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81. 发明授权

US09550147B2 Particulate, heterogeneous solid CO2 absorbent composition, method for its preparation and use thereof 有权
标题翻译：颗粒状，非均质固体二氧化碳吸收剂组合物，其制备方法及用途
公开(公告)号：US09550147B2
公开(公告)日：2017-01-24
申请号：US13382919
申请日：2010-07-06
申请人： Johann Mastin , Julien Meyer , Arne Raaheim
发明人： Johann Mastin , Julien Meyer , Arne Raaheim
IPC分类号： B01D53/02 , B01D53/62 , C01F11/04 , C01F7/16 , B01J20/04 , B01J20/08 , B01J20/30 , B01J20/32 , B01J20/34
CPC分类号： B01D53/62 , B01D53/02 , B01D2251/404 , B01D2253/104 , B01D2257/504 , B01J20/041 , B01J20/08 , B01J20/3035 , B01J20/3078 , B01J20/3204 , B01J20/3236 , B01J20/3433 , B01J20/3483 , B01J2220/4806 , B01J2220/56 , C01F7/164 , C01F11/04 , C01P2002/72 , C01P2002/85 , C01P2002/88 , C01P2004/03 , C01P2004/32 , C01P2004/62 , Y02C10/04 , Y02C10/08 , Y02P20/152
摘要： A particulate, heterogeneous solid CO2 absorbent composition, comprising decomposition products of Ca3Al2O6 after having been heated to a temperature between 500° C. and 925° C. in the presence of H2O and CO2 for a period of time sufficient to allow the Ca3Al2O6 to react and form the particulate, heterogeneous absorbent composition which exhibits a higher concentration of aluminum than calcium in the particle core but a higher concentration of calcium than aluminum at the particle surface. The invention also comprises a method for preparing the particulate, heterogeneous product as well as a method for utilizing the composition for separating CO2 from a process gas.
摘要翻译：在H 2 O和CO 2存在下，将Ca 3 Al 2 O 6的分解产物加热到500℃至925℃之间的温度下，Ca 3 Al 2 O 6反应的时间足以使Ca 3 Al 2 O 6反应并且形成颗粒状非均相吸收剂组合物，其在颗粒芯中表现出比钙更高的铝浓度，但在颗粒表面具有比铝高的钙浓度。本发明还包括一种制备颗粒状非均质产品的方法以及一种利用该组合物从工艺气体中分离CO 2的方法。

82. 发明申请

US20160369148A1 THERMALLY CONDUCTIVE COMPLEX OXIDE, PRODUCTION METHOD THEREFOR, THERMALLY CONDUCTIVE COMPLEX OXIDE-CONTAINING COMPOSITION, AND USE THEREFOR 审中-公开
标题翻译：导热复合氧化物，其生产方法，导热复合氧化物组合物及其用途
公开(公告)号：US20160369148A1
公开(公告)日：2016-12-22
申请号：US15122321
申请日：2015-03-12
申请人： DAINICHISEIKA COLOR & CHEMICALS MFG. CO., LTD.
发明人： Akira NISHIO , Toru KAWAKAMI , Kenichi YAMANE , Naotsugu YAMAMURA , Shingo TOMINAGA
IPC分类号： C09K5/14 , C01G9/00 , C01F7/16 , C09D7/12 , C09D1/00
CPC分类号： C09K5/14 , C01F7/162 , C01F7/164 , C01F7/166 , C01G9/00 , C01G9/006 , C01P2002/32 , C01P2004/10 , C01P2004/20 , C01P2004/54 , C01P2004/61 , C01P2004/62 , C01P2006/32 , C01P2006/40 , C09C1/40 , C09D1/00 , C09D7/61
摘要： An object of the present invention is to provide a thermally conductive composite oxide that can realize physical properties required for coating films, films, and molded products obtained by single use of the thermally conductive composite oxide blended into paints and resin compositions without the need for an improvement measure such as surface treatment and that is excellent in thermal conductivity, water resistance, acid resistance, and electric insulation. The object is achieved by a thermally conductive composite oxide and the production process thereof, the thermally conductive composite oxide being a composite oxide having a spinel structure and containing aluminum as a main component metal and at least one metal other than aluminum, and in the thermally conductive composite oxide, the metal other than aluminum is at least one selected from the group consisting of magnesium, zinc, calcium, and strontium, the ratio, (b mol)/(a mol), of the number of moles (b) of the metal other than aluminum to the number of moles (a) of an aluminum element in the alumina-based compound is 0.1 or more and 1.0 or less, and the Mohs hardness of the thermally conductive composite oxide is less than 9.
摘要翻译：本发明的目的是提供一种导热复合氧化物，其能够实现通过单独使用掺入到涂料和树脂组合物中的导热复合氧化物而获得的涂膜，膜和模制产品所需的物理性能，而不需要表面处理等改善措施，导热性，耐水性，耐酸性，电绝缘性优异。该目的通过导热复合氧化物及其制造方法实现，导热复合氧化物是具有尖晶石结构并且含有铝作为主要成分金属和除了铝之外的至少一种金属的复合氧化物，并且在热导电复合氧化物，除了铝以外的金属是选自镁，锌，钙和锶中的至少一种，摩尔数（b）的比（b mol）/（a mol）氧化铝系化合物中的铝以外的铝元素的摩尔数（a）为0.1以上且1.0以下，导热性复合氧化物的莫氏硬度小于9。

