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71. 发明授权

US4480646A Branched chain olefinic alcohols, thiols, esters and ethers, organoleptic uses thereof, processes for preparing same and intermediates therefor 失效
公开(公告)号：US4480646A
公开(公告)日：1984-11-06
申请号：US329223
申请日：1981-12-10
申请人： Richard M. Boden
发明人： Richard M. Boden
IPC分类号： A23L27/20 , A24B15/32 , C11B9/00 , C11D1/24 , C11D3/395 , A24B3/12 , A24B15/30
CPC分类号： A24B15/32 , A23L27/202 , C11B9/0007 , C11D1/24 , C11D3/3956
摘要： Described are compounds defined according to the structure: ##STR1## taken alone or in admixture wherein one of the dashed lines is a carbon-carbon double bond and each of the other of the dashed lines are carbon-carbon single bonds; wherein R.sub.1 represents C.sub.1 -C.sub.4 alkyl; R.sub.2 represents C.sub.1 -C.sub.4 alkyl; Z represents oxygen or sulfur; R.sub.3 represents hydrogen, MgX, Li, C.sub.1 -C.sub.3 lower alkyl or C.sub.1 -C.sub.3 lower acyl; and wherein X represents chloro, bromo or iodo and uses thereof in augmenting or enhancing the aroma and/or taste of consumable materials such as perfume compositions, colognes, perfumed articles, e.g., solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions or dryer-added fabric softener articles, smoking tobaccos, chewing gums, chewing tobaccos, medicinal products or toothpastes. Also described are processes for preparing such compounds hereinafter described as branched chain olefinic alcohols, thiols, esters and ethers.

72. 发明授权

US4480136A Norbornyl oxyacetaldehyde, organoleptic uses thereof and process for preparing same 失效
标题翻译：降冰片基氧乙醛，感官用途及其制备方法
公开(公告)号：US4480136A
公开(公告)日：1984-10-30
申请号：US456984
申请日：1983-01-10
申请人： Robert P. Belko , Richard M. Boden , Marie R. Hanna
发明人： Robert P. Belko , Richard M. Boden , Marie R. Hanna
IPC分类号： C07C45/38 , C07C47/198 , C11B9/00 , C11D3/50 , C07C47/115
CPC分类号： C11D3/50 , C07C45/38 , C07C47/198 , C11B9/0046 , C07C2102/42 , Y02P20/582
摘要： Described is a compound having the structure: ##STR1## a norbornyl oxyacetaldehyde, prepared by oxidizing the norbornyl oxyethanol compound having the structure: ##STR2## using air or oxygen and a silver or copper chromite catalyst; and organoleptic uses of such oxidation product in the field of perfumery, colognes and perfumed articles (e.g. perfumed plastics, solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions or drier-added fabric softener articles).
摘要翻译：描述了具有以下结构的化合物：通过使用空气或氧气和银或亚铬酸铜催化剂氧化具有以下结构的降冰片基氧基乙醇化合物制备的降冰片基氧乙醛：以及在香料，古龙水和香水制品（例如加香塑料，固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物或干燥剂添加的织物柔软剂制品）领域中的这种氧化产物的感官用途。

