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81. 发明授权

US5703260A Process for the preparation of alkoxytriazolinones 失效
标题翻译：制备烷氧基三唑啉酮的方法
公开(公告)号：US5703260A
公开(公告)日：1997-12-30
申请号：US714668
申请日：1996-09-16
申请人： Heinz-Jurgen Wroblowsky , Klaus Konig
发明人： Heinz-Jurgen Wroblowsky , Klaus Konig
IPC分类号： C07C281/06 , C07D249/12
CPC分类号： C07D249/12 , C07C281/06
摘要： Alkoxytriazolinones of the general formula (I), ##STR1## in which R.sup.1 represents hydrogen, or represents in each case optionally substituted alkyl, alkenyl, alkinyl, cycloalkyl, cycloalkylalkyl, aryl or arylalkyl, and R.sup.2 represents in each case optionally substituted alkyl, alkenyl, alkinyl, cycloalkyl, cycloalkylalkyl, ary or arylalkyl, (which can be used as intermediates for the preparation of herbicidal active compounds) are obtained in very good yields and in high purity by reacting imino(thio)carbonic esters (II) with alkoxyethyl carbazinates (III) ##STR2## in which Q represents O or S, R.sup.3 represents (for example) alkyl, aryl or aralkyl and R.sup.4 represents (for example) alkyl, at -20.degree. C. to +150.degree. C. (1st step) and subjecting the new semicarbazide derivatives (IV) ##STR3## which are formed with elimination of R.sup.3 --QH, if appropriate after intermediate isolation, to a cyclizing condensation reaction at 0.degree. C. to 200.degree. C., without the addition of a base, advantageously under reduced pressure, with the elimination of alkoxyethanols (2nd step).
摘要翻译：通式（I）的烷氧基三唑啉酮，其中R 1表示氢，或在每种情况下表示任选取代的烷基，烯基，炔基，环烷基，环烷基烷基，芳基或芳基烷基，和R 2表示在各种情况下任选取代的通过使亚氨基（硫代）碳酸酯（II）反应，以非常好的产率和高纯度获得烷基，链烯基，炔基，环烷基，环烷基烷基，芳基或芳烷基（可用作制备除草活性化合物的中间体）其中Q代表O或S，R3代表（例如）烷基，芳基或芳烷基，R4代表（例如）烷基，在-20℃至+ 150℃（第1步），在0℃〜200℃进行环化缩合反应，在中间分离后，如果合适，将R3-QH所形成的新的氨基脲衍生物（IV）没有添加基地，优势在减压下，剔除烷氧基乙醇（第二步）。

82. 发明授权

US5654438A Sulphonylaminocarbonyltriazolinones 失效
标题翻译：磺酰氨基羰基三唑啉酮
公开(公告)号：US5654438A
公开(公告)日：1997-08-05
申请号：US656819
申请日：1996-06-03
申请人： Kurt Findeisen , Karl-Heinz Linker , Joachim Kluth , Klaus-Helmut Muller , Hans-Jochem Riebel , Klaus Konig , Hans-Joachim Santel , Robert R. Schmidt
发明人： Kurt Findeisen , Karl-Heinz Linker , Joachim Kluth , Klaus-Helmut Muller , Hans-Jochem Riebel , Klaus Konig , Hans-Joachim Santel , Robert R. Schmidt
IPC分类号： A01N47/38 , A01N57/32 , A01P13/00 , C07D249/12 , C07D249/14 , C07F9/6518 , C07D413/04 , C07D401/04 , C07D403/04
CPC分类号： A01N47/38 , C07D249/12 , C07D249/14
摘要： The invention relates to new sulphonylaminocarbonyltriazolinones of the formula (I) ##STR1## in which Q represents oxygen, sulphur or one of the following groups ##STR2## (in which the radicals R.sup.1, R.sup.2, R.sup.3 and R.sup.4 have the meanings given in the description), as well as to salts of compounds of the formula (I), to processes and novel intermediates for the preparation of the novel compounds, and to their use as herbicides.
摘要翻译：本发明涉及式（I）的新的磺酰基氨基羰基三唑啉酮，其中Q表示氧，硫或以下基团之一：其中基团R 1，R 2，R 3和R 4具有给定的含义在描述中）以及式（I）化合物的盐用于制备新化合物的方法和新中间体，以及它们作为除草剂的用途。

