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81. 发明授权

US4843156A Process for producing high-purity oligoglucosylfructosides 失效
标题翻译：生产高纯度低聚葡糖基果糖苷的方法
公开(公告)号：US4843156A
公开(公告)日：1989-06-27
申请号：US692066
申请日：1985-01-16
申请人： Toshio Miyake , Shuzo Sakai , Takashi Shibuya
发明人： Toshio Miyake , Shuzo Sakai , Takashi Shibuya
IPC分类号： A23L27/30 , C07H1/06 , C07H3/06 , C13K13/00
CPC分类号： C07H3/06 , C13K13/005
摘要： Oligoglucosylfructosides wherein an oligoglucosylfructoside having a polymerization degree of 2 or 3 glucose units are recovered in a high purity from a feed solution additionally containing substantial amounts of higher- and lower-oligosaccharides by sequentially admitting predetermined volumes of the feed solution and water to the column of a strongly-acidic cation exchange resin in alkaline-earth metal form; sequentially separating the effluents from the column into the first fraction rich in the higher oligosaccharide, the second fraction rich in the higher oligosaccharide but highly contaiminated with the oligoglucosylfructoside, the first fraction rich in the oligoglucosylfructoside, the fourth fraction rich in the oligoglucosylfructoside but highly contaminated with the lower oligosaccharide, and the fifth fraction rich in the lower oligosaccharide; and recovering the third fraction. The second- and fourth fractions can be admitted to the column so as to decrease the amount of elution water and also to recover the high-oligoglucosylfructoside fraction in a much higher concentration and recovery yield.
摘要翻译：其中通过依次将预定体积的进料溶液和水顺序地加入到含有大量低聚糖的进料溶液的塔中，通过另外含有大量的高级和低级寡糖的进料溶液以高纯度从高纯度回收聚合度为2或3个葡萄糖单元的寡葡糖基果糖苷碱土金属形式的强酸性阳离子交换树脂; 将从柱中排出的污水依次分离成富含较高寡糖的第一级分，第二级分富含高寡聚物，但与寡葡糖基果糖苷高度接触，第一级富含寡聚葡糖基果糖苷，第四级富含低聚葡糖基果糖苷但高度污染低级寡糖，第五级富含低聚糖; 并回收第三部分。可以将第二和第四级分进入柱，以减少洗脱水的量，并且还可以以更高的浓度和回收率获得高寡葡糖基果糖苷级分。

82. 发明授权

US4824938A Water-soluble dry solid containing proteinaceous bioactive substance 失效
标题翻译：含有蛋白质生物活性物质的水溶性干固体
公开(公告)号：US4824938A
公开(公告)日：1989-04-25
申请号：US093089
申请日：1987-08-31
申请人： Shunsaku Koyama , Toshio Miyake
发明人： Shunsaku Koyama , Toshio Miyake
IPC分类号： A61K38/16 , A61K9/00 , A61K9/08 , A61K38/00 , A61K38/21 , A61K38/22 , A61K38/27 , A61K47/36 , C07K14/485 , C07K14/505 , C07K14/525 , C07K14/555 , C07K14/59 , C07K14/61 , C07K15/00 , A61K37/02 , A61K37/24 , A61K37/48
CPC分类号： A61K9/0019 , A61K47/36 , C07K14/485 , C07K14/505 , C07K14/525 , C07K14/555 , C07K14/59 , C07K14/61
摘要： Proteinaceous bioactive substances (including lymphokine and peptide hormone) in dry solid are extremely stabilized by the presence of the specific polysaccharide mainly composed of repeating maltotriose units. Pullulan, elsinan, and their partial hydrolysates are feasible as the polysaccharide. The weight ratio of the polysaccharide to the substance which effectively stabilizes the latter substance is at least 0.5 on the basis of dry solids. The dry solid is advantageously usable as a test reagent, injection, granule, tablet, suppository or ointment.
摘要翻译：通过主要由重复麦芽三糖单元组成的特定多糖的存在，干燥固体中的蛋白质生物活性物质（包括淋巴因子和肽激素）极度稳定。支链淀粉，elsinan及其部分水解产物作为多糖是可行的。基于干固体，多糖与有效稳定后者物质的物质的重量比至少为0.5。干固体有利地用作试剂，注射剂，颗粒剂，片剂，栓剂或软膏剂。

83. 发明授权

US4816272A Process for preparing noodles and alimentary pastes and premixed flour therefor 失效
标题翻译：制备面条和消化膏以及预混粉的方法
公开(公告)号：US4816272A
公开(公告)日：1989-03-28
申请号：US133813
申请日：1987-12-16
申请人： Masakazu Mitsuhashi , Shuzo Sakai , Toshio Miyake
发明人： Masakazu Mitsuhashi , Shuzo Sakai , Toshio Miyake
IPC分类号： A23L7/109 , A23L1/16 , A23L1/236
CPC分类号： A23L7/109
摘要： Crystalline .alpha.-maltose extremely improves the stability, taste quality and shelf life of noodles and alimentary pastes, as well as decreases the addition of water in their preparation. Since crystalline .alpha.-maltose exerts an activity of binding flour, a satisfiable dough can be obtained with a reduced addition of water. In corporation of crystalline .alpha.-maltose into flour yields a premixed flour for preparing noodles and alimentary pastes, and the addition of water thereto attains an excellent dough products.