73. 发明授权

US4474992A 2-Isopropenyl-1,5-dimethyl-cyclopentane carboxaldehyde, organoleptic uses thereof and process for preparing same 失效
标题翻译： 2-异丙烯基-1,5-二甲基 - 环戊烷甲醛，其感官用途及其制备方法
公开(公告)号：US4474992A
公开(公告)日：1984-10-02
申请号：US474018
申请日：1983-03-10
申请人： Michael Licciardello , Richard M. Boden
发明人： Michael Licciardello , Richard M. Boden
IPC分类号： C07C45/67 , C07C47/45 , C11B9/00 , C11D3/50
CPC分类号： C11D3/50 , C07C45/67 , C07C47/45 , C11B9/003
摘要： Described is 2-isopropenyl-1,5-dimethyl-cyclopentane carboxaldehyde of our invention having the structure: ##STR1## and uses thereof for augmenting or enhancing the aroma of perfumes, colognes and perfumed articles including solid or liquid anionic, cationic, nonionic or zwitterionic detergents, perfumed polymers, fabric softener compositions, fabric softener articles including drier-added fabric softener articles, hair preparations, cosmetic powders, face creams, moisturizers and the like. Also described is a process for preparing 2-isopropenyl-1,5-dimethyl-cyclopentane carboxaldehyde of our invention according to the reaction: ##STR2##
摘要翻译：描述了本发明的2-异丙烯基-1,5-二甲基 - 环戊烷甲醛，其具有以下结构：其用于增强或增强香料，古龙水和加香制品的香气，包括固体或液体阴离子，阳离子，非离子或非离子的两性离子洗涤剂，加香聚合物，织物柔软剂组合物，织物柔软剂制品，包括干燥添加的织物柔软剂制品，头发制剂，化妆粉，面霜，保湿剂等。还描述了根据以下反应制备本发明的2-异丙烯基-1,5-二甲基 - 环戊烷甲醛的方法：

74. 发明授权

US4465863A Branched C.sub.13 -alk-1-en-5-ones, use thereof in perfumery, process for preparing same and intermediates used in said process 失效
标题翻译：支链C13-烷-1-烯-5-酮，其在香料中的应用，其制备方法和所述方法中使用的中间体
公开(公告)号：US4465863A
公开(公告)日：1984-08-14
申请号：US441375
申请日：1982-11-12
申请人： Richard M. Boden , Steven D. Temes , Theodore J. Tyszkiewicz , Marie R. Hanna
发明人： Richard M. Boden , Steven D. Temes , Theodore J. Tyszkiewicz , Marie R. Hanna
IPC分类号： C07C29/48 , C07C45/28 , C07C45/45 , C07C45/68 , C07C49/04 , C07C49/203 , C07D303/04 , C11B9/00
CPC分类号： C11B9/0015 , C07C29/48 , C07C45/28 , C07C45/455 , C07C45/68 , C07C49/04 , C07C49/203 , C07D303/04
摘要： Described are compounds defined according to the structure: ##STR1## wherein R.sub.3, R.sub.4, R.sub.5, R.sub.6 and R.sub.7 represent hydrogen or methyl with the provisos that:(i) the sum total of carbon atoms in R.sub.3, R.sub.4, R.sub.5, R.sub.6 and R.sub.7 is three;(ii) when R.sub.7 is methyl, then R.sub.5 and R.sub.6 are both methyl, and(iii) when either R.sub.3 or R.sub.4 is methyl, then R.sub.7 is hydrogenand wherein R.sub.8 represents hydrogen, acetyl, alkoxyacyl, hydroxyacyl, or alkali metal carboxylate; and R.sub.9 is hydrogen or allyl with the additional proviso that R.sub.8 and R.sub.9 are not both hydrogen.Also described is the use of the subgenus of such compounds defined according to the structure: ##STR2## in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles including solid or liquid nonionic, cationic, anionic or zwitterionic detergents, fabric softener compositions, fabric softener articles, cosmetic powders, hair preparations and the like.
摘要翻译：描述了根据以下结构定义的化合物：其中R 3，R 4，R 5，R 6和R 7表示氢或甲基，条件是：（i）R 3，R 4，R 5，R 6和R 7中的碳原子总和是三（ii）当R 7为甲基时，R 5和R 6均为甲基，（iii）当R 3或R 4为甲基时，R 7为氢，R 8为氢，乙酰基，烷氧基酰基，羟基酰基或碱金属羧酸盐; 并且R 9是氢或烯丙基，另外条件是R 8和R 9不都是氢。还描述了根据以下结构定义的这种化合物亚类的用途：在增加或增强香料组合物，古龙水和加香制品的芳香物质中包括固体或液体非离子，阳离子，阴离子或两性离子洗涤剂，织物柔软剂组合物织物柔软剂制品，化妆粉，头发制剂等。

