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61. 发明授权

US06586562B2 Polyhydroxyalkanoate, method for production thereof and microorganisms for use in the same 失效
标题翻译：聚羟基链烷酸酯，其制备方法和用于其的微生物
公开(公告)号：US06586562B2
公开(公告)日：2003-07-01
申请号：US09748205
申请日：2000-12-27
申请人： Tsutomu Honma , Toyoko Kobayashi , Tetsuya Yano , Shin Kobayashi , Takeshi Imamura , Sakae Suda , Takashi Kenmoku
发明人： Tsutomu Honma , Toyoko Kobayashi , Tetsuya Yano , Shin Kobayashi , Takeshi Imamura , Sakae Suda , Takashi Kenmoku
IPC分类号： C08G6306
CPC分类号： C12P7/62 , C08G63/06 , C08G63/6822 , C08G63/6852 , Y10S435/874
摘要： A polyhydroxyalkanoate having a monomer unit composition represented by General Formula (1): AmB(1−m) (1) wherein A is represented by General Formula (2), B is at least one selected from the group consisting of monomer units represented by General Formula (3) or (4), and m has a value of 0.01 or larger and smaller than 1: wherein n has a value of 0 to 10, k has a value of 3 or 5, and R is at least one group selected from the group consisting of groups represented by General Formulae (5) to (7): in Formula (5) R1 is a group selected from the group consisting of a hydrogen atom (H), halogen atoms, —CN, —NO2, —CF3, —C2F5 and —C3F7; and q is an integer selected from 1 to 8; in Formula (6) R2 is a group selected from the group consisting of a hydrogen atom (H), halogen atoms, —CN, —NO2, —CF3, —C2F5 and —C3F7; and r is an integer selected from 1 to 8; in Formula (7) R3 is a group selected from the group consisting of a hydrogen atom (H), halogen atoms, —CN, —NO2, —CF3, —C2F5 and —C3F7; and s is an integer selected from 1 to 8. The efficient production methods are also provided.
摘要翻译：具有由通式（1）表示的单体单元组成的聚羟基链烷酸酯：其中A由通式（2）表示，B为选自由通式（3）或（4）表示的单体单元中的至少一种，，m的值为0.01以上且小于1，其中n为0〜10，k为3或5，R为选自由通式（5）〜（7）中，式（5）中，R 1为选自氢原子（H），卤素原子，-CN，-NO 2，-CF 3，-C 2 F 5和-C 3 F 7的基团。 q为选自1至8的整数; 在式（6）中，R 2是选自氢原子（H），卤素原子，-CN，-NO 2，-CF 3，-C 2 F 5和-C 3 F 7的基团; 并且r是选自1至8的整数; 在式（7）中，R 3是选自氢原子（H），卤素原子，-CN，-NO 2，-CF 3，-C 2 F 5和-C 3 F 7的基团; s是选自1至8的整数。还提供了有效的制备方法。

62. 发明授权

US06872788B2 Production method of polyester containing epoxy group in side chain and production method of crosslinked polymer 失效
标题翻译：侧链中含有环氧基的聚酯的生产方法和交联聚合物的制备方法
公开(公告)号：US06872788B2
公开(公告)日：2005-03-29
申请号：US10427919
申请日：2003-05-02
申请人： Takeshi Imamura , Etsuko Sugawa , Tetsuya Yano , Shin Kobayashi , Tsutomu Honma , Takashi Kenmoku
发明人： Takeshi Imamura , Etsuko Sugawa , Tetsuya Yano , Shin Kobayashi , Tsutomu Honma , Takashi Kenmoku
IPC分类号： C12N1/28 , C12P7/62 , C08F20/00
CPC分类号： C12P7/625 , C12N1/28 , Y10S435/874
摘要： A method is provided which biosynthesizes a PHA having an epoxy group on a side chain with improved physicochemical properties. Specifically, a method of producing a polyester containing an epoxy group in a side chain thereof using alkene as a raw material is provided which comprises the steps of bringing alkene into contact with a microorganism having an ability to uptake alkene and convert it to a polyester and allowing the microorganism to convert the alkene into a polyester containing an epoxy group in a side chain thereof. Further, a method of producing a crosslinked polymer is provided which comprises reacting the polyester obtained by the above mentioned method with a diamine compound.
摘要翻译：提供一种方法，其生物合成具有改善的物理化学性质的侧链上具有环氧基的PHA。具体地说，提供了使用烯烃作为原料在其侧链中制备含有环氧基的聚酯的方法，其包括使烯与具有吸收烯烃的能力并将其转化为聚酯的微生物接触的步骤，以及允许微生物将烯烃转化成其侧链中含有环氧基的聚酯。此外，提供了一种制备交联聚合物的方法，其包括使通过上述方法获得的聚酯与二胺化合物反应。

