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81. 发明授权

US07557254B2 Method for producing fluorinated organic compounds 有权
标题翻译：氟化有机化合物的制备方法
公开(公告)号：US07557254B2
公开(公告)日：2009-07-07
申请号：US12134629
申请日：2008-06-06
申请人： Sudip Mukhopadhyay , Hsueh Sung Tung , Haridasan Nair , Jingji Ma
发明人： Sudip Mukhopadhyay , Hsueh Sung Tung , Haridasan Nair , Jingji Ma
IPC分类号： C07C17/04 , C07C17/278 , C07C17/281
CPC分类号： B01J27/125 , B01J27/10 , B01J27/12 , C07C17/00 , C07C17/278 , C07C21/18 , C07C19/08
摘要： A method for preparing fluorinated organic compounds wherein at least one fluorinated olefin is reacted with methyl fluoride in the gas-phase and in the presence of a Lewis Acid catalyst to form at least one product having at least 3 carbon atoms.
摘要翻译：一种制备氟化有机化合物的方法，其中至少一种氟化烯烃在气相和路易斯酸催化剂存在下与甲基氟反应形成至少一种具有至少3个碳原子的产物。

82. 发明申请

US20080108854A1 Catalyst promoters for producing trifluoroiodomethane and pentafluoroiodoethane 有权
标题翻译：用于生产三氟碘甲烷和五氟碘乙烷的催化剂促进剂
公开(公告)号：US20080108854A1
公开(公告)日：2008-05-08
申请号：US11901672
申请日：2007-09-18
申请人： Shuwu Yang , Hsueh Sung Tung
发明人： Shuwu Yang , Hsueh Sung Tung
IPC分类号： C07C17/00 , C07C19/08
CPC分类号： C07C19/16 , B01J23/04 , B01J23/06 , B01J23/10 , B01J23/22 , B01J23/24 , B01J23/78 , C07C17/093 , C07C17/10 , C07C17/158 , C07C17/204 , C09K5/044
摘要： The present invention provides a process for the preparation of a fluoroiodoalkane compound represented by the formula CF3(CF2)n—I, wherein n is 0 or 1. The process includes the step of contacting: (i) a compound represented by the formula CF3(CF2)n—Y, wherein Y is selected from H, Cl, Br, and COOH and n is 0 or 1; (ii) a source of iodine; (iii) an alkali or alkaline earth metal salt catalyst supported on a carrier; and (iv) a catalyst promoter for the alkali or alkaline earth metal salt catalyst. The catalyst promoter includes at least one element selected from a transition metal element, a rare earth metal element, a main group element other than the alkali or alkaline earth metal element, any salts thereof, and any combinations thereof. The contacting is carried out at a temperature and pressure and for a length of time sufficient to produce the fluoroiodoalkane compound. The contacting may be carried out in the presence or absence of a solvent and in the presence or absence of oxygen.
摘要翻译：本发明提供一种制备由式CF 3（CF 2）n I-I表示的氟代碘代烷烃化合物的方法，其中n 该方法包括使以下步骤：（i）由式CF 3（CF 2）n表示的化合物 -Y，其中Y选自H，Cl，Br和COOH，n为0或1; （ii）碘源; （iii）负载在载体上的碱金属或碱土金属盐催化剂; 和（iv）碱金属或碱土金属盐催化剂的催化剂促进剂。催化剂促进剂包括选自过渡金属元素，稀土金属元素，除碱金属或碱土金属元素以外的主要基团的元素中的至少一种元素，它们的任何盐及其任何组合。接触在温度和压力下进行足够长的时间以产生氟代碘代烷烃化合物。接触可以在存在或不存在溶剂的情况下以及在存在或不存在氧的情况下进行。