83. 发明授权

US09457334B2 Hydrogen production process 有权
标题翻译：氢气生产过程
公开(公告)号：US09457334B2
公开(公告)日：2016-10-04
申请号：US14759104
申请日：2014-01-09
申请人： Hitachi Zosen Corporation , Kyoto University
发明人： Susumu Hikazudani , Atsushi Wakui , Kazuyuki Hirao , Toshimi Fukui , Junko Nakamoto , Heidy H. Visbal Mendoza
IPC分类号： H01B1/02 , B01J19/12 , H01M8/06 , C01F7/16 , C01B3/06
CPC分类号： B01J19/123 , C01B3/061 , C01F7/164 , C01P2002/72 , C01P2002/84 , H01M8/0606 , Y02E60/36
摘要： The present invention provides a hydrogen production process, which is capable of producing hydrogen, which is a clean source of energy, simply and conveniently without using conventionally-used ammonia, with an extremely high level of safety. In accordance with the present invention, hydrogen is produced by substituting hydrogen for free oxygen in mayenite (Ca24Al28O644+.2O2−) to obtain hydrogen-substituted mayenite (Ca24Al28O644+.4H−) and reacting the resultant hydrogen-substituted mayenite (Ca24Al28O644+.4H−) with water to produce hydrogen, and hydrogen is produced by substituting hydrogen for free oxygen in mayenite (Ca24Al28O644+.2O2−) to obtain hydrogen-substituted mayenite (Ca24Al28O644+.4H−), irradiating the resultant hydrogen-substituted mayenite (Ca24Al28O644+.4H−) with ultraviolet rays to obtain conductive mayenite (Ca24Al28O644+.4e−), and reacting the resultant conductive mayenite (Ca24Al28O644+.4e−) with water to produce hydrogen.
摘要翻译：本发明提供一种氢生产方法，其能够以非常高的安全水平简单且方便地生产作为清洁能源的氢气，而不使用常规使用的氨。根据本发明，通过在钙铝石（Ca24Al28O644 + .2O2-）中用氢代替游离氧，得到氢取代的钙铝石（Ca24Al28O644 + .4H-），并使所得氢取代的钙铝石（Ca24Al28O644 + .4H-）用氢气生成氢，通过在钙铝石（Ca24Al28O644 + .2O2-）中用氢代替游离氧，得到氢取代的钙铝石（Ca24Al28O644 + .4H-），照射得到的氢取代的钙铝石（Ca24Al28O644 + .4H-）用紫外线获得导电的钙铝石（Ca24Al28O644 + .4e-），并使所得的导电钙铝石（Ca24Al28O644 + .4e-）与水反应产生氢。

84. 发明授权

US09428827B2 Method of manufacturing electrically conductive mayenite compound with high electron density 有权
标题翻译：具有高电子密度的导电钙铝石化合物的制造方法
公开(公告)号：US09428827B2
公开(公告)日：2016-08-30
申请号：US14659851
申请日：2015-03-17
申请人： Asahi Glass Company, Limited
发明人： Kazuhiro Ito , Satoru Watanabe , Toshinari Watanabe , Naomichi Miyakawa
IPC分类号： C04B35/44 , C23C14/34 , C01F7/00 , C01F7/16 , C04B35/117
CPC分类号： C23C14/3414 , C01F7/002 , C01F7/164 , C01P2004/61 , C01P2006/40 , C04B35/117 , C04B35/44 , C04B2235/3208 , C04B2235/445 , C04B2235/6587 , C04B2235/664
摘要： A method of manufacturing an electrically conductive mayenite compound, includes (a) preparing a body to be processed, the body to be processed including a mayenite compound or a precursor of a mayenite compound; and (b) performing a heat treatment on the body to be processed under a reducing atmosphere including an aluminum compound and carbon monoxide (CO) gas within a range of 1080° C. to 1450° C., the aluminum compound being a compound that emits aluminum oxide gas during the heat treatment on the body to be processed.
摘要翻译：一种制造导电性钙铝石化合物的方法包括（a）制备待加工体，所述被加工物包括钙铝石化合物或钙铝石化合物的前体; 和（b）在包含铝化合物和一氧化碳（CO））气体的还原气氛下，在1080℃至1450℃的范围内对被处理体进行热处理，所述铝化合物为在被加工物体的热处理过程中发出氧化铝气体。