63. 发明申请

US20050054063A1 Method and apparatus for producing polyhydroxyalkanoate 审中-公开
标题翻译：聚羟基链烷酸酯的制备方法和装置
公开(公告)号：US20050054063A1
公开(公告)日：2005-03-10
申请号：US10940029
申请日：2004-09-14
申请人： Tsutomu Honma , Etsuko Sugawa , Tetsuya Yano , Tsuyoshi Nomoto , Takeshi Imamura , Tomohiro Suzuki , Takashi Kenmoku
发明人： Tsutomu Honma , Etsuko Sugawa , Tetsuya Yano , Tsuyoshi Nomoto , Takeshi Imamura , Tomohiro Suzuki , Takashi Kenmoku
IPC分类号： C08G63/90 , C12M1/00 , C12P7/62 , C12P7/26
CPC分类号： C12P7/625 , C12M47/06
摘要： The present invention provides a method for producing highly purified polyhydroxyalkanoate (PHA) with high yield, by removing cell components other than PHA from cells containing PHA. Moreover, the present invention provides a method for simply removing or reducing chlorine remained in the collected PHA particles, when a treatment with an oxidizing agent containing hypochlorite is performed in the production of PHA as described above. One of the above-described methods comprises a step of treating cells containing polyhydroxyalkanoate with an oxidizing agent containing at least hypochlorite, a step of separating the treated cells into a water-soluble fraction and a water-insoluble fraction, and a step of reducing chlorine remained in the water-insoluble fraction. The step of reducing chlorine may be a step of washing the water-insoluble fraction with a hot water, thiosulfate solution or polar solvent solution containing at least an organic polar solvent in which polyhydroxyalkanoate is insoluble.
摘要翻译：本发明提供了通过从含有PHA的细胞中除去PHA以外的细胞成分而以高产率生产高纯度聚羟基链烷酸酯（PHA）的方法。此外，本发明提供了如上所述在生产PHA中进行含有次氯酸盐的氧化剂的处理时，简单地除去或还原所收集的PHA颗粒中残留的氯的方法。上述方法之一包括用至少含有次氯酸盐的氧化剂处理含有聚羟基链烷酸酯的细胞的步骤，将经处理的细胞分离成水溶性级分和水不溶性级分的步骤以及还原氯保留在水不溶性部分中。还原氯的步骤可以是用至少含有聚羟基链烷酸酯不溶的有机极性溶剂的热水，硫代硫酸盐溶液或极性溶剂溶液洗涤水不溶性部分的步骤。

64. 发明授权

US06861496B2 Polyhydroxyalkonoate and method of producing same, and ω-(2-thienylsulfanyl) alkanoic acid and method of producing same 失效
标题翻译：聚羟基链烷酸酯及其制造方法，ω-（2-噻吩基硫烷基）链烷酸及其制造方法
公开(公告)号：US06861496B2
公开(公告)日：2005-03-01
申请号：US10641090
申请日：2003-08-15
申请人： Takashi Kenmoku , Etsuko Sugawa , Tetsuya Yano , Tsuyoshi Nomoto , Takeshi Imamura , Tomohiro Suzuki , Tsutomu Honma
发明人： Takashi Kenmoku , Etsuko Sugawa , Tetsuya Yano , Tsuyoshi Nomoto , Takeshi Imamura , Tomohiro Suzuki , Tsutomu Honma
IPC分类号： C08G63/60 , C07D333/34 , C08G63/68 , C08G63/688 , C12P7/62 , C12P11/00 , C12R1/38 , C08G63/02
CPC分类号： C12P7/625 , C07D333/34 , C08G63/6882 , C12P11/00 , Y10S435/874 , Y10S435/877
摘要： PHA containing a novel 3-hydroxy-thioalkanoic acid unit having a highly reactive thienyl group in a side chain thereof, and a method of producing the same are provided. Specifically, 5-(2-thienylsulfanyl) valeric acid represented by Chemical Formula [4] below and 6-(2-thienylsulfanyl) hexanoic acid represented by Chemical Formula [5] below are provided. Further, a method of producing PHA, comprising the step of collecting PHA from cells of a microorganism cultured in a medium containing the valeric acid or hexanoic acid, and a novel PHA represented by Chemical Formula [1] below are provided. (n denotes an integer of 1 to 9)
摘要翻译：提供了含有其侧链中具有高反应性噻吩基的新型3-羟基 - 硫代链烷酸单元的PHA及其制备方法。具体地，提供由下述化学式[4]表示的5-（2-噻吩基硫烷基）戊酸和由下述化学式[5]表示的6-（2-噻吩基硫烷基）己酸。此外，提供了一种制备PHA的方法，其包括从含有戊酸或己酸的培养基中培养的微生物的细胞和由下述化学式[1]表示的新型PHA收集PHA的步骤（n表示 1〜9的整数）