84. 发明授权

US4777162A Inclusion compound of eicosapentaenoic acid and food product containing the same 失效
标题翻译：二十碳五烯酸的包合物和含有它们的食品
公开(公告)号：US4777162A
公开(公告)日：1988-10-11
申请号：US843645
申请日：1986-03-25
申请人： Hiromi Hijiya , Masakazu Mitsuhashi , Toshio Miyake
发明人： Hiromi Hijiya , Masakazu Mitsuhashi , Toshio Miyake
IPC分类号： A23L1/03 , A23G3/00 , A23G3/36 , A23L1/00 , A23L1/30 , A61K9/62 , A61K47/48 , C08B37/00 , C08B37/16 , A61K31/19 , A61K31/715
CPC分类号： A23G3/368 , A23L33/12 , A23P10/30 , A61K47/48969 , B82Y5/00 , C08B37/0015
摘要： A novel EPA/CD inclusion compound and a food product containing the same are disclosed. The undesirable odor of EPA is masked by including it into such EPA/CD inclusion compound. Gamma-CD is most favorable because it includes much more EPA, and highly stabilizes it. The EPA/CD inclusion compound is advantageously usable in perorally- or parenterally-usable products directed to the promotion or maintenance of health.
摘要翻译：公开了一种新型EPA / CD包合物和含有该化合物的食品。通过将EPA包含在这种EPA / CD包合物中来掩盖EPA的不良气味。 Gamma-CD是最有利的，因为它包含更多的EPA，并且高度稳定。 EPA / CD包合物有利地用于旨在促进或维持健康的经口或肠胃外可用的产品。

85. 发明授权

US4623394A Gradually disintegrable molded article 失效
标题翻译：逐渐崩解成型品
公开(公告)号：US4623394A
公开(公告)日：1986-11-18
申请号：US719434
申请日：1985-04-03
申请人： Satoshi Nakamura , Hiromi Hijiya , Toshio Miyake
发明人： Satoshi Nakamura , Hiromi Hijiya , Toshio Miyake
IPC分类号： A61K9/20 , A61K9/22 , A61K47/36 , B29D7/01 , B29K96/00 , C08L1/00 , C08L5/00 , C08L27/00
CPC分类号： A61K9/205 , C08L5/00
摘要： A novel molded article exhibiting a gradual disintegration effect is prepared with pullulan. The effect is imparted by incorporating heteromannan into a pullulan molded article in an amount not exceeding the weight of the pullulan used. Galactomannans (e.g. guar gum, tara gum, and locust bean gum) and glucomannans (e.g. konjak mannan) are feasible as the heteromannan. The molded article is advantageously usable for industrial materials, pharmaceuticals, consumers' products, etc.
摘要翻译：用支链淀粉制备展现出逐渐崩解效果的新型成型品。通过将异甘露聚糖以不超过所使用的支链淀粉的重量的量引入支链淀粉模制品中来赋予该效果。半乳甘露聚糖（例如瓜尔胶，塔拉胶和刺槐豆胶）和葡甘聚糖（例如魔芋甘露聚糖）作为异甘露聚糖是可行的。成型品有利地用于工业材料，药品，消费者的产品等。

