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71. 发明授权

US08202962B2 Integrated steam heating in polyester production process 有权
标题翻译：在聚酯生产过程中集成蒸汽加热
公开(公告)号：US08202962B2
公开(公告)日：2012-06-19
申请号：US12558020
申请日：2009-09-11
申请人： Alan George Wonders , James Donald Simpson , Bruce Roger DeBruin
发明人： Alan George Wonders , James Donald Simpson , Bruce Roger DeBruin
IPC分类号： C08G63/02 , C08G63/00
CPC分类号： C08G63/78 , Y02P20/125
摘要： Processes for making polyesters in a polyester production facility are disclosed, that include the steps of: forming a reaction medium comprising at least one monomer that includes terephthalic acid (TPA) and/or an ester derivative of TPA; subjecting at least a portion of the reaction medium to one or more chemical reactions in the polyester production facility to thereby produce the polyester; heating at least a portion of the reaction medium via indirect heat exchange with high-pressure steam, wherein the heating causes at least a portion of the high-pressure steam to condense and thereby provide pressurized condensed water; flashing at least a portion of the pressurized condensed water to thereby produce lower-pressure steam; and heating one or more process fluid streams of the polyester production facility via indirect heat exchange with at least a portion of the lower-pressure steam, wherein the process fluid streams include any stream that is formed predominately of the reaction medium and/or the at least one monomer.
摘要翻译：公开了在聚酯生产设备中制备聚酯的方法，其包括以下步骤：形成包含至少一种包含对苯二甲酸（TPA）和/或TPA的酯衍生物的单体的反应介质; 使至少一部分反应介质在聚酯制造设备中进行一次或多次化学反应，从而制造聚酯; 通过与高压蒸汽的间接热交换来加热至少一部分反应介质，其中加热使至少一部分高压蒸汽冷凝，从而提供加压的冷凝水; 闪烁至少一部分加压冷凝水，从而产生低压蒸汽; 以及通过与所述低压蒸汽的至少一部分的间接热交换来加热所述聚酯生产设备的一个或多个过程流体流，其中所述过程流体流包括主要由所述反应介质和/或所述反应介质形成的任何流至少一种单体。

72. 发明授权

US08198397B2 Integrated steam heating in polyester production process 有权
标题翻译：在聚酯生产过程中集成蒸汽加热
公开(公告)号：US08198397B2
公开(公告)日：2012-06-12
申请号：US12558003
申请日：2009-09-11
申请人： Alan George Wonders , James Donald Simpson , Bruce Roger DeBruin
发明人： Alan George Wonders , James Donald Simpson , Bruce Roger DeBruin
IPC分类号： C08G64/00 , C08G63/02
CPC分类号： C08G63/78 , Y02P20/125
摘要： Integrated processes for making polyesters are disclosed, that include the steps of: (a) producing an aromatic polycarboxylic acid in a monomer production facility; (b) producing a polyester in a polyester production facility, wherein the producing of the polyester comprises the substeps of: (i) forming a polyester reaction medium comprising at least a portion of the aromatic polycarboxylic acid from the monomer production facility, (ii) subjecting at least a portion of the polyester reaction medium to one or more chemical reactions to thereby produce the polyester, (iii) heating the polyester reaction medium at one or more locations in the polyester production facility via indirect heat exchange with high-pressure steam, wherein the heating causes at least a portion of the high-pressure steam to condense and thereby provide pressurized condensed water, and (iv) flashing at least a portion of the pressurized condensed water to thereby produce lower-pressure steam; and (c) using at least a portion of the lower-pressure steam to provide thermal energy to the monomer production facility.
摘要翻译：公开了制造聚酯的综合方法，包括以下步骤：（a）在单体生产设备中制备芳族多元羧酸; （b）在聚酯制造设备中制造聚酯，其中聚酯的制造包括以下子步骤：（i）从单体生产设备形成包含至少一部分芳族多元羧酸的聚酯反应介质，（ii）使聚酯反应介质的至少一部分进行一个或多个化学反应从而生产聚酯，（iii）通过与高压蒸汽的间接热交换在聚酯生产设备中的一个或多个位置处加热聚酯反应介质，其中所述加热使得所述高压蒸汽的至少一部分冷凝，从而提供加压的冷凝水，和（iv）使加压冷凝水的至少一部分闪蒸，从而产生低压蒸汽; 和（c）使用至少一部分低压蒸汽来向单体生产设备提供热能。

