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71. 发明授权

US09484578B2 Method for the synthesis of metal cyanometallates 有权
标题翻译：金属氰化金属合成方法
公开(公告)号：US09484578B2
公开(公告)日：2016-11-01
申请号：US14289746
申请日：2014-05-29
申请人： Sharp Laboratories of America, Inc.
发明人： Yuhao Lu , Long Wang , Sean Vail , Jong-Jan Lee
IPC分类号： H01M4/58 , C01C3/11 , C01C3/12
CPC分类号： H01M4/58 , C01C3/11 , C01C3/12 , C01P2002/50 , C01P2006/40
摘要： Methods are presented for synthesizing metal cyanometallate (MCM). A first method provides a first solution of AXM2Y(CN)Z, to which a second solution including M1 is dropwise added. As a result, a precipitate is formed of ANM1PM2Q(CN)R.FH2O, where N is in the range of 1 to 4. A second method for synthesizing MCM provides a first solution of M2C(CN)B, which is dropwise added to a second solution including M1. As a result, a precipitate is formed of M1[M2S(CN)G]1/T. DH2O, where S/T is greater than or equal to 0.8. Low vacancy MCM materials are also presented.
摘要翻译：提出了合成金属氰金属（MCM）的方法。第一种方法提供AXM2Y（CN）Z的第一溶液，向其中滴加包含M1的第二溶液。结果，由ANM1PM2Q（CN）R.FH2O形成沉淀物，其中N在1至4的范围内。合成MCM的第二种方法是提供M2C（CN）B的第一溶液，将其逐滴加入包括M1的第二个解决方案。结果，M1 [M2S（CN）G] 1 / T形成沉淀物。 DH2O，其中S / T大于或等于0.8。还提出了低空缺MCM材料。

72. 发明申请

US20160056467A1 Alkali-Ion Battery with Enhanced Transition Metal Cyanometallate Electrode Structure 有权
标题翻译：具有增强的金属氰酸金属电极结构的碱性离子电池
公开(公告)号：US20160056467A1
公开(公告)日：2016-02-25
申请号：US14928559
申请日：2015-10-30
申请人： Sharp Laboratories of America, Inc.
发明人： Jie Song , Yuhao Lu , Xin Zhao
IPC分类号： H01M4/58 , H01M2/16 , H01M10/0525 , H01M10/058 , H01M4/583 , H01M4/38 , H01M4/56 , H01M4/62 , H01M10/054
CPC分类号： H01M4/5825 , C01C3/11 , H01M2/162 , H01M2/1626 , H01M2/1646 , H01M4/136 , H01M4/1397 , H01M4/381 , H01M4/387 , H01M4/56 , H01M4/622 , H01M4/623 , H01M10/054 , H01M10/0585
摘要： An alkali-ion battery is provided with a transition metal cyanometallate (TMCM) sheet cathode and a non-alkaline metal anode. The fabrication method mixes TMCM powders, conductive additives, and a polytetrafluoroethylene binder with a solution containing water, forming a wet paste. The wet paste is formed into a free-standing sheet of cathode active material, which is laminated to a cathode current collector, forming a cathode electrode. The free-standing sheet of cathode active material has a thickness typically in the range of 100 microns to 2 millimeters. The cathode electrode is assembled with a non-alkaline metal anode electrode and an ion-permeable membrane interposed between the cathode electrode and anode electrode, forming an assembly. The assembly is dried at a temperature of greater than 100 degrees C. The dried assembly is then inserted into a container (case) and electrolyte is added. Thick anodes made from free-standing sheets of active material can be similarly formed.
摘要翻译：碱金属离子电池具有过渡金属氰金属（TMCM）片阴极和非碱性金属阳极。制造方法将TMCM粉末，导电添加剂和聚四氟乙烯粘合剂与含有水的溶液混合，形成湿糊状物。将湿糊剂形成为阴极活性物质的自立片，其被层叠到阴极集电体上，形成阴极电极。独立的阴极活性材料片的厚度通常在100微米至2毫米的范围内。阴极与非碱性金属阳极电极和置于阴极电极和阳极电极之间的离子透过膜组装，形成组件。将组件在大于100摄氏度的温度下干燥。然后将干燥的组件插入容器（壳体）中并加入电解质。可以类似地形成由自立的活性材料片制成的厚阳极。