65. 发明授权

US06828074B2 Binder resin containing polyhydroxyalkanoate, toner containing the binder resin, and image-forming method and image-forming apparatus which make use of the toner 失效
标题翻译：含有聚羟基链烷酸酯的粘合剂树脂，含有粘合剂树脂的调色剂，以及使用该调色剂的图像形成方法和图像形成装置
公开(公告)号：US06828074B2
公开(公告)日：2004-12-07
申请号：US10133578
申请日：2002-04-29
申请人： Tetsuya Yano , Etsuko Sugawa , Takeshi Imamura , Takashi Kenmoku
发明人： Tetsuya Yano , Etsuko Sugawa , Takeshi Imamura , Takashi Kenmoku
IPC分类号： G03G9087
CPC分类号： C08G63/06 , C12P7/625 , G03G9/08755 , G03G9/08795 , G03G9/08797
摘要： A polyhydroxyalkanoate (PHA) comprised of two kinds of units, a 3-hydroxybutyrate (3HB) unit and a 3-hydroxyhexanoate (3HHx) unit is used as a binder resin. This provides a binder resin which is biodegradable and can more highly contribute to the conservation of natural environment.
摘要翻译：使用由两种单元组成的聚羟基链烷酸酯（PHA），3-羟基丁酸酯（3HB）单元和3-羟基己酸酯（3HHx）单元作为粘合剂树脂。这提供了可生物降解的粘合剂树脂，并且可以更有效地保护自然环境。

66. 发明授权

US06808854B2 POLYHYDROXYALKANOATES HAVING IN ITS SIDE CHAIN PHENYLSULFINYL STRUCTURE AND/OR PHENYL SULFONYL STRUCTURE AND PRODUCTION PROCESS THEREFOR; CHARGE CONTROL AGENT, TONER BINDER AND TONER CONTAINING SAME; AND IMAGE FORMING METHOD AND IMAGE FORMING APPARATUS USING THE TONER 失效
标题翻译：其链烷基结构和/或苯基磺酰基结构及其制备方法中的聚羟基烷酸酯; 充电控制剂，包含其的调色剂和调色剂; 和图像形成方法和使用调色剂的图像形成装置
公开(公告)号：US06808854B2
公开(公告)日：2004-10-26
申请号：US10133671
申请日：2002-04-29
申请人： Takeshi Imamura , Etsuko Sugawa , Tetsuya Yano , Takashi Kenmoku
发明人： Takeshi Imamura , Etsuko Sugawa , Tetsuya Yano , Takashi Kenmoku
IPC分类号： G03G900
CPC分类号： G03G9/08795 , C08G63/6882 , C12P7/625 , C12P11/00 , G03G9/08755 , G03G9/08791 , G03G9/08797 , G03G9/09733 , G03G9/09775
摘要： The present invention provides a novel polyhydroxyalkanoate (PHA) containing a 3-hydroxyalkanoic unit which has at its side chain terminal a substituted phenylsulfinyl group and/or a substituted phenylsulfonyl group, and a production process thereof. The novel PHA can be produced by oxidizing with a peroxide a biosynthetic PHA containing a 3-hydroxyalkanoic unit which has at its side chain terminal a substituted phenylsufanyl group. The novel PHA has a superior function as a charge control agent, besides is biodegradable, hence is contributable to environmental conservation.
摘要翻译：本发明提供一种含有3-羟基链烷酸单元的新型聚羟基链烷酸酯（PHA）及其制造方法，其在侧链侧具有取代的苯基亚磺酰基和/或取代的苯基磺酰基。新型PHA可以通过用过氧化物氧化含有3-羟基链烷酸单体的生物合成PHA来制备，其在其侧链末端具有取代的苯基苯甲酰基。该新型PHA作为电荷控制剂具有优异的功能，此外是可生物降解的，因此有助于环境保护。