83. 发明授权

US07071367B1 Direct one-step synthesis of CF3-I 失效
标题翻译：直接一步合成CF3-I
公开(公告)号：US07071367B1
公开(公告)日：2006-07-04
申请号：US11007919
申请日：2004-12-09
申请人： Sudip Mukhopadhyay , Hsueh Sung Tung
发明人： Sudip Mukhopadhyay , Hsueh Sung Tung
IPC分类号： C07C17/00
CPC分类号： C07C17/093 , C07C17/158 , C07C17/204 , C07C19/16
摘要： The present invention provides a process for the preparation of trifluoromethyl iodide. The process includes the step of: contacting in a reactor a compound represented by the formula: CF3—W and a compound represented by the formula: Z-I wherein W is selected from CF3, hydrogen and bromine; Z is selected from hydrogen, iodine and chlorine. The step of contacting is carried out, optionally in the presence of a catalyst and further optionally in the presence of air, at a temperature, pressure and for a length of time sufficient to produce the trifluoromethyl iodide.
摘要翻译：本发明提供了制备三氟甲基碘的方法。该方法包括以下步骤：在反应器中接触由下式表示的化合物：<？in-line-formula description =“In-line Formulas”end =“lead”？> CF 3 - W <？in-line-formula description =“In-line Formulas”end =“tail”？>和由以下公式表示的化合物：<？in-line-formula description =“In-line Formulas”end =“lead “？”ZI <？in-line-formula description =“In-line Formulas”end =“tail”？>其中W选自CF 3，氢和溴; Z选自氢，碘和氯。任选地在催化剂存在下进一步任选地在空气存在下，在足以产生三氟甲基碘的温度，压力和一段时间内进行接触步骤。

84. 发明授权

US06787678B1 Method of removing water from hydrofluorocarbon manufacturing processes 失效
标题翻译：从氢氟碳化物制造工艺中去除水的方法
公开(公告)号：US06787678B1
公开(公告)日：2004-09-07
申请号：US10733036
申请日：2003-12-11
申请人： Hsueh Sung Tung , Jason T. Stuck
发明人： Hsueh Sung Tung , Jason T. Stuck
IPC分类号： C07C1738
CPC分类号： C07B39/00 , C07C17/38 , Y02P20/582
摘要： Disclosed are improved fluorination processes and fluorine-containing compositions which involve introducing to one or more fluorination process compositions a water reactive agent in an amount and under conditions effective to decrease the amount of water in that composition. The water reactive agent is preferably introduced to the fluorination process at a location downstream of the fluorination reaction, in amounts and under conditions effective to produce a relatively lower concentration of water in the composition, and preferably throughout the fluorination process.
摘要翻译：公开了改进的氟化方法和含氟组合物，其涉及在有效降低该组合物中的水量的量和条件下向一种或多种氟化方法组合物引入水反应剂。水反应剂优选在氟化反应的下游位置以有效地在组合物中产生相对较低浓度的水，并且优选在整个氟化过程中的量和条件下引入氟化过程。