83. 发明授权

US5554761A Herbicidal sulphonylaminocarbonyltriazolinones having two substituents bonded via oxygen 失效
标题翻译：具有通过氧键连接的两个取代基的除草磺酰基氨基羰基三唑啉酮
公开(公告)号：US5554761A
公开(公告)日：1996-09-10
申请号：US547698
申请日：1995-10-19
申请人： Wilhelm Haas , Klaus-Helmut Muller , Klaus Konig , Hans-Joachim Santel , Klaus Lurssen , Robert R. Schmidt
发明人： Wilhelm Haas , Klaus-Helmut Muller , Klaus Konig , Hans-Joachim Santel , Klaus Lurssen , Robert R. Schmidt
IPC分类号： A01N47/38 , A01N51/00 , C07D249/12 , C07D249/14 , C07D401/12 , C07D403/12 , C07D405/12 , C07D409/12 , C07D471/04 , C07D487/04
CPC分类号： C07D401/12 , A01N47/38 , A01N51/00 , C07D249/12 , C07D249/14 , C07D403/12 , C07D405/12 , C07D409/12 , C07D471/04 , C07D487/04
摘要： Herbicidal sulphonylaminocarbonyltriazolinones having two substituents bonded via oxygen, of the formula ##STR1## in which R.sup.1 represents hydrogen or an optionally substituted radical from the series comprising alkyl, alkenyl, alkinyl, cycloalkyl, cycloalkenyl and aralkyl,R.sup.2 represents an optionally substituted radical from the series comprising alkyl, alkenyl, alkinyl, cycloalkyl, cycloalkenyl and aralkyl, andR.sup.3 represents an optionally substituted radical from the series comprising alkyl, aralkyl, aryl and heteroaryl,and their salts.
摘要翻译：具有下式的其中R1表示氢的烷基，烯基，炔基，环烷基，环烯基和芳烷基的任意取代的基团通过氧连接的具有两个取代基的除草性磺酰基氨基羰基三唑啉酮，R2表示任选取代的基团由烷基，烯基，炔基，环烷基，环烯基和芳烷基组成的系列，R 3代表包含烷基，芳烷基，芳基和杂芳基的其中任意取代的基团及其盐。

84. 发明授权

US5523479A Process for the preparation of ethercarboxylic acids 失效
标题翻译：制备醚羧酸的方法
公开(公告)号：US5523479A
公开(公告)日：1996-06-04
申请号：US230282
申请日：1994-04-20
申请人： Josef Sanders , Klaus Konig
发明人： Josef Sanders , Klaus Konig
IPC分类号： C07C51/367 , C07C67/31 , C07C59/10 , C07C59/125 , C07C59/245
CPC分类号： C07C67/31 , C07C51/367
摘要： A process for the preparation of carboxylic acids which contain ether groups by the catalytically accelerated addition of alcoholic hydroxyl groups from mono- or polyhydric alcohols to tertiary-alkyl esters of .alpha.,.beta.-unsaturated carboxylic acids, and followed with acid hydrolysis of the tertiary-alkyl .beta.-ethercarboxylate obtained as intermediates in this way.
摘要翻译：通过催化加速将醇羟基从一元醇或多元醇加成加成α，β-不饱和羧酸的叔烷基酯，然后酸性水解叔丁醇，制备含有醚基团的羧酸的方法，以此方式获得的作为中间体的β-羧酸叔丁酯。

85. 发明授权

US5461149A Herbicidal substituted triazolinones 失效
标题翻译：除草取代的三唑啉酮
公开(公告)号：US5461149A
公开(公告)日：1995-10-24
申请号：US210223
申请日：1994-03-18
申请人： Markus Lindig , Kurt Findeisen , Klaus-Helmut Muller , Hans-Joachim Santel , Robert R. Schmidt , Harry Strang , Dieter Feucht , Klaus Konig , Klaus Lurssen
发明人： Markus Lindig , Kurt Findeisen , Klaus-Helmut Muller , Hans-Joachim Santel , Robert R. Schmidt , Harry Strang , Dieter Feucht , Klaus Konig , Klaus Lurssen
IPC分类号： A01N47/38 , C07D249/12 , C07D249/14 , C07D405/12
CPC分类号： C07D405/12 , A01N47/38 , C07D249/12
摘要： Intermediates for herbicides, the intermediates having the formulas ##STR1## in which R.sup.1 represents alkyl having 3 to 4 carbon atoms or represents cyclopropyl,R.sup.3 and R.sup.4 independently of one another represent hydrogen, alkyl, aralkyl or arylQ represents NH.sub.z or ##STR2## and R.sup.1-1 represents alkyl.
摘要翻译：除草剂的中间体，其中R 1表示具有3至4个碳原子的烷基或者表示环丙基，R 3和R 4彼此独立地具有式（IV）和（VI）的化合物的中间体代表氢，烷基，芳烷基或芳基Q代表NHz或R1和R1-1代表烷基。