86. 发明授权

US4557927A Food products and process for producing same 失效
标题翻译：食品及其制作方法
公开(公告)号：US4557927A
公开(公告)日：1985-12-10
申请号：US582475
申请日：1984-02-22
申请人： Toshio Miyake , Hiromi Hijiya , Shinji Suzuki , Teruo Matsumoto
发明人： Toshio Miyake , Hiromi Hijiya , Shinji Suzuki , Teruo Matsumoto
IPC分类号： A23C9/13 , A23C11/10 , A23G1/00 , A23G1/40 , A23G1/42 , A23G3/00 , A23G3/42 , A23G3/48 , A23G4/00 , A23G4/06 , A23G4/10 , A23L17/60 , A23L21/15 , A61K8/60 , A61Q11/00 , C07H15/256 , C07H17/07 , C12G3/06 , C12P19/44 , C08B37/00 , A23L1/236 , A61K7/16
CPC分类号： A23G1/423 , A23C11/103 , A23C9/13 , A23G1/40 , A23G3/42 , A23G3/48 , A23G4/068 , A23G4/10 , A23L17/60 , A23L21/15 , A61K8/602 , A61Q11/00 , C07H15/256 , C07H17/07 , C12G3/06 , C12P19/44
摘要： Novel alpha-glycosylated soybean glycosides wherein one or more glucosyl residues are bound to the soybean glycoside moiety are prepared. Alpha-glycosylation can be enzymatically achieved by subjecting an aqueous solution containing a soybean glycoside, e.g. soyasaponin or isoflavonoid, and an alpha-glucosyl saccharide to an alpha-glucosyl transferase. Suitable alpha-glucosyl saccharides are liquefied starch, partially hydrolyzed starch and sucrose. Alpha-glucosidase, alpha-amylase, cyclodextrin glucanotransferase, dextransucrase, dextran dextrinase and amylosucrase are usable as the alpha-glucosyl transferase. Since in the alpha-glycosylated soybean glycosides the undesirable bitter, astringent, harsh and lingering choky tastes which are common in intact soybean glycosides are reduced or even eliminated by the alpha-glycosylation, they are suitable for use in food products or orally-usable products wherein taste is an important factor.
摘要翻译：制备其中一个或多个葡糖基残基与大豆糖苷部分结合的新型α-糖基化大豆糖苷。 α-糖基化可以通过使含有大豆糖苷的水溶液，例如，大豆皂角苷或异黄酮，和α-葡糖基糖对α-葡糖基转移酶。合适的α-葡糖基糖是液化淀粉，部分水解淀粉和蔗糖。 α-葡糖苷酶，α-淀粉酶，环糊精葡聚糖转移酶，葡聚糖糊精酶，葡聚糖糊精酶和淀粉蔗糖酶可用作α-葡糖基转移酶。由于在α-糖基化的大豆糖苷中，完整大豆糖苷中常见的不希望的苦味，收敛性，苛刻和挥之不去的口味通过α-糖基化降低甚至消除，它们适用于食品或口服制品其中味道是重要的因素。

87. 发明授权

US4486417A Flurocarbon-water emulsion for hyperalimentation containing maltose 失效
标题翻译：用于含麦芽糖的过度活化的氟碳水乳液
公开(公告)号：US4486417A
公开(公告)日：1984-12-04
申请号：US320745
申请日：1981-11-12
申请人： Kaname Sugimoto , Toshio Miyake
发明人： Kaname Sugimoto , Toshio Miyake
IPC分类号： A61K9/10 , A61K9/00 , A61K9/107 , A61P3/00 , A61P3/06 , A61K31/70 , A01N57/26
CPC分类号： A61K9/0029
摘要： A process for the production of an O/W emulsion for hyperalimentation comprising homogenization of a composition comprising hydrophobic substance, emulsifier, water and maltose into minute droplets of O/W emulsion. The emulsion can provide a higher caloric nutritive supplement to patients than conventional emulsions using glycerin. It is stable over a wide temperature range and it can be stored for long periods of time. The emulsion is particularly useful in emergency medical situations where enteral or parenteral hyperalimentation is required for the patient.
摘要翻译：一种用于生产用于过度补液的O / W乳液的方法，包括将包含疏水物质，乳化剂，水和麦芽糖的组合物均匀化成微小的O / W乳液液滴。使用甘油的乳液可以提供比常规乳液更高的热量营养补充剂。它在很宽的温度范围内是稳定的，可以长时间储存。该乳剂在患者需要肠内或肠胃外过度增生的紧急医疗情况下特别有用。

88. 发明授权

US4219571A Process for producing a sweetener 失效
标题翻译：生产甜味剂的方法
公开(公告)号：US4219571A
公开(公告)日：1980-08-26
申请号：US915876
申请日：1978-06-15
申请人： Toshio Miyake
发明人： Toshio Miyake
IPC分类号： A23L27/30 , C12P19/18 , C12P19/56 , A23L1/236
CPC分类号： C12P19/56 , A23L27/36 , C12P19/18 , Y10S426/804
摘要： A sweetener containing alpha-glycosyl stevioside which is obtained by allowing alpha-glucosyltransferase to react on an aqueous solution containing stevioside and alpha-glucosyl sugar compound.
摘要翻译：含有α-糖基甜菊苷的甜味剂，其通过使α-葡糖基转移酶在含有甜菊苷和α-葡糖基糖化合物的水溶液中反应而获得。