85. 发明授权

US06702929B2 Purification of 1,1,1,3,3-pentafluorobutane 有权
标题翻译： 1,1,1,3,3-五氟丁烷的纯化
公开(公告)号：US06702929B2
公开(公告)日：2004-03-09
申请号：US10337836
申请日：2003-01-07
申请人： Stephen Frederic Yates , Hsueh Sung Tung
发明人： Stephen Frederic Yates , Hsueh Sung Tung
IPC分类号： C07C1700
CPC分类号： C07C17/395 , C07C19/08
摘要： In the synthesis of 1,1,1,3,3-pentafluorobutane (R-365mfc), a mixture of R-365mfc and the impurity 1,1,1,3-tetrafluoro-2-butene (R-1354mzy) is purified and R-1354mzy is removed from the mixture by contacting the mixture with 1-5 mols of chlorine for each mol of R-1354mzy in the presence of ultraviolet light having a wavelength between about 300 to 400 nm which provides at least 0.02 watts-hour/kg of the mixture. The R-1354mzy is reduced to below 10 wt. ppm as it is converted to 2,3-dichloro-1,1,1,3-tetrafluorobutane (R-354) or other butane containing more chlorine and having a higher boiling point than R-365mfc. The butane(s) may be separated more easily from R-365mfc. The photochlorination is effected in a manner such that at least about 96 weight percent of the starting amount of R-365mfc is maintained in the mixture.
摘要翻译：在1,1,1,3,3-五氟丁烷（R-365mfc）的合成中，纯化R-365mfc和杂质1,1,1,3-四氟-2-丁烯（R-1354mzy）的混合物并且在波长在约300至400nm之间的紫外光存在下，将混合物与1-5摩尔氯接触，每摩尔R-1354毫摩尔，从混合物中除去R-1354mzy，该紫外线提供至少0.02瓦时 / kg混合物。将R-1354mzy还原成低于10wt。 ppm，因为它被转化为2,3-二氯-1,1,1,3-四氟丁烷（R-354）或其它含有更多氯且沸点高于R-365mfc的丁烷。丁烷可能更容易从R-365mfc分离出来。光氯化以这样的方式进行，使得至少约96重量％的起始量的R-365mfc保持在混合物中。

86. 发明授权

US06596910B2 Process for the manufacture of fluorocarbons 有权
公开(公告)号：US06596910B2
公开(公告)日：2003-07-22
申请号：US10057570
申请日：2002-01-25
申请人： Hsueh Sung Tung , Clayton Herbert Carson , Hang Thanh Pham
发明人： Hsueh Sung Tung , Clayton Herbert Carson , Hang Thanh Pham
IPC分类号： C07C1700
CPC分类号： C07C19/08 , C07C17/087 , C07C17/206 , C07C17/21 , C07C17/38 , Y02P20/582
摘要： Disclosed is an improved HFC manufacturing processes of the type which produces an intermediate product stream that includes a mixture of HF and at least one compound, usually an HCFC, which is relatively resistant to further fluorination. The improvement involves separating the unreactive compound(s) from the product stream, preferably using liquid:liquid phase separation, and substantially avoiding recycle of the unreactive compound to the fluorination reaction. The separated unreactive compound(s) are substantially free of HF.

87. 发明授权

US06534467B2 Azeotrope-like composition of 1,2,2-trichloro-1,3,3,3-tetrafluoropropane and hydrogen fluoride 有权
标题翻译： 1,2,2-三氯-1,3,3,3-四氟丙烷和氟化氢的类共沸组合物
公开(公告)号：US06534467B2
公开(公告)日：2003-03-18
申请号：US09768638
申请日：2001-01-24
申请人： Hang Thanh Pham , Rajiv Ratna Singh , Hsueh Sung Tung
发明人： Hang Thanh Pham , Rajiv Ratna Singh , Hsueh Sung Tung
IPC分类号： C11D750
CPC分类号： C09K5/00 , C07C17/386 , C07C19/10
摘要： The invention relates to azeotropic and azeotrope-like mixtures of 1,2,2-trichloro-1,3,3,3-tetrafluoropropane (commonly known as HCFC-224aa, and with the IUPAC name of 2,2,3-trichloro-1,1,1,3-tetrafluoropropane;registry number 139754-75-9) and hydrogen fluoride (hydrofluoric acid), which are useful as intermediates in the production of 1,1,3,3,3-pentafluoropropane (HFC-245-fa) and 1,1,1,2,2,3,3-heptafluoropropane (HFC-227ca).
摘要翻译：本发明涉及1,2,2-三氯-1,3,3,3-四氟丙烷（通常称为HCFC-224aa）和IUPAC名称为2,2,3-三氯-1,3,3,3-四氟丙烷的共沸和类共沸混合物， 1,1,1,3-四氟丙烷，注册号139754-75-9）和氟化氢（氢氟酸），它们可用作生产1,1,3,3,3-五氟丙烷（HFC-245 -fa）和1,1,1,2,2,3,3-七氟丙烷（HFC-227ca）。

