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71. 发明申请

US20090287026A1 METHOD FOR PRODUCING FLUORINATED ORGANIC COMPOUNDS 有权
标题翻译：生产氟化有机化合物的方法
公开(公告)号：US20090287026A1
公开(公告)日：2009-11-19
申请号：US12466271
申请日：2009-05-14
申请人： Haluk Kopkalli , Yuon Chiu , Hsueh Sung Tung
发明人： Haluk Kopkalli , Yuon Chiu , Hsueh Sung Tung
IPC分类号： C07C17/25
CPC分类号： C07C21/18 , C07C17/087 , C07C17/204 , C07C17/206 , C07C17/25 , C07C19/10
摘要： Disclosed is a process for producing tetrafluoropropene comprising: (a) catalytically fluorinating at least one tetrafluoropropene in a first reactor to produce HCFO-1233xf; (b) reacting said HCFO-1233xf with hydrogen fluoride in a second reactor to produce HCFC-244bb; (c) recycling at least a portion of said HCFC-244bb back to said first reactor as recycled HCFC-244bb; and (d) catalytically dehydrochlorinating said recycled HCFC-244bb in said first reactor to produce HFO-1234yf.
摘要翻译：公开了一种生产四氟丙烯的方法，包括：（a）在第一反应器中催化氟化至少一种四氟丙烯以产生HCFO-1233xf; （b）在第二反应器中使所述HCFO-1233xf与氟化氢反应以产生HCFC-244bb; （c）将所述HCFC-244bb的至少一部分再循环回所述第一反应器作为再循环HCFC-244bb; 和（d）在所述第一反应器中对所述再循环HCFC-244bb进行催化脱氯化氢以产生HFO-1234yf。

72. 发明申请

US20090270661A1 PROCESS FOR DEHYDROFLUORINATION OF 3-CHLORO-1,1,1,3-TETRAFLUOROPROPANE TO 1-CHLORO-3,3,3-TRIFLUOROPROPENE 有权
标题翻译： 3-氯代-1,1,1,3-四氢吡喃的脱氢方法制备1-氯-3,3,3-三氟硼烷的方法
公开(公告)号：US20090270661A1
公开(公告)日：2009-10-29
申请号：US12419002
申请日：2009-04-06
申请人： Haiyou Wang , Hsueh Sung Tung
发明人： Haiyou Wang , Hsueh Sung Tung
IPC分类号： C07C17/23
CPC分类号： C07C17/25 , C07C21/18
摘要： A process for making 1-chloro-3,3,3-trifluoropropene. The process has the following step: dehydrofluorinating 3-chloro-1,1,1,3-tetrafluoropropane under conditions sufficient to effect dehydrofluorination in the presence of a catalyst. Preferred catalysts are selected from the group consisting of (i) one or more halogenated trivalent or higher valent metal oxides, (ii) one or more trivalent or higher valent metal halides, and (iii) one or more natural or synthetic graphite materials.
摘要翻译：制备1-氯-3,3,3-三氟丙烯的方法。该方法具有以下步骤：在足以在催化剂存在下进行脱氟化氢的条件下，将3-氯-1,1,1,3-四氟丙烷脱氟化氢。优选的催化剂选自（i）一种或多种卤代三价或更高价金属氧化物，（ii）一种或多种三价或更高价金属卤化物，和（iii）一种或多种天然或合成石墨材料。

73. 发明申请

US20090270660A1 PROCESS FOR GEOMETRIC ISOMERIZATION OF HALOGENATED OLEFINS 有权
标题翻译：氢化烯烃的几何异构化过程
公开(公告)号：US20090270660A1
公开(公告)日：2009-10-29
申请号：US12499509
申请日：2009-07-08
申请人： HAIYOU WANG , Hsueh Sung Tung
发明人： HAIYOU WANG , Hsueh Sung Tung
IPC分类号： C07C17/358
CPC分类号： C07C17/358 , C07C21/18
摘要： Disclosed are processes for the conversion of isomerizable halogenated C2-C6 olefins from one geometric form to a more preferred geometric form. Preferred process aspects comprise converting C2-C6 olefin in a cis-form to a trans-form comprising exposing the cis-form of the compound, preferably contained in process stream, to conditions effective to convert at least about 50 percent, and even more preferably at least about 70 percent, of the cis-form compound to the trans-form compound. Preferably the catalyst comprises at least one Lewis acid metal fluoride.
摘要翻译：公开了将可异构化的卤代C 2 -C 6烯烃从一种几何形式转化为更优选的几何形式的方法。优选的方法方面包括将顺式形式的C 2 -C 6烯烃转化为反式，其包括将顺式形式的化合物（优选包含在工艺流中）暴露于有效转化至少约50％，甚至更优选至少约70％的顺式化合物转化成反式化合物。优选地，催化剂包含至少一种路易斯酸金属氟化物。