85. 发明授权

US08377413B2 Method for preparing mayenite-containing oxide and method for preparing electroconductive mayenite-containing oxide 有权
标题翻译：制备含钙锰氧化物的方法及其制备含导电钙铝氧化物的方法
公开(公告)号：US08377413B2
公开(公告)日：2013-02-19
申请号：US13192568
申请日：2011-07-28
申请人： Kazuhiro Ito , Satoru Watanabe , Naomichi Miyakawa , Setsuro Ito , Kazunari Watanabe
发明人： Kazuhiro Ito , Satoru Watanabe , Naomichi Miyakawa , Setsuro Ito , Kazunari Watanabe
IPC分类号： C01F7/00
CPC分类号： C01F7/164 , C01P2006/40
摘要： To provide a method for preparing a mayenite-containing oxide containing a mayenite type compound and having a hydride ion density of at least 1×1018/cm3 without need for expensive facilities, control of complicated reaction conditions or a long period of reaction time. A method for preparing a mayenite-containing oxide, which comprises a firing step of heating a starting material having a molar ratio of CaO:Al2O3 being from 9:10 to 14:5 based on the oxides at a temperature of from 900 to 1,300° C. to obtain a fired powder and a hydrogenation step of firing the fired powder at a temperature of at least 1,210° C. and lower than 1,350° C. in a hydrogen-containing gas having an oxygen partial pressure of at most 1,000 Pa to obtain a mayenite-containing oxide containing a mayenite type compound and having a hydride ion density of at least 1×1018/cm3, and a method for preparing an electroconductive mayenite-containing oxide, which comprises irradiating the obtained mayenite-containing oxide with an ultraviolet ray etc. to obtain a mayenite-containing oxide containing an electroconductive mayenite type compound.
摘要翻译：为了提供一种制备含有钙铝石型化合物并且氢化物离子密度为至少1×1018 / cm3而不需要昂贵的设备，控制复杂的反应条件或长时间的反应时间的钙铝氧化物的方法。一种含有钙铝石的氧化物的制造方法，其特征在于，在900〜1300℃的温度下，对CaO：Al 2 O 3的摩尔比为9:10〜14:5的原料进行加热，以获得烧制粉末和氢化步骤，在氧分压至多为1000Pa的含氢气体中，在至少1,210℃且低于1350℃的温度下焙烧烧制粉末至得到含有钙铝石型化合物，含氢离子密度为1×1018 / cm3以上的含钙锰矿的氧化物，以及制造含导电性钙铝的氧化物的方法，其包括用紫外线照射所得到的含有钙铝的氧化物以获得含有导电钙铝石型化合物的含有钙铝的氧化物。

86. 发明申请

US20110293494A1 PROCEDURE FOR OBTAINING CALCIUM ALUMINATE FROM WASTE OBTAINED FOLLOWING TREATMENT OF SALINE DROSS FROM THE PRODUCTION OF SECONDARY ALUMINIUM 审中-公开
标题翻译：从生产二次铝中获得硫酸钙的方法从废弃物中获得的废铝
公开(公告)号：US20110293494A1
公开(公告)日：2011-12-01
申请号：US13145060
申请日：2010-01-20
申请人： José Martinez Iglesias , Alejandro Salinas Tuya , Fernando Marquinez Peña
发明人： José Martinez Iglesias , Alejandro Salinas Tuya , Fernando Marquinez Peña
IPC分类号： C01F7/16 , C22B1/245
CPC分类号： C01F7/164 , C01P2002/72 , C04B35/44 , C04B35/62204 , C04B35/6261 , C04B35/62695 , C04B35/6303 , C04B35/632 , C04B35/634 , C04B35/636 , C04B35/6365 , C04B35/653 , C04B2235/3208 , C22B7/04 , Y02P10/212
摘要： Procedure for obtaining calcium aluminate from the dry waste generated in the treatment, for recovery of metallic Al and salts, of the saline dross produced in the metallurgy of secondary aluminium and calcium oxide and/or CaO precursor. The procedure may produce briquettes or pellets of precursors of calcium aluminate through cold sintering or premolten calcium aluminate through hot sintering.
摘要翻译：在二次铝和氧化钙和/或CaO前体的冶金中生产的盐水浮渣的金属Al和盐的回收产生的干燥废物中获得铝酸钙的方法。该方法可以通过冷烧或通过热烧结产生铝酸铝前体来生产铝酸钙前体的块状或块状颗粒。