89. 发明授权

US08765416B2 Particulate composition containing anhydrous crystalline 2-O-alpha-D-glucosyl-L-ascorbic acid, process for producing the same, and uses thereof 有权
标题翻译：含有无水结晶2-O-α-D-葡糖基-L-抗坏血酸的颗粒组合物，其制备方法及其用途
公开(公告)号：US08765416B2
公开(公告)日：2014-07-01
申请号：US12875786
申请日：2010-09-03
申请人： Takashi Shibuya , Seisuke Izawa , Tomoyuki Nishimoto , Shigeharu Fukuda , Toshio Miyake
发明人： Takashi Shibuya , Seisuke Izawa , Tomoyuki Nishimoto , Shigeharu Fukuda , Toshio Miyake
IPC分类号： C12P19/44
CPC分类号： C12P19/60 , A23L33/10 , A23L33/15 , A61K8/0241 , A61K8/676 , A61K8/732 , A61K31/7048 , A61K2800/57 , A61K2800/654 , A61Q19/02 , C07H17/04 , Y10T428/2982
摘要： The present invention aims to provide a particulate composition containing anhydrous crystalline 2-O-α-D-glucosyl-L-ascorbic acid having a significantly, hardly solidifiable property compared to conventional ones in a grade for use in quasi-drugs; a process for producing the same; and uses thereof. The present invention solves the above object by providing a particulate composition containing anhydrous crystalline 2-O-α-D-glucosyl-L-ascorbic in an amount of over 98.0% by weight but less than 99.9% by weight, on a dry solid basis; or a degree of crystallinity of 90% or higher for anhydrous crystalline 2-O-α-D-glucosyl-L-ascorbic acid; and by providing a process for producing the same and uses thereof.
摘要翻译：本发明的目的在于提供一种含有无水结晶2-O-α-D-葡糖基-L-抗坏血酸的颗粒组合物，其与用于准药物的级别相比，具有显着难以固化的性能; 其制造方法; 及其用途。本发明通过提供含有无水结晶2-O-α-D-葡糖基-L-抗坏血酸的颗粒组合物来解决上述目的，其含量超过98.0重量％但小于99.9重量％，基于干固体 ; 或无水结晶的2-O-α-D-葡糖基-L-抗坏血酸的结晶度为90％以上; 并提供其制造方法及其用途。

90. 发明申请

US20140178943A9 PROCESS FOR PRODUCING A PARTICULATE COMPOSITION COMPRISING ANHYDROUS CRYSTALLINE 2-O-ALPHA-D-GLUCOSYL-L-ASCORBIC ACID 有权
标题翻译：生产包含无水晶体2-O-ALPHA-D-葡萄糖-L-抗坏血酸的颗粒组合物的方法
公开(公告)号：US20140178943A9
公开(公告)日：2014-06-26
申请号：US13980223
申请日：2012-03-07
申请人： Takashi Shibuya , Seisuke Izawa , Tomoyuki Nishimoto , Shigeharu Fukuda , Toshio Miyake
发明人： Takashi Shibuya , Seisuke Izawa , Tomoyuki Nishimoto , Shigeharu Fukuda , Toshio Miyake
IPC分类号： C12P19/18
CPC分类号： A61K31/7048 , A61K9/16 , C07H17/04 , C12P19/18 , C12P19/60 , C12Y204/01019
摘要： The invention provides a process for enabling the production of a particulate composition containing anhydrous crystalline ascorbic acid 2-glucoside that does not significantly cake even when the production yield of ascorbic acid 2-glucoside does not reach 35% by weight. The process for producing a particulate composition containing anhydrous crystalline ascorbic acid 2-glucoside, which comprises allowing a CGTase to act on a solution containing either liquefied starch or dextrin and L-ascorbic acid and then allowing a glucoamylase to act on the resulting solution to obtain a solution with an ascorbic acid 2-glucoside production yield of at least 27%, purifying the obtained solution to increase the ascorbic acid 2-glucoside content to a level of over 86% by weight, precipitating anhydrous crystalline ascorbic acid 2-glucoside by a controlled cooling method or pseudo-controlled cooling method, collecting the precipitated anhydrous crystalline ascorbic acid 2-glucoside, and ageing and drying the collected anhydrous crystalline ascorbic acid 2-glucoside.
摘要翻译：本发明提供了一种能够生产含有抗坏血酸2-葡萄糖苷的无水结晶抗坏血酸2-葡萄糖苷的颗粒组合物的方法，即使当抗坏血酸2-葡萄糖苷的产率不达到35重量％时也不显着。制备含有无水结晶抗坏血酸2-葡萄糖苷的颗粒组合物的方法，其包括使CGT酶作用于含有液化淀粉或糊精和L-抗坏血酸的溶液，然后使葡糖淀粉酶作用于所得溶液以获得将抗坏血酸2-葡萄糖苷产率至少为27％的溶液，纯化得到的溶液，将抗坏血酸2-葡萄糖苷含量提高至86重量％以上，将无水结晶性抗坏血酸2-葡萄糖苷通过控制冷却方式或假控制冷却方法，收集沉淀的无水结晶抗坏血酸2-葡萄糖苷，并对收集的无水结晶抗坏血酸2-葡萄糖苷进行老化和干燥。

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