73. 发明授权

US08658251B2 Method of producing structural member having prussian blue-type metal complex nanoparticles, structural member obtained by the method, substrate, electrochromic device, rectifying device, and photo responding device, using the structural member 失效
标题翻译：制备具有普鲁士蓝型金属络合物纳米颗粒的结构件的方法，通过该方法获得的结构件，基板，电致变色装置，整流装置和光响应装置，使用结构件
公开(公告)号：US08658251B2
公开(公告)日：2014-02-25
申请号：US13001116
申请日：2009-06-26
申请人： Tohru Kawamoto , Hisashi Tanaka , Masato Kurihara , Masatomi Sakamoto , Ayako Oomura , Hiroshi Watanabe , Akihito Goto
发明人： Tohru Kawamoto , Hisashi Tanaka , Masato Kurihara , Masatomi Sakamoto , Ayako Oomura , Hiroshi Watanabe , Akihito Goto
IPC分类号： B05D3/00 , B05D1/40 , B05D3/02
CPC分类号： C23C26/00 , B82Y30/00 , C01C3/11 , C01C3/12 , C01P2002/72 , C01P2002/77 , C01P2004/04 , C01P2004/52 , C01P2004/64 , C01P2006/40 , C23C24/08 , C23C28/00
摘要： A method of producing a structural member having Prussian blue-type metal complex nanoparticles, the method including: constructing the structural member stabilized by a particular process in producing the structural member by providing nanoparticles consisting of Prussian blue-type metal complex onto a substrate; and a structural member having Prussian blue-type metal complex nanoparticles, the structural member having water-dispersible nanoparticles consisting of Prussian blue-type metal complex provided on a substrate and the structural member being stabilized in water by a particular process.
摘要翻译：一种制备具有普鲁士蓝型金属络合物纳米颗粒的结构件的方法，所述方法包括：通过将由普鲁士蓝型金属络合物构成的纳米颗粒提供到基底上来构造通过特定方法稳定的结构构件来制造结构构件; 和具有普鲁士蓝型金属络合物纳米颗粒的结构构件，该结构构件具有由在基体上提供的普鲁士蓝型金属络合物组成的水分散性纳米颗粒，并且结构构件通过特定方法稳定在水中。

74. 发明授权

US08349221B2 Method of producing prussian blue-type metal complex nanoparticles, and prussian blue-type metal complex nanoparticles obtained by the method, dispersion of the nanoparticles, method of regulating the color of the nanoparticles, and electrode and transmitted light-regulator each using the nanoparticles 有权
标题翻译：制备普鲁士蓝型金属络合物纳米颗粒的方法和通过该方法获得的普鲁士蓝型金属络合物纳米颗粒，纳米颗粒的分散体，调节纳米颗粒颜色的方法，以及每个使用纳米颗粒的电极和透射光调节剂
公开(公告)号：US08349221B2
公开(公告)日：2013-01-08
申请号：US12521520
申请日：2007-12-28
申请人： Tohru Kawamoto , Hisashi Tanaka , Shigeo Hara , Masato Kurihara , Masatomi Sakamoto
发明人： Tohru Kawamoto , Hisashi Tanaka , Shigeo Hara , Masato Kurihara , Masatomi Sakamoto
IPC分类号： C07F15/02
CPC分类号： C01C3/11 , B82Y30/00 , C01C3/12 , C01P2002/72 , C01P2002/77 , C01P2002/84 , C01P2004/04 , C01P2004/64 , C09D11/037 , C09D11/322 , C09D11/38 , G02F1/1523 , G02F2001/1517
摘要： A method of producing Prussian blue metal complex nanoparticles and Prussian blue metal complex nanoparticles obtained by the method, a dispersion of the nanoparticles, a method of regulating the color of the nanoparticles, and an electrode and a transmitted light-regulator each using the nanoparticles. Prussian blue metal complex nanoparticles are produced by: mixing an aqueous solution containing a metal cyano complex anion having metal atom MA as a central metal and an aqueous solution containing a cation of metal atom MB; thereby precipitating the crystal of a Prussian blue metal complex having the metal atom MA and the metal atom MB; and then mixing the Prussian blue metal complex with an aqueous solution containing a metal cyano complex anion having the metal atom MC as a central metal and/or an aqueous solution containing a cation of the metal atom MD.
摘要翻译：通过该方法制备普鲁士蓝金属络合物纳米颗粒和普鲁士蓝金属络合物纳米颗粒的方法，纳米颗粒的分散体，调节纳米颗粒颜色的方法，以及每个使用纳米颗粒的电极和透射光调节剂。普鲁士蓝金属络合物纳米颗粒通过以下方式制备：将含有金属原子MA的金属氰基络合物阴离子的水溶液作为中心金属和含有金属原子MB的阳离子的水溶液混合; 从而析出具有金属原子MA和金属原子MB的普鲁士蓝金属络合物的晶体; 然后将普鲁士蓝金属络合物与含有金属原子MC作为中心金属的金属氰基络合物阴离子和/或含有金属原子MD阳离子的水溶液的水溶液混合。