86. 发明授权

US5356865A Substituted 5-alkoxy-1,2,4-triazol-3-(thi)ones 失效
标题翻译：取代的5-烷氧基-1,2,4-三唑-3-（硫）
公开(公告)号：US5356865A
公开(公告)日：1994-10-18
申请号：US976185
申请日：1992-11-06
申请人： Klaus-Helmut Muller , Klaus Konig , Joachim Kluth , Klaus Lurssen , Hans-Joachim Santel , Robert R. Schmidt
发明人： Klaus-Helmut Muller , Klaus Konig , Joachim Kluth , Klaus Lurssen , Hans-Joachim Santel , Robert R. Schmidt
IPC分类号： C07D249/12 , C07D403/12 , C07D405/12 , C07D409/12 , A01N43/653
CPC分类号： C07D403/12 , C07D249/12 , C07D405/12 , C07D409/12
摘要： Herbicidal 5-alkoxy-1,2,4-triazol-3-(thi)ones of the gerneral formula ##STR1## (in which the radicals R.sup.1, R.sup.2, R.sup.3, X and Y have the meanings given in the description), processes for their preparation, and their use as herbicides, and also new intermediates of the formula (II) ##STR2##
摘要翻译：除草剂5-烷氧基-1,2,4-三唑-3-（thi）取代的式（I）（其中基团R 1，R 2，R 3，X和Y具有在说明书中给出的含义）），它们的制备方法和它们作为除草剂的用途，以及式（II）的新的中间体<图像（II）

87. 发明授权

US5273958A Substituted triazolinones 失效
标题翻译：取代的三唑啉酮
公开(公告)号：US5273958A
公开(公告)日：1993-12-28
申请号：US871788
申请日：1992-04-20
申请人： Dietmar Kuhnt , Klaus-Helmut Muller , Kurt Findeisen , Klaus Konig , Klaus Lurssen , Hans-Joachim Santel , Robert R. Schmidt
发明人： Dietmar Kuhnt , Klaus-Helmut Muller , Kurt Findeisen , Klaus Konig , Klaus Lurssen , Hans-Joachim Santel , Robert R. Schmidt
IPC分类号： A01N47/38 , C07D249/12 , C07D405/12 , A01N43/653
CPC分类号： C07D249/12 , A01N47/38
摘要： The invention relates to novel substituted triazolinones of the general formula (I) ##STR1## in which R.sup.1 represents alkyl or cycloalkyl,R.sup.2 represents cycloalkyl which is optionally substituted by aryl, arylalkyl, arylalkenyl or arylalkinyl, or represents a radical of the formula ##STR2## X represents oxygen or sulphur and Y represents oxygen or sulphur, whereR.sup.3, R.sup.4, R.sup.5, R.sup.6, R.sup.7 and R.sup.8 represent hydrogen or alkyl,R.sup.9 represents in each case optionally substituted cycloalkyl, aryl or heteroaryl andn represents a number 0, 1, 2 or 3,but with the exception of those compounds in which, simultaneously, R.sup.1 represents a methyl radical, X represents oxygen, Y represents oxygen and R.sup.2 represents a radical of the formula ##STR3## a plurality of processes and novel intermediates for their preparation, and their use as herbicides.
摘要翻译：本发明涉及通式（I）的化合物（I）的取代三唑啉酮，其中R1代表烷基或环烷基，R2代表任选被芳基，芳基烷基，芳基烯基或芳基炔基取代的环烷基，或代表式X表示氧或硫，Y表示氧或硫，其中R 3，R 4，R 5，R 6，R 7和R 8表示氢或烷基，R 9在各情况下表示任选取代的环烷基，芳基或杂芳基，n表示数 0,1,2或3，但是除了其中R1代表甲基基团的那些化合物除外，X代表氧，Y代表氧，R2代表下式的基团：多种方法及其制备中的新型中间体及其作为除草剂的用途。

