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71. 发明公开

US20240308863A1 LOW VACANCY Fe-SUBSTITUTED Mn-BASED PRUSSIAN BLUE ANALOGUE 审中-公开
公开(公告)号：US20240308863A1
公开(公告)日：2024-09-19
申请号：US18604260
申请日：2024-03-13
申请人： Natron Energy, Inc.
发明人： Ashenafi Damtew Mamuye , Daniel Friebel , Aniruddh Shrivastava
IPC分类号： C01C3/11 , H01B1/10 , H01M4/02 , H01M4/58
CPC分类号： C01C3/11 , H01B1/10 , H01M4/58 , C01P2002/52 , C01P2002/72 , C01P2002/76 , C01P2004/03 , C01P2006/40 , H01M2004/021 , H01M2004/028
摘要： A system and method implementing and manufacturing transition metal cyanide coordination compounds (TMCCC) comprising Na, Fe, Mn, C, H, N, S, and O, wherein the TMCCC have 0-14% hexacyanometallate vacancies such as for application in electrochemical cells, including sodium ion secondary batteries; further including both sodium and potassium with and without sulfate.

72. 发明授权

US12071354B2 Multifunctional co-ordination framework materials 有权
公开(公告)号：US12071354B2
公开(公告)日：2024-08-27
申请号：US17046947
申请日：2019-04-12
申请人： RUX TECHNOLOGY PTY LTD
发明人： Jehan Rux Rustom Kanga , Cameron John Kepert
IPC分类号： C01C3/11 , B01J20/22 , C01B3/00 , C01C3/12 , C07F15/00 , C07F15/02 , C07F15/04 , C07F15/06
CPC分类号： C01C3/11 , B01J20/226 , C01C3/12 , C07F15/0053 , C07F15/025 , C07F15/045 , C07F15/065 , C01B3/001
摘要： Disclosed herein is a class of co-ordination framework materials having various useful properties. The co-ordination frameworks comprise complexes of M2[M′(CN)6] or Ax(M2[M′(CN)6]), wherein M is selected from V, Cr, Mn, Fe, Co, Ni, Cu, Ag, Au, Zn, Ru, Rh, Pd and Pt; M′ is selected from Fe and Ru; A (when present) is located in the pores of the framework and is selected from Li+, Na+, K+, Be2+, Mg2+ and Ca2+; and x (when present) is 0

73. 发明授权

US09966602B2 Metal cyanometallates 有权
公开(公告)号：US09966602B2
公开(公告)日：2018-05-08
申请号：US15279588
申请日：2016-09-29
申请人： Sharp Laboratories of America, Inc.
发明人： Yuhao Lu , Long Wang , Sean Vail , Jong-Jan Lee
IPC分类号： H01M4/00 , H01M4/58 , C01C3/11 , C01C3/12
CPC分类号： H01M4/58 , C01C3/11 , C01C3/12 , C01P2002/50 , C01P2006/40
摘要： Methods are presented for synthesizing metal cyanometallate (MCM). A first method provides a first solution of AXM2Y(CN)Z, to which a second solution including M1 is dropwise added. As a result, a precipitate is formed of ANM1PM2Q (CN)R.FH2O, where N is in the range of 1 to 4. A second method for synthesizing MCM provides a first solution of M2C(CN)B, which is dropwise added to a second solution including M1. As a result, a precipitate is formed of M1[M2S(CN)G]1/T.DH2O, where S/T is greater than or equal to 0.8. Low vacancy MCM materials are also presented.

74. 发明授权

US09637395B2 Fluorine free tungsten ALD/CVD process 有权
公开(公告)号：US09637395B2
公开(公告)日：2017-05-02
申请号：US14431116
申请日：2013-09-26
申请人： ENTEGRIS, INC.
发明人： Weimin Li , David W. Peters , Scott L. Battle , William Hunks
IPC分类号： C07F11/00 , C01G41/00 , C23C16/16 , C23C16/18 , C23C16/448 , C01C3/11 , C09D5/24 , H01B1/02
CPC分类号： C01G41/006 , C01C3/11 , C07F11/00 , C07F11/005 , C09D5/24 , C23C16/16 , C23C16/18 , C23C16/4485 , H01B1/02
摘要： A tungsten precursor useful for forming tungsten-containing material on a substrate, e.g., in the manufacture of microelectronic devices. The tungsten precursor is devoid of fluorine content, and may be utilized in a solid delivery process or other vapor deposition technique, to form films such as elemental tungsten for metallization of integrated circuits, or tungsten nitride films or other tungsten compound films that are useful as base layers for subsequent elemental tungsten metallization.