74. 发明申请

US20090209791A1 PROCESS FOR THE MANUFACTURE OF FLUORINATED OLEFINS 有权
标题翻译：氟化烯烃的制备方法
公开(公告)号：US20090209791A1
公开(公告)日：2009-08-20
申请号：US12389110
申请日：2009-02-19
申请人： Michael Van Der Puy , George R. Cook , Peter H. Sheidle , Kevin D. Uhrich , Haiyou Wang , Hsueh Sung Tung
发明人： Michael Van Der Puy , George R. Cook , Peter H. Sheidle , Kevin D. Uhrich , Haiyou Wang , Hsueh Sung Tung
IPC分类号： C07C17/00 , C07C17/25
CPC分类号： C07C17/25 , C07C17/354 , C07C17/38 , C07C19/14 , C07C19/08
摘要： A process for the production of fluorinated olefins, preferably fluorinated propenes, by contacting a feed stream containing a fluorinated olefin and hydrogen with a first amount of catalyst to produce the hydrofluorocarbon, wherein a first exit stream contains unreacted fluorinated olefin and hydrogen; contacting the first exit stream with a second amount of catalyst to produce a hydrofluorocarbon, wherein the second amount of catalyst is preferably greater than the first amount of catalyst; and contacting the hydrofluorocarbon with a catalyst for dehydrohalogenation to produce a product stream of fluorinated olefin.
摘要翻译：通过使包含氟化烯烃和氢气的进料流与第一量催化剂接触以产生氢氟烃来生产氟化烯烃，优选氟化丙烯的方法，其中第一出口流含有未反应的氟化烯烃和氢; 使第一出口流与第二量的催化剂接触以产生氢氟烃，其中第二量的催化剂优选大于第一量的催化剂; 并将氢氟烃与用于脱卤化氢的催化剂接触以产生氟化烯烃的产物流。

75. 发明授权

US07557254B2 Method for producing fluorinated organic compounds 有权
标题翻译：氟化有机化合物的制备方法
公开(公告)号：US07557254B2
公开(公告)日：2009-07-07
申请号：US12134629
申请日：2008-06-06
申请人： Sudip Mukhopadhyay , Hsueh Sung Tung , Haridasan Nair , Jingji Ma
发明人： Sudip Mukhopadhyay , Hsueh Sung Tung , Haridasan Nair , Jingji Ma
IPC分类号： C07C17/04 , C07C17/278 , C07C17/281
CPC分类号： B01J27/125 , B01J27/10 , B01J27/12 , C07C17/00 , C07C17/278 , C07C21/18 , C07C19/08
摘要： A method for preparing fluorinated organic compounds wherein at least one fluorinated olefin is reacted with methyl fluoride in the gas-phase and in the presence of a Lewis Acid catalyst to form at least one product having at least 3 carbon atoms.
摘要翻译：一种制备氟化有机化合物的方法，其中至少一种氟化烯烃在气相和路易斯酸催化剂存在下与甲基氟反应形成至少一种具有至少3个碳原子的产物。