88. 发明授权

US5266555A Substituted triazoles 失效
标题翻译：取代三唑
公开(公告)号：US5266555A
公开(公告)日：1993-11-30
申请号：US911450
申请日：1992-07-10
申请人： Kurt Findeisen , Dietmar Kuhnt , Klaus-Helmut Muller , Klaus Konig , Hans-Joachim Santel , Klaus Lurssen , Robert R. Schmidt
发明人： Kurt Findeisen , Dietmar Kuhnt , Klaus-Helmut Muller , Klaus Konig , Hans-Joachim Santel , Klaus Lurssen , Robert R. Schmidt
IPC分类号： A01N43/653 , C07D249/14 , C07D405/12
CPC分类号： A01N43/653 , C07D249/14
摘要： The invention relates to new substituted triazoles of the general formula (1) ##STR1## in which R.sup.1 represents alkyl,R.sup.2 represents alkyl,R.sup.3 represents alkyl,R.sup.4 represents in each case optionally substituted cycloalkyl or aryl,R.sup.5 represents either hydrogen, alkyl or cyano andR.sup.6 represents hydrogen or alkyl orR.sup.5 and R.sup.6 together represent divalent alkanediyl,A represents one of the radicals --CH.sub.2 --CH.sub.2 --; --CH(CH.sub.3)--CH.sub.2 --; --CH.sub.2 --O--; --CH.sub.2 --S--; --CH.sub.2 --N(R.sup.7)--; --CH.dbd.CH-- or --C.dbd.C-- andX represents oxygen or sulphur, whereR.sup.7 represents hydrogen, alkyl or alkanoyl,but with the exception of the compound 5-dimethylamino-4-methyl-3-(4-phenylbut-2-ylaminocarbonyl)-1,2,4-triazole,a plurality of processes for their preparation, and their use as herbicides.
摘要翻译：本发明涉及通式（1）的新的取代三唑，其中R 1表示烷基，R 2表示烷基，R 3表示烷基，R 4表示在各种情况下任选取代的环烷基或芳基，R 5表示氢，烷基或氰基，R 6表示氢或烷基或R 5和R 6一起表示二价烷二基，A表示基团-CH 2 -CH 2 - 之一; -CH（CH 3）-CH 2 - ; -CH 2 -O-; -CH 2 -S-; -CH 2 -N（R 7） - ; -CH = CH-或-C = C-，X表示氧或硫，其中R7表示氢，烷基或烷酰基，但化合物5-二甲基氨基-4-甲基-3-（4-苯基丁-2- 芳基氨基羰基）-1,2,4-三唑，多种制备方法及其作为除草剂的用途。