75. 发明授权

US06214234B1 Method for the removal of cesium from radioactive waste liquids 有权
标题翻译：从放射性废液中去除铯的方法
公开(公告)号：US06214234B1
公开(公告)日：2001-04-10
申请号：US09202453
申请日：1998-12-15
申请人： Risto Harjula , Jukka Lehto
发明人： Risto Harjula , Jukka Lehto
IPC分类号： C02F142
CPC分类号： G21F9/12 , B01J39/02 , B01J39/09 , C01C3/11 , C01D17/00 , C01P2004/50 , C01P2004/61 , C22B3/42 , C22B26/10 , G21F9/007 , Y02P10/234
摘要： A method for removal of cesium from aqueous solution, particularly from nuclear waste liquids. The cesium-containing aqueous solution is contacted with a solid-state hexacyanoferrate compound of a transition element for binding cesium to the hexacyanoferrate. The aqueous solution of reduced cesium content is separated from the hexacyanoferrate. Preferably, a nickel or cobalt hexacyanoferrate is utilized having a fraction of exchangeable transition elements smaller than 35 %. The hexacyanoferrate compound of said transition element may be produced by slowly adding an aqueous solution of the hexacyanoferrate into the transition element salt solution, the concentration of the transition element salt solution being at least 0.35 mol/l, stirring the mixture at ambient temperature during the addition, and separating and recovering the resulting hexacyanoferrate precipitate from the mixture. This method has achieved volume reductions—that is, volume of cesium-containing waste liquid remaining in the ion-exchange column reduced from volume of cesium-containing aqueous solution treated—of as much as 9000 fold.
摘要翻译：一种从水溶液中除去铯的方法，特别是从核废液中除去铯。含铯水溶液与用于将铯结合到六氰基铁酸盐的过渡元素的固态六氰基铁酸盐化合物接触。将还原的铯含量的水溶液与六氰基铁酸盐分离。优选地，使用具有小于35％的可交换过渡元素的一部分的六氰基铁酸镍或钴。所述过渡元素的六氰基铁酸盐化合物可以通过将六氰基铁酸盐的水溶液缓慢加入到过渡元素盐溶液中，过渡元素盐溶液的浓度为至少0.35mol / l，在环境温度下搅拌该混合物加入，并从混合物中分离和回收得到的六氰基铁酸盐沉淀。该方法已经实现体积减少 - 即离子交换塔中残留的含铯废液体积比处理的含铯水溶液的体积减少多达9000倍。

76. 发明授权

US4545966A Cuprous aluminum cyano trichloride: CuAl(CN)Cl.sub.3 : its preparation and use for the reversible complexing of unsaturated ligands 失效
标题翻译：氰化三氯化铝：CuAl（CN）Cl 3：其制备和用于不饱和配体的可逆络合
公开(公告)号：US4545966A
公开(公告)日：1985-10-08
申请号：US535165
申请日：1983-09-23
申请人： David G. Walker
发明人： David G. Walker
IPC分类号： B01D53/14 , C01B32/40 , C01C3/11 , C07C7/156
CPC分类号： C01B31/18 , B01D53/1493 , C01C3/11 , C07C7/156
摘要： An aromatic solution of the compound CuAl(CN)Cl.sub.3 alone or with additional solid CuAl(CN)Cl.sub.3 is used for the separation of some unsaturated compound (olefin, acetylene or carbon monoxide) from a feedstream.The feedstream is contacted with the solvent to form a complex of the ligand (olefin, acetylene or carbon monoxide). The feedstream is then separated from the solvent. The solvent is then treated with some combination of heat and lowered pressure to separate the ligand from the solvent. The ligand poor solvent is then recycled to contact fresh feedstream.
摘要翻译：化合物CuAl（CN）Cl3单独或附加固体CuAl（CN）Cl 3的芳香溶液用于从进料流中分离出一些不饱和化合物（烯烃，乙炔或一氧化碳）。使原料流与溶剂接触以形成配体（烯烃，乙炔或一氧化碳）的络合物。然后将原料流与溶剂分离。然后用热和低压的一些组合处理溶剂以将配体与溶剂分离。然后将配体不良溶剂再循环以接触新鲜进料流。

