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    • 88. 发明申请
    • DISTILLATION EQUIPMENT FOR PRODUCING SPONGE TITANIUM
    • 用于生产海绵钛的蒸馏设备
    • US20120306131A1
    • 2012-12-06
    • US13585715
    • 2012-08-14
    • Xuemin CHENQingdong YELiping HUMing YIN
    • Xuemin CHENQingdong YELiping HUMing YIN
    • C22B9/00
    • C22B34/1277F27B14/04F27B19/04
    • The present invention provides a piece of distillation equipment for producing sponge titanium, which includes a heating furnace and a reactor for containing a condensate, wherein a heating furnace cover is arranged above the heating furnace, a reactor cover is arranged above the reactor, the heating furnace cover is connected with the reactor cover by a pipe, a resistance wire is arranged on the pipe, each lifting device is arranged above the heating furnace cover and the reactor cover, a vacuum-pumping pipe is arranged above a heater cover, and a first metal sealing ring is arranged between the reactor cover and the reactor. The present invention has the beneficial effects that the distillation equipment can ensure normal production, and effectively ensure the quality of sponge titanium product. The problem of distillation tube blockage is solved by adopting a metal gasket.
    • 本发明提供一种用于生产海绵钛的蒸馏设备,其包括加热炉和用于容纳冷凝物的反应器,其中加热炉盖布置在加热炉上方,反应器盖布置在反应器上方,加热 炉盖通过管道与反应堆盖连接,管道上布置有电阻丝,每个提升装置设置在加热炉盖和反应堆盖上方,真空抽吸管布置在加热器盖的上方, 第一金属密封环设置在反应器盖和反应器之间。 本发明具有蒸馏设备可以保证正常生产,有效保证海绵钛产品质量的有益效果。 蒸馏管堵塞的问题是采用金属垫片来解决的。
    • 90. 发明申请
    • METHOD FOR PREPARING SPONGE TITANIUM FROM POTASSIUM FLUOTITANATE BY ALUMINOTHERMIC REDUCTION
    • 通过氧化铝还原从氟磷酸钙制备海绵钛的方法
    • US20120304823A1
    • 2012-12-06
    • US13585721
    • 2012-08-14
    • Xuemin CHENJun YANGZhi ZHOU
    • Xuemin CHENJun YANGZhi ZHOU
    • C22B5/00
    • C22B34/1277
    • The invention provides a method for preparing sponge titanium from potassium fluotitanate by aluminothermic reduction, comprising the following steps: a reaction step: aluminum and zinc are mixed under a vacuum state, and the mixture is then reacted with potassium fluotitanate; a distillation step: KF, AlF3 and Zn generated by reaction are distilled out under a vacuum state; and a cooling step: sponge titanium is obtained subsequent to banking cooling. The invention further provides another method for preparing sponge titanium from potassium fluotitanate by aluminothermic reduction, comprising the following steps: a reaction step: aluminum and magnesium are mixed under a vacuum argon introduction condition, and the mixture is then reacted with potassium fluotitanate; a distillation step: KF, AlF3, MgF2 and Mg generated by reaction are distilled out under a vacuum state; and a cooling step: sponge titanium is obtained subsequent to banking cooling.
    • 本发明提供了一种通过铝热还原从氟酸钾制备海绵钛的方法,包括以下步骤:反应步骤:将铝和锌在真空状态下混合,然后使该混合物与氟钛酸钾反应; 蒸馏步骤:在真空状态下蒸馏出由反应产生的KF,AlF 3和Zn; 和冷却步骤:在银行冷却之后获得海绵钛。 本发明还提供另一种通过铝热还原由氟钛酸钾制备海绵钛的方法,包括以下步骤:反应步骤:在真空氩气引入条件下将铝和镁混合,然后使该混合物与氟钛酸钾反应; 蒸馏步骤:在真空状态下蒸馏出由反应产生的KF,AlF 3,MgF 2和Mg; 和冷却步骤:在银行冷却之后获得海绵钛。