75. 发明授权

US09567231B2 System and method for large scale synthesis of metal cyanometallates 有权
标题翻译：金属氰化金属的大规模合成的系统和方法
公开(公告)号：US09567231B2
公开(公告)日：2017-02-14
申请号：US15230395
申请日：2016-08-06
申请人： Sharp Laboratories of America, Inc.
发明人： Yuhao Lu , Wei Pan , Sean Vail , Jong-Jan Lee
IPC分类号： H01M4/56 , C01C3/11 , B01J19/18 , B01J19/24 , H01M4/58 , H01M10/0525 , H01M10/054
CPC分类号： C01C3/11 , B01J19/1862 , B01J19/2445 , B01J2219/00051 , B01J2219/24 , C01C3/12 , C01P2006/40 , H01M2/162 , H01M2/1646 , H01M4/136 , H01M4/1397 , H01M4/381 , H01M4/387 , H01M4/58 , H01M4/5825 , H01M4/622 , H01M4/623 , H01M10/0525 , H01M10/054 , H01M10/0585
摘要： A system and method are presented for the large scale synthesis of metal cyanometallates (MCMs). First and second precursor solutions are added to a main reactor, where the first precursor includes M1 metal cations. The second precursor solution includes AX′M2(CN)Z′, where M1 and M2 are from a first group of metals and A is from a second group of metals including alkali or alkaline earth metals. In response to stirring the first and second precursors, MCM particles are formed with the formula AXM1NM2M(CN)Z.d[H2O]ZEO.e[H2O]BND, in solution. In response to aging in the secondary reactor, the size of the MCM particles is increases. The aged MCM particles in solution are then transferred to a separation tank, where the aged MCM particles are filtered from the solution and collected. The solution reclaimed from the separation tank back is added back into the main reactor.
摘要翻译：提出了一种用于大规模合成金属氰金属（MCM）的系统和方法。将第一和第二前体溶液加入到主反应器中，其中第一前体包括M1金属阳离子。第二前体溶液包括AX'M2（CN）Z'，其中M1和M2来自第一组金属，A来自第二组金属，包括碱金属或碱土金属。响应于搅拌第一和第二前体，在溶液中用式AXM1NM2M（CN）Z.d [H2O] ZEO.e [H2O] BND形成MCM颗粒。响应于二次反应器中的老化，MCM颗粒的尺寸增加。然后将溶液中的老化MCM颗粒转移到分离槽中，其中将老化的MCM颗粒从溶液中过滤并收集。从分离罐回收的溶液回到主反应器中。

76. 发明申请

US20170018774A1 Metal Cyanometallates 有权
标题翻译：金属氰酸金属盐
公开(公告)号：US20170018774A1
公开(公告)日：2017-01-19
申请号：US15279588
申请日：2016-09-29
申请人： Sharp Laboratories of America, Inc.
发明人： Yuhao Lu , Long Wang , Sean Vail , Jong-Jan Lee
IPC分类号： H01M4/58 , C01C3/12 , C01C3/11
CPC分类号： H01M4/58 , C01C3/11 , C01C3/12 , C01P2002/50 , C01P2006/40
摘要： Methods are presented for synthesizing metal cyanometallate (MCM). A first method provides a first solution of AXM2Y(CN)Z, to which a second solution including M1 is dropwise added. As a result, a precipitate is formed of ANM1PM2Q (CN)R.FH2O, where N is in the range of 1 to 4. A second method for synthesizing MCM provides a first solution of M2C(CN)B, which is dropwise added to a second solution including M1. As a result, a precipitate is formed of M1[M2S(CN)G]1/T.DH2O, where S/T is greater than or equal to 0.8. Low vacancy MCM materials are also presented.
摘要翻译：提出了合成金属氰金属（MCM）的方法。第一种方法提供AXM2Y（CN）Z的第一溶液，向其中滴加包含M1的第二溶液。结果，由ANM1PM2Q（CN）R.FH2O形成沉淀物，其中N在1至4的范围内。合成MCM的第二种方法是提供M2C（CN）B的第一溶液，将其逐滴加入包括M1的第二个解决方案。结果，由M1 [M2S（CN）G] 1 / T.DH2O形成沉淀物，其中S / T大于或等于0.8。还提出了低空缺MCM材料。