76. 发明申请

US20080108854A1 Catalyst promoters for producing trifluoroiodomethane and pentafluoroiodoethane 有权
标题翻译：用于生产三氟碘甲烷和五氟碘乙烷的催化剂促进剂
公开(公告)号：US20080108854A1
公开(公告)日：2008-05-08
申请号：US11901672
申请日：2007-09-18
申请人： Shuwu Yang , Hsueh Sung Tung
发明人： Shuwu Yang , Hsueh Sung Tung
IPC分类号： C07C17/00 , C07C19/08
CPC分类号： C07C19/16 , B01J23/04 , B01J23/06 , B01J23/10 , B01J23/22 , B01J23/24 , B01J23/78 , C07C17/093 , C07C17/10 , C07C17/158 , C07C17/204 , C09K5/044
摘要： The present invention provides a process for the preparation of a fluoroiodoalkane compound represented by the formula CF3(CF2)n—I, wherein n is 0 or 1. The process includes the step of contacting: (i) a compound represented by the formula CF3(CF2)n—Y, wherein Y is selected from H, Cl, Br, and COOH and n is 0 or 1; (ii) a source of iodine; (iii) an alkali or alkaline earth metal salt catalyst supported on a carrier; and (iv) a catalyst promoter for the alkali or alkaline earth metal salt catalyst. The catalyst promoter includes at least one element selected from a transition metal element, a rare earth metal element, a main group element other than the alkali or alkaline earth metal element, any salts thereof, and any combinations thereof. The contacting is carried out at a temperature and pressure and for a length of time sufficient to produce the fluoroiodoalkane compound. The contacting may be carried out in the presence or absence of a solvent and in the presence or absence of oxygen.
摘要翻译：本发明提供一种制备由式CF 3（CF 2）n I-I表示的氟代碘代烷烃化合物的方法，其中n 该方法包括使以下步骤：（i）由式CF 3（CF 2）n表示的化合物 -Y，其中Y选自H，Cl，Br和COOH，n为0或1; （ii）碘源; （iii）负载在载体上的碱金属或碱土金属盐催化剂; 和（iv）碱金属或碱土金属盐催化剂的催化剂促进剂。催化剂促进剂包括选自过渡金属元素，稀土金属元素，除碱金属或碱土金属元素以外的主要基团的元素中的至少一种元素，它们的任何盐及其任何组合。接触在温度和压力下进行足够长的时间以产生氟代碘代烷烃化合物。接触可以在存在或不存在溶剂的情况下以及在存在或不存在氧的情况下进行。

77. 发明申请

US20070129579A1 Processes for selective dehydrohalogenation of halogenated alkanes 有权
标题翻译：用于卤代烷烃选择性脱卤化氢的方法
公开(公告)号：US20070129579A1
公开(公告)日：2007-06-07
申请号：US11588465
申请日：2006-10-27
申请人： Haiyou Wang , Hsueh Sung Tung
发明人： Haiyou Wang , Hsueh Sung Tung
IPC分类号： C07C21/18
CPC分类号： C07C17/206 , C07C17/25 , C07C19/08 , C07C21/18
摘要： Disclosed are processes for producing halogenated olefins, and preferably tetrafluorinated propene(s), from one or more alkanes having both fluorine substituents and non-fluorine substituents, preferably with a high degree of conversion and selectivity. Preferably the process comprises the use of a catalyzed reaction in which the catalyst is selected from the group consisting of activated carbons, halogentated mono- and di-valent metal oxides, mono- and di-valent Lewis acid metal halides, zero-valent metals, and combinations of these.
摘要翻译：公开了一种或多种具有氟取代基和非氟取代基的烷烃的卤代烯烃，优选四氟化丙烯的制备方法，优选具有高转化率和选择性。优选地，该方法包括使用催化反应，其中催化剂选自活性炭，卤化一价和二价金属氧化物，一价和二价路易斯酸金属卤化物，零价金属，以及这些的组合。

78. 发明授权

US07071367B1 Direct one-step synthesis of CF3-I 失效
标题翻译：直接一步合成CF3-I
公开(公告)号：US07071367B1
公开(公告)日：2006-07-04
申请号：US11007919
申请日：2004-12-09
申请人： Sudip Mukhopadhyay , Hsueh Sung Tung
发明人： Sudip Mukhopadhyay , Hsueh Sung Tung
IPC分类号： C07C17/00
CPC分类号： C07C17/093 , C07C17/158 , C07C17/204 , C07C19/16
摘要： The present invention provides a process for the preparation of trifluoromethyl iodide. The process includes the step of: contacting in a reactor a compound represented by the formula: CF3—W and a compound represented by the formula: Z-I wherein W is selected from CF3, hydrogen and bromine; Z is selected from hydrogen, iodine and chlorine. The step of contacting is carried out, optionally in the presence of a catalyst and further optionally in the presence of air, at a temperature, pressure and for a length of time sufficient to produce the trifluoromethyl iodide.
摘要翻译：本发明提供了制备三氟甲基碘的方法。该方法包括以下步骤：在反应器中接触由下式表示的化合物：<？in-line-formula description =“In-line Formulas”end =“lead”？> CF 3 - W <？in-line-formula description =“In-line Formulas”end =“tail”？>和由以下公式表示的化合物：<？in-line-formula description =“In-line Formulas”end =“lead “？”ZI <？in-line-formula description =“In-line Formulas”end =“tail”？>其中W选自CF 3，氢和溴; Z选自氢，碘和氯。任选地在催化剂存在下进一步任选地在空气存在下，在足以产生三氟甲基碘的温度，压力和一段时间内进行接触步骤。