89. 发明授权

US5194085A Herbicidal substituted triazolinones 失效
标题翻译：除草取代的三唑啉酮
公开(公告)号：US5194085A
公开(公告)日：1993-03-16
申请号：US660321
申请日：1991-02-22
申请人： Markus Lindig , Kurt Findeisen , Klaus-Helmut Muller , Hans-Joachim Santel , Robert R. Schmidt , Harry Strang , Dieter Feucht , Klaus Konig , Klaus Lurssen
发明人： Markus Lindig , Kurt Findeisen , Klaus-Helmut Muller , Hans-Joachim Santel , Robert R. Schmidt , Harry Strang , Dieter Feucht , Klaus Konig , Klaus Lurssen
IPC分类号： A01N47/38 , C07D249/12 , C07D405/12
CPC分类号： C07D405/12 , A01N47/38 , C07D249/12
摘要： Herbicidally active substituted triazolinones of the formula ##STR1## in which R.sup.1 represents hydrogen, alkyl, alkenyl, alkinyl, halogenoalkyl, halogenoalkenyl, halogenoalkinyl, alkoxyalkyl, cycloalkyl, cycloalkylalkyl, or represents tetrahydrofuranyl, tetrahydrofuranylalkyl, or represents in each case optionally substituted aralkyl or aryl,R.sup.2 represents hydrogen, alkyl, alkenyl, alkinyl, halogenoalkyl, halogenoalkenyl, halogenoalkinyl, cyanoalkyl, hydroxyalkyl, alkoxyalkyl, alkoxycarbonylalkyl, alkoxycarbonylalkenyl, alkylaminoalkyl, dialkylaminoalkyl, or represents in each case optionally substituted cycloalkyl, cycloalkylalkyl, cycloalkenyl or cycloalkenylalkyl, or represents optionally substituted heterocyclylalkyl, or represents in each case optionally substituted aralkyl, aroyl, aryl, aralkyloxy or aryloxy, or represents alkoxy, alkenyloxy or alkinyloxy,X represents oxygen or sulphur andY represents oxygen or sulphur.New intermediates therefor are also shown.
摘要翻译：式（I）的除草活性取代的三唑啉酮，其中R 1表示氢，烷基，烯基，炔基，卤代烷基，卤代烯基，卤代烯基，烷氧基烷基，环烷基，环烷基烷基，或代表四氢呋喃基，四氢呋喃基烷基，或表示在各种情况下任选取代芳烷基或芳基，R 2表示氢，烷基，烯基，炔基，卤代烷基，卤代烯基，卤代烷基，氰基烷基，羟基烷基，烷氧基烷基，烷氧基羰基烷基，烷氧基羰基烯基，烷基氨基烷基，二烷基氨基烷基，或在每种情况下表示任选取代的环烷基，环烷基烷基，环烯基或环烯基烷基，或或者表示任意取代的芳烷基，芳酰基，芳基，芳烷氧基或芳氧基，或表示烷氧基，烯氧基或烷氧基，X表示氧或硫，Y表示氧或硫。还显示了其新的中间体。

90. 发明授权

US5043092A Process for the production of polyisocyanate mixtures containing uretdione and isocyanurate groups 失效
标题翻译：制备含有脲二酮和异氰脲酸酯基团的多异氰酸酯混合物的方法
公开(公告)号：US5043092A
公开(公告)日：1991-08-27
申请号：US323538
申请日：1989-03-13
申请人： Josef Pedain , Klaus Konig , Winfried Dell
发明人： Josef Pedain , Klaus Konig , Winfried Dell
IPC分类号： C07B61/00 , C07D229/00 , C07D251/34 , C08G18/78 , C08G18/79 , C09D175/00 , C09D175/04
CPC分类号： C08G18/792 , C07D229/00 , C07D251/34 , C08G18/798 , C08G2150/20
摘要： The present invention is directed to a process for the production of polyisocyanate mixtures containing isocyanurate groups and uretdione groups in a molar ratio of about 1:9 to 9:1 by oligomerizing a portion of the isocyanate groups of hexamethylene diisocyanate using trialkyl phosphines and/or peralkylated phosphorus acid triamides as the catalysts which accelerate the dimerization and trimerization of isocyanate groups, terminating the reaction at the desired degree of oligomerization by the addition of a catalyst poison and removing unreacted hexamethylene diisocyanate to a residual content of at most 0.5% by weight, characterized in that, before addition of the catalyst, the hexamethylene diisocyanate starting material is freed from carbon dioxide to a residual content of less than 20 ppm (weight).The present invention is also directed to the polyisocyanates containing uretdione groups and isocyanurate groups obtainable by this process and their use, optionally blocked by blocking agents for isocyanate groups, as the isocyanate component for the production of polyisocyanate polyaddition products.
摘要翻译：本发明涉及通过使用三烷基膦和/或它们的一部分使六亚甲基二异氰酸酯的一部分异氰酸酯基团低聚而制备含有摩尔比为约1:9至9:1的异氰脲酸酯基和脲二酮基团的多异氰酸酯混合物的方法和/或全烷基化的磷酸三酰胺作为加速异氰酸酯基团的二聚和三聚的催化剂，通过加入催化剂毒物终止反应在所需的低聚度程度，并除去未反应的六亚甲基二异氰酸酯至残余含量至多0.5重量％其特征在于，在加入催化剂之前，将六亚甲基二异氰酸酯原料从二氧化碳中除去至少于20ppm（重量）的残留量。本发明还涉及含有脲二酮基团和异氰脲酸酯基团的多异氰酸酯基团，其可通过该方法获得，并且其用途，任选地被异氰酸酯基团的封闭剂封闭，作为用于制备多异氰酸酯加聚产物的异氰酸酯组分。

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