75. 发明授权

US4464280A Organoleptic uses of phenyl ethyl methyl carbonate mixtures 失效
标题翻译：感官使用苯基乙基甲基碳酸酯混合物
公开(公告)号：US4464280A
公开(公告)日：1984-08-07
申请号：US546390
申请日：1983-10-28
申请人： Richard M. Boden , Theodore J. Tyszkiewicz , Hugh Watkins
发明人： Richard M. Boden , Theodore J. Tyszkiewicz , Hugh Watkins
IPC分类号： C11B9/00 , C11D17/00
CPC分类号： C11B9/0061
摘要： Described is phenylethyl methylcarbonate having the structure: ##STR1## mixtures of same with 3-methyl-1-phenyl-pentenol-5 and/or one or more butanoyl cyclohexane derivative as well as processes and compositions for the use in perfume aroma augmenting, modifying, altering and enhancing compositions and as perfume, cologne and perfumed article aroma imparting materials of said phenylethyl methylcarbonate and mixtures thereof with 3-methyl-1-phenyl-pentenol-5 and/or one or more butanoyl cyclohexane derivatives.
摘要翻译：描述了具有以下结构的苯乙基甲基碳酸酯：其与3-甲基-1-苯基 - 戊烯醇-5和/或一种或多种丁酰基环己烷衍生物的混合物以及用于香料香气增强，改性的方法和组合物改变和增强组合物以及所述苯甲基碳酸苯乙酯及其与3-甲基-1-苯基 - 戊烯醇-5和/或一种或多种丁酰基环己烷衍生物的混合物的香料，科隆和香料制品香气赋予材料。

76. 发明授权

US4454111A Prenyl methyl carbonate and organoleptic uses thereof 失效
标题翻译：碳酸甲酯和其感官用途
公开(公告)号：US4454111A
公开(公告)日：1984-06-12
申请号：US528545
申请日：1983-09-01
申请人： Richard M. Boden , Manfred H. Vock , Theodore J. Tyszkiewicz
发明人： Richard M. Boden , Manfred H. Vock , Theodore J. Tyszkiewicz
IPC分类号： A23L27/20 , A61K7/16 , A61K7/26 , A61K9/68
CPC分类号： A23L27/2052 , A23L27/202
摘要： Processes and compositions are described for use in foodstuff, chewing gum, toothpaste and medicinal product flavor and aroma augmenting, modifying, enhancing and imparting compositions and as foodstuffs, chewing gums, toothpastes and medicinal product aroma imparting materials of prenyl methyl carbonate defined according to the structure: ##STR1## Also described are uses of said prenyl methyl carbonate in conjunction with cyclic acetals of 2-methyl-2-pentenal defined according to the structures: ##STR2##
摘要翻译：方法和组合物描述用于食品，口香糖，牙膏和药用产品香料和香气增强，改性，增强和赋予组合物，并且作为食品，口香糖，牙膏和根据本发明限定的限制的甲基丙烯酸甲酯的药用产品香气赋予材料结构：还描述了所述甲基丙烯酸甲酯与2-甲基-2-戊烯醛的环状缩醛的结合的用途，所述2-甲基-2-戊烯醛根据以下结构定义：

77. 发明授权

US4447365A 2-Ethyl hexyl and isobornyl methyl carbonates 失效
标题翻译： 2-乙基己基和异冰片基碳酸甲酯
公开(公告)号：US4447365A
公开(公告)日：1984-05-08
申请号：US458964
申请日：1983-01-18
申请人： Richard M. Boden , Michael Licciardello , Theodore J. Tyszkiewicz
发明人： Richard M. Boden , Michael Licciardello , Theodore J. Tyszkiewicz
IPC分类号： C11B9/00 , C07C69/96 , A61K7/46
CPC分类号： C11B9/0046 , C11B9/0015 , C11B9/0061
摘要： Described are the alkyl and bicycloalkyl methyl carbonates defined according to the structure: ##STR1## wherein R represents 2-ethyl hexyl, having the structure: ##STR2## or isobornyl having the structure: ##STR3## and uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles.
摘要翻译：描述了根据以下结构定义的烷基和双环烷基甲基碳酸酯：其中R表示2-乙基己基，具有以下结构的结构：具有以下结构的结构：其具有以下结构：其用于增强或增强香气的香水组合物，古龙水和香水制品。