87. 发明申请

US20110182803A1 PROCESS FOR PRODUCING AN OXIDE 有权
标题翻译：生产氧化物的方法
公开(公告)号：US20110182803A1
公开(公告)日：2011-07-28
申请号：US13080769
申请日：2011-04-06
申请人： Kazuhiro ITO , Satoru Watanabe , Kazunari Watanabe , Setsuro Ito
发明人： Kazuhiro ITO , Satoru Watanabe , Kazunari Watanabe , Setsuro Ito
IPC分类号： C01F7/16
CPC分类号： C01F7/164 , C01P2004/61 , C01P2006/40
摘要： The present invention relates to a method for producing an oxide containing a conductive mayenite type compound and having an electron concentration of 1×1018/cm3 or more, from a raw material which is a combination of a calcium compound and an aluminum compound or is a compound containing calcium and aluminum, each having a molar ratio of calcium oxide and aluminum oxide ranging from 9:10 to 14:5 in terms of the oxides, the method including the steps of: heating and holding the raw material at 900 to 1,300° C. to produce a calcined powder containing at least one oxide selected from the group consisting of a calcium aluminate, calcium oxide and aluminum oxide; and heating and holding the calcined powder at 1,200° C. to less than 1,415° C. under a reduction atmosphere in an inert gas atmosphere or a vacuum atmosphere each having an oxygen partial pressure of 1,000 Pa or less.
摘要翻译：本发明涉及由钙化合物和铝化合物的组合的原料生成含有导电性钙铝石型化合物的氧化物的电子浓度为1×1018 / cm3以上的氧化物的方法，包含钙和铝的化合物，其氧化物和氧化铝的摩尔比为9:10至14:5，氧化物的方法包括以下步骤：将原料加热至900至1300℃ 以制备含有选自铝酸钙，氧化钙和氧化铝中的至少一种氧化物的煅烧粉末; 在惰性气体气氛或氧气分压为1000Pa以下的真空气氛中，在还原气氛下，将煅烧后的粉末在1,200℃加热保持至小于1415℃。

88. 发明申请

US20110155970A1 MAYENITE-TYPE COMPOUND AND PROCESS FOR PRODUCTION OF SAME 有权
标题翻译：多晶型化合物及其制造方法
公开(公告)号：US20110155970A1
公开(公告)日：2011-06-30
申请号：US13034765
申请日：2011-02-25
申请人： Kazuhiro ITO , Satoru Watanabe , Naomichi Miyakawa , Setsuro Ito
发明人： Kazuhiro ITO , Satoru Watanabe , Naomichi Miyakawa , Setsuro Ito
IPC分类号： H01B1/02
CPC分类号： C01F7/164 , C01F7/16 , C01F7/162 , C01F7/166 , C01P2002/50 , C01P2002/86 , C01P2006/40 , C01P2006/60 , H01J11/40
摘要： The present invention relates to a mayenite-type compound in which a part of Ca of a mayenite-type compound containing Ca, Al and oxygen is substituted by at least one kind of an atom M selected from the group consisting of Be, Mg and Sr, in which the mayenite-type compound has an atom number ratio represented by M/(Ca+M) of from 0.01 to 0.50, and at least a part of free oxygen ions in a mayenite-type crystal structure are substituted by anions of an atom having electron affinity smaller than that of an oxygen atom.
摘要翻译：本发明涉及一种钙铝型化合物，其中含有Ca，Al和氧的钙铝石型化合物的Ca的一部分Ca被选自Be，Mg和Sr中的至少一种原子M所取代，其中钙铝石型化合物具有由M /（Ca + M）表示的原子数比为0.01至0.50，并且钙铝石型晶体结构中的至少一部分游离氧离子被阴离子所取代具有小于氧原子的电子亲和力的原子。