73. 发明授权

US08178054B2 Optimized liquid-phase oxidation 有权
公开(公告)号：US08178054B2
公开(公告)日：2012-05-15
申请号：US12702725
申请日：2010-02-09
申请人： Alan George Wonders , Lee Reynolds Partin , Wayne Scott Strasser , Marcel de Vreede
发明人： Alan George Wonders , Lee Reynolds Partin , Wayne Scott Strasser , Marcel de Vreede
IPC分类号： B01J19/24 , B01J19/00 , B01J19/18
CPC分类号： B01J19/1881 , B01J4/002 , B01J10/002 , B01J19/1806 , B01J19/1862 , B01J19/1875 , B01J19/2405 , B01J19/245 , B01J19/246 , B01J19/2465 , B01J19/26 , B01J2219/00006 , B01J2219/0004 , B01J2219/00105 , B01J2219/00182 , B01J2219/00186 , C07C51/265 , C07C63/26
摘要： Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.

74. 发明申请

US20110190536A1 Oxidation System with Sidedraw Secondary Reactor 有权
标题翻译： Sidedraw二次反应器氧化系统
公开(公告)号：US20110190536A1
公开(公告)日：2011-08-04
申请号：US12957730
申请日：2010-12-01
申请人： Ashfaq Shaikh , Alan George Wonders , David Lange
发明人： Ashfaq Shaikh , Alan George Wonders , David Lange
IPC分类号： C07C51/265 , B01J8/00
CPC分类号： B01J8/228 , B01J8/22 , B01J10/00 , B01J2208/00274 , B01J2208/003 , C07C51/265 , C07C63/26
摘要： Disclosed are process and apparatus for vertical splitting of the oxygen supply to a post-oxidation reactor. Further disclosed are process and apparatus for supplying reaction medium to a post-oxidation reactor at a mid-level inlet. Such apparatus and process can assist in reducing oxygen pinch throughout the post-oxidation reactor.
摘要翻译：公开了用于将氧气供应垂直分离到后氧化反应器的方法和装置。还公开了用于在中级入口向后氧化反应器供应反应介质的方法和装置。这种设备和方法可以帮助减少整个后氧化反应器中的氧气。

75. 发明授权

US07868125B2 Production of non-solid-stated polyester particles having solid-stated properties 有权
标题翻译：制备具有固体特性的非固体聚酯颗粒
公开(公告)号：US07868125B2
公开(公告)日：2011-01-11
申请号：US12394478
申请日：2009-02-27
申请人： Bruce Roger DeBruin , Tommy Ray Maddox, II , John Alan Wabshall, Jr. , Steven Lee Stafford , Stephen Weinhold , Robert Noah Estep , Mary Therese Jernigan , Steven Paul Bellner , Alan George Wonders , John Guy Franjione
发明人： Bruce Roger DeBruin , Tommy Ray Maddox, II , John Alan Wabshall, Jr. , Steven Lee Stafford , Stephen Weinhold , Robert Noah Estep , Mary Therese Jernigan , Steven Paul Bellner , Alan George Wonders , John Guy Franjione
IPC分类号： C08G63/02 , C08G63/00
CPC分类号： C08G63/90 , B29B9/065 , B29B9/12 , B29B9/16 , B29B2009/165 , C08J3/122 , C08J2367/02 , F26B5/08 , F26B17/24 , Y10T428/2998
摘要： A process for producing non-solid-stated polyester polymer particles having one or more properties similar to polyester polymer particles that have undergone solid-state processing. In one embodiment, the process comprises (a) forming polyester polymer particles from a polyester polymer melt; (b) quenching at least a portion of the particles, (c) drying at least a portion of the particles, (d) crystallizing at least a portion of the particles, (e) annealing at least a portion of the particles. At all points during and between steps (b) through (e), the average bulk temperature of the particles is maintained above 165° C.
摘要翻译：一种制备具有与经过固态加工的聚酯聚合物颗粒相似的一种或多种性能的非固体聚酯聚合物颗粒的方法。在一个实施方案中，该方法包括（a）从聚酯聚合物熔体形成聚酯聚合物颗粒; （b）淬灭至少一部分颗粒，（c）干燥至少一部分颗粒，（d）使至少一部分颗粒结晶，（e）退火至少一部分颗粒。在步骤（b）至（e）期间和之间的所有点，颗粒的平均体温保持在165℃以上。

