcined dolomite or hydroxide thereof is added as a removing agent (e), and a similar synthetic gas (d) for adjusting the pH is blown. P, S and Si made difficultly or slightly soluble by the agent (e) are filtered off with the filter 3 together with undissolved residue, and a high quality extracted soln. is recovered.

90. 发明专利

JPS54100999A TREATMENT OF WASTE SLAG 失效
公开(公告)号：JPS54100999A
公开(公告)日：1979-08-09
申请号：JP770778
申请日：1978-01-26
申请人： TOKUYAMA SODA KK , SUMITOMO METAL IND
发明人： YAMADA KAZUNARI , IBA MASAHISA , MARUKAWA YUUJIYOU , OKAMOTO SETSUO
IPC分类号： C01D7/00 , C01D7/26 , C22B1/00 , C22B7/04
摘要： PURPOSE:To recover high purity alkali carbonate which is reusable from filtrate by the procedure in which waste slag produced when molten pig iron is desulfurized or dephosphorated by an alkali carbonate is extracted with hot water while blowing CO2 into the apparatus, and then the extracted solution is mixed with iron ion and sediment is filtered. CONSTITUTION:The molten pig iron obtained at the blast furnace 1 is sent to the desulfurization and dephosphoration process 2 to cause reaction with Na2CO3 added in a fixed amount, whereby S is converted into Na2S and P is converted into sodium phosphate. And, the pig iron thus treated is sent to the converter 6 and mixed with CaO, etc. for refining, and then sent to the casting process 7. On the other hand, the waste slag formed in the process 2 is sent to the extraction and washing process 3, where extraction and washing are made with hot water while injecting CO2-containing gas to crystallize most of S ion in the form of iron sulfide. And, the extracted solution is sent to the sedimentation tank 4 and mixed with iron ion to precipitate iron sulfide and iron phosphate and removed them. Then, the filtrate is concentrated and then sent to the fractional crystallization process 5 to separate NaCO3 sediment for removal and recovery.

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