89. 发明授权

US07662357B2 Hydrogen-containing electrically conductive inorganic compound 有权
标题翻译：含氢导电无机化合物
公开(公告)号：US07662357B2
公开(公告)日：2010-02-16
申请号：US10511715
申请日：2003-04-18
申请人： Hideo Hosono , Masahiro Hirano , Katsuro Hayashi
发明人： Hideo Hosono , Masahiro Hirano , Katsuro Hayashi
IPC分类号： C01F7/00
CPC分类号： H01B1/08 , C01B3/00 , C01F7/164 , C01F7/166 , C01P2006/40 , C04B35/44 , C04B2235/3208 , C04B2235/3213 , C04B2235/44 , C04B2235/6565 , C04B2235/658 , C04B2235/6582 , C04B2235/96 , C30B7/00 , C30B7/005 , Y02E60/324
摘要： Disclosed is a 12CaO.7Al2O3 compound, a 12SrO.7Al2O3 compound, or a mixed crystal compound of 12CaO.7Al2O3 and 12SrO.7Al2O3, which contains a negative hydrogen ion (H−, H2−, H2− at a concentration of 1×1018 cm−3 or more. A negative hydrogen ion comprising a primary component of a hydride ion is incorporated into C12A7 (12CaO.7Al2O3), so that a function of being converted from an insulative material to an electrically conductive material in a sustained manner by means of irradiation with light can be exhibited even in the normal atmosphere at a room temperature. The present invention also provides a solid electrolyte capable of conducting a negative hydrogen ion, and means for releasing a hydride ion from the inside of a solid into a gaseous phase using an electric field.
摘要翻译：公开了12Ca0.7Al2O3化合物，12SrO.7Al2O3化合物或12CaO.7Al2O3和12SrO.7Al2O3的混合晶体化合物，它含有负氢离子（H，H 2 - ，H 2 - 浓度为1×10 18 cm -1） 3以上，含有氢离子主要成分的负氢离子被并入到C12A7（12Ca0.7Al2O3）中，使得通过照射以持续的方式从绝缘材料转变为导电材料的功能本发明还提供能够导入负氢离子的固体电解质，以及使氢化物离子从固体内部释放到气相中的方法，使用电场。

90. 发明授权

US07507289B2 Electroconductive 12CaO—7Al2O3 and compound of same type, and method for preparation thereof 有权
标题翻译：导电性12CaO-7Al2O3和相同类型的化合物及其制备方法
公开(公告)号：US07507289B2
公开(公告)日：2009-03-24
申请号：US10561968
申请日：2004-02-12
申请人： Hideo Hosono , Masahiro Hirano , Katsuro Hayashi , Masashi Miyakawa , Isao Tanaka
发明人： Hideo Hosono , Masahiro Hirano , Katsuro Hayashi , Masashi Miyakawa , Isao Tanaka
IPC分类号： C30B1/10
CPC分类号： H01B1/08 , C01F7/164 , C01F7/166 , C01P2006/40 , C04B35/44 , C04B35/653 , C04B2235/3208 , C04B2235/3213 , C04B2235/604 , C04B2235/6587 , C04B2235/664 , C04B2235/787 , C04B2235/94
摘要： In a solid solution system of Al2O3 and CAO or SrO, it has been difficult to obtain a material having a high electrical conductivity (>10−4 S·cm−) at room temperature.A compound is provided in which electrons at a high concentration are introduced into a 12CaO.7Al2O3 compound, a 12SrO.7Al2O3 compound, or a mixed crystal compound containing 12CaO.7Al2O3 and 12SrO.7Al2O3. The compound formed by substituting all the free oxygen ions with electrons is regarded as an electride compound in which [Ca24Al28O64]4+(4e−) or [Sr24Al28O64]4+(4e−) serves as a cation and electrons serve as anions. When a single crystal or a hydrostatic pressure press molded material of a fine powder thereof is held at approximately 700° C. in an alkaline metal vapor or an alkaline earth metal vapor, melt of a hydrostatic pressure press molded material of a powder is held at approximately 1,600° C. in a carbon crucible, followed by slow cooling for solidification, or a thin film of the compound held at approximately 600° C. is implanted with rare gas ions, a great number of the free oxygen ions can be substituted with electrons.
摘要翻译：在Al 2 O 3和CAO或SrO的固溶体系中，难以在室温下获得具有高电导率（> 10 -4 S.cm-）的材料。提供了一种化合物，其中将高浓度的电子引入12CaO.7Al2O3化合物，12SrO.7Al2O3化合物或含有12CaO.7Al2O3和12SrO.7Al2O3的混合晶体化合物。通过用电子代替全部游离氧离子形成的化合物被认为是其中[Ca24Al28O64] 4+（4e-）或[Sr24Al28O64] 4+（4e-）用作阳离子的电子化合物，电子用作阴离子。当在碱金属蒸气或碱土金属蒸气中将其细粉末的单晶或静水压成型材料保持在约700℃时，将粉末的流体静压加压成型材料的熔体保持在在碳坩埚中约1600℃，然后缓慢冷却固化，或者在约600℃保持的化合物薄膜注入稀有气体离子，大量的游离氧离子可被电子。

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