76. 发明授权

US07659427B2 Optimized liquid-phase oxidation 有权
公开(公告)号：US07659427B2
公开(公告)日：2010-02-09
申请号：US12116249
申请日：2008-05-07
申请人： Alan George Wonders , Wayne Scott Strasser , Marcel de Vreede , J. Thomas Tidwell
发明人： Alan George Wonders , Wayne Scott Strasser , Marcel de Vreede , J. Thomas Tidwell
IPC分类号： C07C51/16
CPC分类号： B01J8/22 , B01J4/002 , B01J8/1818 , B01J8/1872 , B01J8/222 , B01J2219/00006 , B01J2219/0004 , B01J2219/00162 , C07C51/265 , C07C63/26
摘要： Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.

77. 发明授权

US07608733B2 Optimized liquid-phase oxidation 有权
公开(公告)号：US07608733B2
公开(公告)日：2009-10-27
申请号：US11154479
申请日：2005-06-16
申请人： Alan George Wonders , Howard Wood Jenkins, Jr. , Lee Reynolds Partin , Wayne Scott Strasser , Marcel de Vreede
发明人： Alan George Wonders , Howard Wood Jenkins, Jr. , Lee Reynolds Partin , Wayne Scott Strasser , Marcel de Vreede
IPC分类号： C07C51/16
CPC分类号： C07C51/265 , C07C63/26
摘要： Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.

78. 发明授权

US07589231B2 Optimized liquid-phase oxidation 失效
公开(公告)号：US07589231B2
公开(公告)日：2009-09-15
申请号：US11153993
申请日：2005-06-16
申请人： Alan George Wonders , Howard Wood Jenkins, Jr. , Lee Reynolds Partin , Wayne Scott Strasser , Marcel de Vreede
发明人： Alan George Wonders , Howard Wood Jenkins, Jr. , Lee Reynolds Partin , Wayne Scott Strasser , Marcel de Vreede
IPC分类号： C07C51/16
CPC分类号： B01J8/226 , B01J8/1818 , B01J8/1872 , B01J8/222 , B01J19/006 , B01J2219/0004 , C07C51/265 , C07C63/26
摘要： Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.

79. 发明申请

US20080242887A1 Optimized liquid-phase oxidation 有权
公开(公告)号：US20080242887A1
公开(公告)日：2008-10-02
申请号：US12116249
申请日：2008-05-07
申请人： Alan George Wonders , Wayne Scott Strasser , Marcel de Vreede , J. Thomas Tidwell
发明人： Alan George Wonders , Wayne Scott Strasser , Marcel de Vreede , J. Thomas Tidwell
IPC分类号： C07C51/215
CPC分类号： B01J8/22 , B01J4/002 , B01J8/1818 , B01J8/1872 , B01J8/222 , B01J2219/00006 , B01J2219/0004 , B01J2219/00162 , C07C51/265 , C07C63/26
摘要： Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.

80. 发明授权

US07381836B2 Optimized liquid-phase oxidation 有权
公开(公告)号：US07381836B2
公开(公告)日：2008-06-03
申请号：US11154165
申请日：2005-06-16
申请人： Alan George Wonders , Lee Reynolds Partin , Wayne Scott Strasser , Marcel de Vreede , Puneet Gupta
发明人： Alan George Wonders , Lee Reynolds Partin , Wayne Scott Strasser , Marcel de Vreede , Puneet Gupta
IPC分类号： C07C51/255
CPC分类号： B01J8/222 , B01J4/002 , B01J8/1818 , B01J8/1872 , B01J19/006 , B01J2219/00006 , B01J2219/0004 , C07C51/265 , C07C63/26
摘要： Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.

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