77. 发明授权

US09484578B2 Method for the synthesis of metal cyanometallates 有权
标题翻译：金属氰化金属合成方法
公开(公告)号：US09484578B2
公开(公告)日：2016-11-01
申请号：US14289746
申请日：2014-05-29
申请人： Sharp Laboratories of America, Inc.
发明人： Yuhao Lu , Long Wang , Sean Vail , Jong-Jan Lee
IPC分类号： H01M4/58 , C01C3/11 , C01C3/12
CPC分类号： H01M4/58 , C01C3/11 , C01C3/12 , C01P2002/50 , C01P2006/40
摘要： Methods are presented for synthesizing metal cyanometallate (MCM). A first method provides a first solution of AXM2Y(CN)Z, to which a second solution including M1 is dropwise added. As a result, a precipitate is formed of ANM1PM2Q(CN)R.FH2O, where N is in the range of 1 to 4. A second method for synthesizing MCM provides a first solution of M2C(CN)B, which is dropwise added to a second solution including M1. As a result, a precipitate is formed of M1[M2S(CN)G]1/T. DH2O, where S/T is greater than or equal to 0.8. Low vacancy MCM materials are also presented.
摘要翻译：提出了合成金属氰金属（MCM）的方法。第一种方法提供AXM2Y（CN）Z的第一溶液，向其中滴加包含M1的第二溶液。结果，由ANM1PM2Q（CN）R.FH2O形成沉淀物，其中N在1至4的范围内。合成MCM的第二种方法是提供M2C（CN）B的第一溶液，将其逐滴加入包括M1的第二个解决方案。结果，M1 [M2S（CN）G] 1 / T形成沉淀物。 DH2O，其中S / T大于或等于0.8。还提出了低空缺MCM材料。

78. 发明申请

US20160056467A1 Alkali-Ion Battery with Enhanced Transition Metal Cyanometallate Electrode Structure 有权
标题翻译：具有增强的金属氰酸金属电极结构的碱性离子电池
公开(公告)号：US20160056467A1
公开(公告)日：2016-02-25
申请号：US14928559
申请日：2015-10-30
申请人： Sharp Laboratories of America, Inc.
发明人： Jie Song , Yuhao Lu , Xin Zhao
IPC分类号： H01M4/58 , H01M2/16 , H01M10/0525 , H01M10/058 , H01M4/583 , H01M4/38 , H01M4/56 , H01M4/62 , H01M10/054
CPC分类号： H01M4/5825 , C01C3/11 , H01M2/162 , H01M2/1626 , H01M2/1646 , H01M4/136 , H01M4/1397 , H01M4/381 , H01M4/387 , H01M4/56 , H01M4/622 , H01M4/623 , H01M10/054 , H01M10/0585
摘要： An alkali-ion battery is provided with a transition metal cyanometallate (TMCM) sheet cathode and a non-alkaline metal anode. The fabrication method mixes TMCM powders, conductive additives, and a polytetrafluoroethylene binder with a solution containing water, forming a wet paste. The wet paste is formed into a free-standing sheet of cathode active material, which is laminated to a cathode current collector, forming a cathode electrode. The free-standing sheet of cathode active material has a thickness typically in the range of 100 microns to 2 millimeters. The cathode electrode is assembled with a non-alkaline metal anode electrode and an ion-permeable membrane interposed between the cathode electrode and anode electrode, forming an assembly. The assembly is dried at a temperature of greater than 100 degrees C. The dried assembly is then inserted into a container (case) and electrolyte is added. Thick anodes made from free-standing sheets of active material can be similarly formed.
摘要翻译：碱金属离子电池具有过渡金属氰金属（TMCM）片阴极和非碱性金属阳极。制造方法将TMCM粉末，导电添加剂和聚四氟乙烯粘合剂与含有水的溶液混合，形成湿糊状物。将湿糊剂形成为阴极活性物质的自立片，其被层叠到阴极集电体上，形成阴极电极。独立的阴极活性材料片的厚度通常在100微米至2毫米的范围内。阴极与非碱性金属阳极电极和置于阴极电极和阳极电极之间的离子透过膜组装，形成组件。将组件在大于100摄氏度的温度下干燥。然后将干燥的组件插入容器（壳体）中并加入电解质。可以类似地形成由自立的活性材料片制成的厚阳极。