78. 发明授权

US4440961A Branched chain olefinic alcohols, thiols, esters and ethers, organoleptic uses thereof, processes for preparing same and intermediates therefor 失效
标题翻译：支链烯烃，硫醇，酯和醚，其感官用途，制备方法及其中间体
公开(公告)号：US4440961A
公开(公告)日：1984-04-03
申请号：US422525
申请日：1982-09-23
申请人： Richard M. Boden
发明人： Richard M. Boden
IPC分类号： C07C2/28 , C07C29/40 , C07C29/68 , C07C33/025 , C07C33/03 , C07C45/46 , C11B9/00 , C11D3/50 , C07C69/007 , C07C149/08 , C07C153/09
CPC分类号： C11D3/50 , C07C2/28 , C07C29/40 , C07C29/68 , C07C33/025 , C07C33/03 , C07C45/46 , C11B9/0015 , C07C2531/06 , C07C2531/10
摘要： Described are compounds defined according to the structure: ##STR1## taken alone or in admixture wherein one of the dashed lines is a carbon-carbon double bond and each of the other of the dashed lines are carbon-carbon single bonds; wherein R.sub.1 represents C.sub.1 -C.sub.4 alkyl; R.sub.2 represents C.sub.1 -C.sub.4 alkyl; Z represents oxygen or sulfur; R.sub.3 represents hydrogen, MgX, Li, C.sub.1 -C.sub.3 lower alkyl or C.sub.1 -C.sub.3 lower acyl; and wherein X represents chloro, bromo or iodo and uses thereof in augmenting or enhancing the aroma and/or taste of consumable materials such as perfume compositions, colognes, perfumed articles, e.g., solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions or dryer-added fabric softener articles, smoking tobaccos, chewing gums, chewing tobaccos, medicinal products or toothpastes. Also described are processes for preparing such compounds hereinafter described as branched chain olefinic alcohols, thiols, esters and ethers.
摘要翻译：描述的是根据以下结构定义的化合物：单独使用或混合物，其中虚线之一是碳 - 碳双键，另一个虚线中的每一个都是碳 - 碳单键; 其中R1表示C1-C4烷基; R2代表C1-C4烷基; Z表示氧或硫; R3表示氢，MgX，Li，C1-C3低级烷基或C1-C3低级酰基; 并且其中X表示氯，溴或碘，并且其用途用于增强或增强消耗材料的香气和/或味道，例如香料组合物，古龙水，加香制品，例如固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物软化剂组合物或干燥剂添加的织物柔软剂制品，吸烟烟草，口香糖，咀嚼烟草，药用产品或牙膏。还描述了制备这种化合物的方法，其在下文中描述为支链烯烃，硫醇，酯和醚。