88. 发明授权

US06524496B2 Azeotrope-like composition of 1,1,1,3,3-pentafluoropropane and 1-chloro-1,1,3,3,3-pentafluoropropane 有权
公开(公告)号：US06524496B2
公开(公告)日：2003-02-25
申请号：US09813501
申请日：2001-03-21
申请人： Kane David Cook , Rajiv Ratna Singh , Hsueh Sung Tung
发明人： Kane David Cook , Rajiv Ratna Singh , Hsueh Sung Tung
IPC分类号： C09K504
CPC分类号： C10M131/04 , C09K5/045 , C09K2205/122 , C09K2205/32 , C10N2220/30 , C10N2240/30
摘要： Provided are azeotropic and azeotrope-like mixtures of 1,1,1,3,3-pentafluoropropane (HFC-245fa) and 1-chloro-1,1,3,3,3-pentafluoropropane (HCFC-235fa) that are useful as intermediates in the production of HFC-245fa. A process for separating HFC-245fa and HCFC-235fa is also provided. HFC-245fa is useful as a nontoxic, zero ozone depleting fluorocarbon useful as solvents, blowing agents, refrigerants, cleaning agents, aerosol propellants, heat transfer media, gaseous dielectrics, fire extinguishing compositions and power cycle working fluids.

89. 发明授权

US06514928B1 Azeotrope-like compositions of pentafluoropropane and water 有权
标题翻译：五氟丙烷和水的类共沸组合物
公开(公告)号：US06514928B1
公开(公告)日：2003-02-04
申请号：US09268000
申请日：1999-03-15
申请人： Leslie Bruce Bement , Mary Charlotte Bogdan , Clayton Herbert Carson , Peter Brian Logsdon , Hang Thanh Pham , Rajiv Ratna Singh , Hsueh Sung Tung , Ronald Riegal , David John Williams , Kevin Donald Uhrich
发明人： Leslie Bruce Bement , Mary Charlotte Bogdan , Clayton Herbert Carson , Peter Brian Logsdon , Hang Thanh Pham , Rajiv Ratna Singh , Hsueh Sung Tung , Ronald Riegal , David John Williams , Kevin Donald Uhrich
IPC分类号： C11D1708
CPC分类号： C11D7/5036 , C11D7/505
摘要： This invention provides azeotrope-like compositions of 1,1,1,3,3-pentafluoropropane and water that are environmentally desirable for use as refrigerants, aerosol propellants, metered dose inhalers, blowing agents for polymer foam, heat transfer media, and gaseous dielectrics.
摘要翻译：本发明提供1,1,1,3,3-五氟丙烷和水的类共沸组合物，其作为制冷剂，气溶胶推进剂，计量吸入器，用于聚合物泡沫的发泡剂，传热介质和气体电介质是环境需要的。

90. 发明授权

US06365566B1 Azeotrope-like compositions of pentafluorobutane and water 有权
标题翻译：五氟丁烷和水的类共沸组合物
公开(公告)号：US06365566B1
公开(公告)日：2002-04-02
申请号：US09813495
申请日：2001-03-21
申请人： Mary C. Bogdan , Hang T. Pham , Hsueh Sung Tung , David J. Williams , Leslie Bement
发明人： Mary C. Bogdan , Hang T. Pham , Hsueh Sung Tung , David J. Williams , Leslie Bement
IPC分类号： C08J914
CPC分类号： C08J9/146 , C08J2375/04 , C09K3/30
摘要： This invention provides azeotropic and azeotrope-like compositions of 1,1,1,3,3-pentafluorobutane and water that are environmentally desirable for use as blowing agents and solvents.
摘要翻译：本发明提供1,1,1,3,3-五氟丁烷和水的共沸和类共沸组合物，其作为发泡剂和溶剂是环境需要的。

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