79. 发明授权

US08658251B2 Method of producing structural member having prussian blue-type metal complex nanoparticles, structural member obtained by the method, substrate, electrochromic device, rectifying device, and photo responding device, using the structural member 失效
标题翻译：制备具有普鲁士蓝型金属络合物纳米颗粒的结构件的方法，通过该方法获得的结构件，基板，电致变色装置，整流装置和光响应装置，使用结构件
公开(公告)号：US08658251B2
公开(公告)日：2014-02-25
申请号：US13001116
申请日：2009-06-26
申请人： Tohru Kawamoto , Hisashi Tanaka , Masato Kurihara , Masatomi Sakamoto , Ayako Oomura , Hiroshi Watanabe , Akihito Goto
发明人： Tohru Kawamoto , Hisashi Tanaka , Masato Kurihara , Masatomi Sakamoto , Ayako Oomura , Hiroshi Watanabe , Akihito Goto
IPC分类号： B05D3/00 , B05D1/40 , B05D3/02
CPC分类号： C23C26/00 , B82Y30/00 , C01C3/11 , C01C3/12 , C01P2002/72 , C01P2002/77 , C01P2004/04 , C01P2004/52 , C01P2004/64 , C01P2006/40 , C23C24/08 , C23C28/00
摘要： A method of producing a structural member having Prussian blue-type metal complex nanoparticles, the method including: constructing the structural member stabilized by a particular process in producing the structural member by providing nanoparticles consisting of Prussian blue-type metal complex onto a substrate; and a structural member having Prussian blue-type metal complex nanoparticles, the structural member having water-dispersible nanoparticles consisting of Prussian blue-type metal complex provided on a substrate and the structural member being stabilized in water by a particular process.
摘要翻译：一种制备具有普鲁士蓝型金属络合物纳米颗粒的结构件的方法，所述方法包括：通过将由普鲁士蓝型金属络合物构成的纳米颗粒提供到基底上来构造通过特定方法稳定的结构构件来制造结构构件; 和具有普鲁士蓝型金属络合物纳米颗粒的结构构件，该结构构件具有由在基体上提供的普鲁士蓝型金属络合物组成的水分散性纳米颗粒，并且结构构件通过特定方法稳定在水中。

80. 发明授权

US08349221B2 Method of producing prussian blue-type metal complex nanoparticles, and prussian blue-type metal complex nanoparticles obtained by the method, dispersion of the nanoparticles, method of regulating the color of the nanoparticles, and electrode and transmitted light-regulator each using the nanoparticles 有权
标题翻译：制备普鲁士蓝型金属络合物纳米颗粒的方法和通过该方法获得的普鲁士蓝型金属络合物纳米颗粒，纳米颗粒的分散体，调节纳米颗粒颜色的方法，以及每个使用纳米颗粒的电极和透射光调节剂
公开(公告)号：US08349221B2
公开(公告)日：2013-01-08
申请号：US12521520
申请日：2007-12-28
申请人： Tohru Kawamoto , Hisashi Tanaka , Shigeo Hara , Masato Kurihara , Masatomi Sakamoto
发明人： Tohru Kawamoto , Hisashi Tanaka , Shigeo Hara , Masato Kurihara , Masatomi Sakamoto
IPC分类号： C07F15/02
CPC分类号： C01C3/11 , B82Y30/00 , C01C3/12 , C01P2002/72 , C01P2002/77 , C01P2002/84 , C01P2004/04 , C01P2004/64 , C09D11/037 , C09D11/322 , C09D11/38 , G02F1/1523 , G02F2001/1517
摘要： A method of producing Prussian blue metal complex nanoparticles and Prussian blue metal complex nanoparticles obtained by the method, a dispersion of the nanoparticles, a method of regulating the color of the nanoparticles, and an electrode and a transmitted light-regulator each using the nanoparticles. Prussian blue metal complex nanoparticles are produced by: mixing an aqueous solution containing a metal cyano complex anion having metal atom MA as a central metal and an aqueous solution containing a cation of metal atom MB; thereby precipitating the crystal of a Prussian blue metal complex having the metal atom MA and the metal atom MB; and then mixing the Prussian blue metal complex with an aqueous solution containing a metal cyano complex anion having the metal atom MC as a central metal and/or an aqueous solution containing a cation of the metal atom MD.
摘要翻译：通过该方法制备普鲁士蓝金属络合物纳米颗粒和普鲁士蓝金属络合物纳米颗粒的方法，纳米颗粒的分散体，调节纳米颗粒颜色的方法，以及每个使用纳米颗粒的电极和透射光调节剂。普鲁士蓝金属络合物纳米颗粒通过以下方式制备：将含有金属原子MA的金属氰基络合物阴离子的水溶液作为中心金属和含有金属原子MB的阳离子的水溶液混合; 从而析出具有金属原子MA和金属原子MB的普鲁士蓝金属络合物的晶体; 然后将普鲁士蓝金属络合物与含有金属原子MC作为中心金属的金属氰基络合物阴离子和/或含有金属原子MD阳离子的水溶液的水溶液混合。

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