79. 发明授权

US4425264A Branched chain ketones used in augmenting or enhancing the aroma of perfumes, colognes and perfumed articles and the like process for preparing same 失效
标题翻译：用于增加或增强香水，古龙水和香水制品香气的分支链酮及其制备方法
公开(公告)号：US4425264A
公开(公告)日：1984-01-10
申请号：US384962
申请日：1982-06-04
申请人： Richard M. Boden , Theodore J. Tyszkiewicz
发明人： Richard M. Boden , Theodore J. Tyszkiewicz
IPC分类号： C07C45/46 , C07C49/04 , C11B9/00 , A61K7/46
CPC分类号： C11B9/0007 , C07C45/46 , C07C49/04
摘要： Described are acylated derivatives of triisobutylene defined according to the generic structures: ##STR1## wherein, in each of the molecules one of the dashed lines represents a carbon-carbon double bond and each of the other of the dashed lines represents a carbon-carbon single bond; and wherein, in each of the molecules R.sub.3 represents methyl or ethyl; uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles (e.g., solid or liquid anionic, cationic, nonionic, zwitterionic detergents, cosmetic powders, hair sprays and the like) as well as processes for preparing same by first trimerizing isobutylene to form one or more compounds defined according to at least one of the structures: ##STR2## wherein in each of the molecules one of the dashed lines represents a carbon-carbon double bond and each of the other dashed lines represent carbon-carbon single bonds; and then reacting one or more of these trimerized isobutylene derivatives with an acyl anhydride having the structure: ##STR3## wherein, R.sub.1 and R.sub.2 are the same or different and each represents methyl or ethyl in the presence of a Lewis acid catalyst such as boron trifluoride etherate or stannic chloride thereby forming the acylated branched chain ketones of our invention defined according to at least one of the structures: ##STR4##
摘要翻译：描述了根据通用结构定义的三异丁烯的酰化衍生物：其中，在每个分子中，虚线之一表示碳 - 碳双键，并且每个虚线表示碳 - 碳单键; 并且其中，在每个分子中，R 3表示甲基或乙基; 用于增强或增强香水组合物，古龙水和香料制品（例如固体或液体阴离子，阳离子，非离子，两性离子洗涤剂，化妆品粉末，喷发剂等）的香气以及通过首先三聚制备方法异丁烯以形成根据以下结构中的至少一个所定义的一种或多种化合物：其中在每个分子中，虚线之一表示碳 - 碳双键，并且每个其它虚线代表碳 - 碳单键; 然后将这些三聚异丁烯衍生物中的一种或多种与具有以下结构的酰基酸反应：其中，在路易斯酸催化剂如三氟化硼存在下，R 1和R 2相同或不同，各自表示甲基或乙基乙醚化物或氯化锡，从而形成我们发明的酰化支链酮，其根据以下结构中的至少一个限定： + TR

80. 发明授权

US4421679A Methyl substituted-2-oxohexane derivatives and processes for preparing and using same 失效
公开(公告)号：US4421679A
公开(公告)日：1983-12-20
申请号：US345665
申请日：1982-02-04
申请人： Richard M. Boden , Lambert Dekker , Frederick L. Schmitt , Augustinus G. Van Loveren
发明人： Richard M. Boden , Lambert Dekker , Frederick L. Schmitt , Augustinus G. Van Loveren
IPC分类号： C11B9/00 , C11D1/24 , C11D3/395 , C11D3/50 , A61K7/46
CPC分类号： C11D3/50 , C11B9/0007 , C11D1/24 , C11D3/3956
摘要： Described are methods for augmenting or enhancing the aroma of perfumes and perfumed articles by adding thereto perfume aroma augmenting or enhancing quantities of novel methyl substituted-2-oxohexane derivatives produced by dimerizing isoamylene (2-methyl-2-butene) and then oxidizing the resulting product using formic acid and hydrogen peroxide; and optionally reacting the resulting product with a methyl Grignard reagent such as methyl magnesium chloride followed by hydrolysis; as well as perfume compositions, colognes and perfumed articles including solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, hair preparations, perfumed polymers and deodorant compositions as well as bleaching compositions containing same.Also covered is the genus of compounds defined according to the structure: ##STR1## wherein R.sub.1 and R.sub.2 taken together represent oxygen; or wherein, taken separately, R.sub.1 is hydroxyl and R.sub.2 is methyl or R.sub.1 is oxymagnesium halide and R.sub.2 is methyl; and wherein R.sub.3, R.sub.4, R.sub.5, R.sub.6 and R.sub.7 represent hydrogen or methyl with the provisos that:(i) the sum total of carbon atoms in R.sub.3, R.sub.4, R.sub.5, R.sub.6 and R.sub.7 is three;(ii) when R.sub.7 is methyl, then R.sub.5 and R.sub.6 are both methyl, and(iii) when either R.sub.3 or R.sub.4 is methyl, then R.sub.7 is hydrogen.

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