77. 发明授权

US4171344A Crystal growth from solution 失效
标题翻译：晶体从溶液中生长
公开(公告)号：US4171344A
公开(公告)日：1979-10-16
申请号：US483303
申请日：1974-06-26
申请人： Howard J. Guggenheim
发明人： Howard J. Guggenheim
IPC分类号： C01C3/11 , C01C3/00
CPC分类号： C30B29/58 , C01C3/11 , C30B35/002 , C30B7/14
摘要： Crystals are grown from solution by the introduction of a first fluid into a second fluid by permeation through a porous partition. Introduction of the first fluid produces supersaturation of the desired material in the combined fluid in the vicinity of the partition. Supersaturation results in the production of crystals. The crystals grow from the partition into the solution. The supersaturation is produced by one of several mechanisms including: chemical reaction producing a less soluble element or compound; decomplexation produced by dilution or pH change; and introduction of solution into a solvent in which the material is less soluble.
摘要翻译：晶体从溶液中生长，通过渗透通过多孔隔板将第一流体引入第二流体。引入第一种流体会在隔板附近的组合流体中产生所需材料的过饱和度。过饱和导致晶体生成。晶体从分区生长到溶液中。过饱和由几种机理之一产生，包括：产生较少可溶性元素或化合物的化学反应; 通过稀释或pH变化产生的络合; 并将溶液引入其中材料较不溶解的溶剂中。

78. 发明授权

US3904737A Metal cyanide complexes 失效
标题翻译：金属氰化物络合物
公开(公告)号：US3904737A
公开(公告)日：1975-09-09
申请号：US25007972
申请日：1972-05-03
申请人： PARIS RENE ANTOINE , AMBLARD PAUL ALEXIS , ROUSSET ABEL CLAUDE
发明人： PARIS RENE ANTOINE , AMBLARD PAUL ALEXIS , ROUSSET ABEL CLAUDE
IPC分类号： C01C3/08 , C01C3/11 , C01F15/00 , C01B21/00 , C01F17/00
CPC分类号： C01C3/08 , C01C3/11
摘要： Metal cyanide complexes of a single metal or mixed-metal complexes in which a metal is complexed with cyanide. The metals preferably include magnesium, beryllium, aluminum, chromium, titanium, zirconium, thorium, yttrium and cobalt and nickel in addition to the lanthanide metals. An aqueous solution is prepared and the complex is isolated by crystallization with a stoichiometry of the metals determined by their proportions in the solution.
摘要翻译：金属氰化物复合物，其中金属与氰化物络合的单一金属或混合金属络合物。除镧系金属之外，金属优选包括镁，铍，铝，铬，钛，锆，钍，钇和钴和镍。制备水溶液，并通过结晶化，通过其在溶液中的比例确定的金属的化学计量分离络合物。

79. 发明授权

US3655453A Cathode material for solid state batteries 失效
标题翻译：固体电池用阴极材料
公开(公告)号：US3655453A
公开(公告)日：1972-04-11
申请号：US3655453D
申请日：1970-07-16
申请人： UNION CARBIDE CORP
发明人： LOUZOS DEMETRIOS V , MELLORS GEOFFREY W
IPC分类号： C01C3/11 , H01M4/36 , H01M4/58 , H01M6/18 , H01M13/02 , C01C3/08 , H01M15/06
CPC分类号： H01M6/18 , C01C3/11 , C01P2006/40 , H01M4/36 , H01M4/58
摘要： The reaction product of elemental iodine and cyanides of zinc, cadmium or alkali metal produced by heating equimolar proportions of iodine and the cyanide at a temperature of about 220* C. in a sealed vessel in the absence of water is a good cathode material for solid electrolyte cells.
摘要翻译：在不存在水的情况下，在密封容器中，在约220℃的温度下加热等摩尔比例的碘和氰化物而产生的元素碘和锌，镉或碱金属的氰化物的反应产物是用于固体的良好的阴极材料电解质电池。

80. 发明授权

US1977440A Manufacture of lead sulphocyanide 失效
标题翻译：铅亚硫氰酸铅的制造
公开(公告)号：US1977440A
公开(公告)日：1934-10-16
申请号：US65726333
申请日：1933-02-17
申请人： DU PONT
发明人： ROBERTS HARRIS CHARLES
IPC分类号： C01C3/11 , C01C3/20
CPC分类号： C01C3/20 , C01C3/11

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