79. 发明授权

US06787678B1 Method of removing water from hydrofluorocarbon manufacturing processes 失效
标题翻译：从氢氟碳化物制造工艺中去除水的方法
公开(公告)号：US06787678B1
公开(公告)日：2004-09-07
申请号：US10733036
申请日：2003-12-11
申请人： Hsueh Sung Tung , Jason T. Stuck
发明人： Hsueh Sung Tung , Jason T. Stuck
IPC分类号： C07C1738
CPC分类号： C07B39/00 , C07C17/38 , Y02P20/582
摘要： Disclosed are improved fluorination processes and fluorine-containing compositions which involve introducing to one or more fluorination process compositions a water reactive agent in an amount and under conditions effective to decrease the amount of water in that composition. The water reactive agent is preferably introduced to the fluorination process at a location downstream of the fluorination reaction, in amounts and under conditions effective to produce a relatively lower concentration of water in the composition, and preferably throughout the fluorination process.
摘要翻译：公开了改进的氟化方法和含氟组合物，其涉及在有效降低该组合物中的水量的量和条件下向一种或多种氟化方法组合物引入水反应剂。水反应剂优选在氟化反应的下游位置以有效地在组合物中产生相对较低浓度的水，并且优选在整个氟化过程中的量和条件下引入氟化过程。

80. 发明授权

US06702929B2 Purification of 1,1,1,3,3-pentafluorobutane 有权
标题翻译： 1,1,1,3,3-五氟丁烷的纯化
公开(公告)号：US06702929B2
公开(公告)日：2004-03-09
申请号：US10337836
申请日：2003-01-07
申请人： Stephen Frederic Yates , Hsueh Sung Tung
发明人： Stephen Frederic Yates , Hsueh Sung Tung
IPC分类号： C07C1700
CPC分类号： C07C17/395 , C07C19/08
摘要： In the synthesis of 1,1,1,3,3-pentafluorobutane (R-365mfc), a mixture of R-365mfc and the impurity 1,1,1,3-tetrafluoro-2-butene (R-1354mzy) is purified and R-1354mzy is removed from the mixture by contacting the mixture with 1-5 mols of chlorine for each mol of R-1354mzy in the presence of ultraviolet light having a wavelength between about 300 to 400 nm which provides at least 0.02 watts-hour/kg of the mixture. The R-1354mzy is reduced to below 10 wt. ppm as it is converted to 2,3-dichloro-1,1,1,3-tetrafluorobutane (R-354) or other butane containing more chlorine and having a higher boiling point than R-365mfc. The butane(s) may be separated more easily from R-365mfc. The photochlorination is effected in a manner such that at least about 96 weight percent of the starting amount of R-365mfc is maintained in the mixture.
摘要翻译：在1,1,1,3,3-五氟丁烷（R-365mfc）的合成中，纯化R-365mfc和杂质1,1,1,3-四氟-2-丁烯（R-1354mzy）的混合物并且在波长在约300至400nm之间的紫外光存在下，将混合物与1-5摩尔氯接触，每摩尔R-1354毫摩尔，从混合物中除去R-1354mzy，该紫外线提供至少0.02瓦时 / kg混合物。将R-1354mzy还原成低于10wt。 ppm，因为它被转化为2,3-二氯-1,1,1,3-四氟丁烷（R-354）或其它含有更多氯且沸点高于R-365mfc的丁烷。丁烷可能更容易从R-365mfc分离出来。光氯化以这样的方式进行，使得至少约96重量％的起始量的R-365mfc保持在混合物中。

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