67. 发明授权

US06803444B2 Polyhydroxyalkanoate polyester having vinyl phenyl structure in the side chain and its production method 失效
标题翻译：侧链中具有乙烯基苯基结构的聚羟基链烷酸酯聚酯及其制备方法
公开(公告)号：US06803444B2
公开(公告)日：2004-10-12
申请号：US10084167
申请日：2002-02-28
申请人： Tomohiro Suzuki , Etsuko Sugawa , Tetsuya Yano , Tsuyoshi Nomoto , Takeshi Imamura , Tsutomu Honma , Takashi Kenmoku
发明人： Tomohiro Suzuki , Etsuko Sugawa , Tetsuya Yano , Tsuyoshi Nomoto , Takeshi Imamura , Tsutomu Honma , Takashi Kenmoku
IPC分类号： C08G6306
CPC分类号： C12P7/625 , C08G63/06 , Y10S435/874 , Y10S435/877
摘要： Polyhydroxyalkanoate type polyester that comprises one unit % or more of 3-hydroxy-&ohgr;-(4-vinylphenyl)alkanoic acid units. A microbial production method is also provided.
摘要翻译：包含一个单元％以上的3-羟基-ω-（4-乙烯基苯基）链烷酸单元的聚羟基链烷酸酯型聚酯。还提供微生物生产方法。

68. 发明授权

US06686439B2 Polyhydroxyalkanoate and method of producing same, and &ohgr;-(2-thienylsulfanyl) alkanoic acid and method of producing same 失效
标题翻译：聚羟基链烷酸酯及其制造方法，ω-（2-噻吩基硫烷基）链烷酸及其制造方法
公开(公告)号：US06686439B2
公开(公告)日：2004-02-03
申请号：US10084168
申请日：2002-02-28
申请人： Takashi Kenmoku , Etsuko Sugawa , Tetsuya Yano , Tsuyoshi Nomoto , Takeshi Imamura , Tomohiro Suzuki , Tsutomu Honma
发明人： Takashi Kenmoku , Etsuko Sugawa , Tetsuya Yano , Tsuyoshi Nomoto , Takeshi Imamura , Tomohiro Suzuki , Tsutomu Honma
IPC分类号： C08G6302
CPC分类号： C12P7/625 , C07D333/34 , C08G63/6882 , C12P11/00 , Y10S435/874 , Y10S435/877
摘要： PHA containing a novel 3-hydroxy-thioalkanoic acid unit having a highly reactive thienyl group in a side chain thereof, and a method of producing the same are provided. Specifically, 5-(2-thienyl-sulfanyl)valeric acid represented by Chemical Formula [4] below and 6-(2-thienylsulfanyl)hexanoic acid represented by Chemical Formula [5] below are provided. Further, a method of producing PHA, comprising the step of collecting PHA from cells of a microorganism cultured in a medium containing the valeric acid or hexanoic acid, and a novel PHA represented by Chemical Formula [1] below are provided. (n denotes an integer of 1 to 9)
摘要翻译：提供了含有其侧链中具有高反应性噻吩基的新型3-羟基 - 硫代链烷酸单元的PHA及其制备方法。具体地，提供由下述化学式[4]表示的5-（2-噻吩基 - 硫烷基）戊酸和由下述化学式[5]表示的6-（2-噻吩基硫烷基）己酸。此外，提供了一种制备PHA的方法，其包括从含有戊酸或己酸的培养基中培养的微生物的细胞和由下述化学式[1]表示的新型PHA收集PHA的步骤（n表示 1〜9的整数）

69. 发明授权

US06649381B1 Polyhydroxyalkanoate, method for production thereof and microorganisms for use in the same 失效
标题翻译：聚羟基链烷酸酯，其制备方法和用于其的微生物
公开(公告)号：US06649381B1
公开(公告)日：2003-11-18
申请号：US10411319
申请日：2003-04-11
申请人： Tsutomu Honma , Toyoko Kobayashi , Tetsuya Yano , Shin Kobayashi , Takeshi Imamura , Sakae Suda , Takashi Kenmoku
发明人： Tsutomu Honma , Toyoko Kobayashi , Tetsuya Yano , Shin Kobayashi , Takeshi Imamura , Sakae Suda , Takashi Kenmoku
IPC分类号： C12P762
CPC分类号： C12P7/62 , C08G63/06 , C08G63/6822 , C08G63/6852 , Y10S435/874
摘要： A polyhydroxyalkanoate having a monomer unit composition represented by General Formula (1): AmB(1−m) (1) wherein A is represented by General Formula (2), B is at least one selected from the group consisting of monomer units represented by General Formula (3) or (4), and m has a value of 0.01 or larger and smaller than 1: wherein n has a value of 0 to 10, k has a value of 3 or 5, and R is at least one group selected from the group consisting of groups represented by General Formulae (5) to (7): in Formula (5) R1 is a group selected from the group consisting of a hydrogen atom (H), halogen atoms, —CN, —NO2, —CF3, —C2F5 and —C3F7; and q is an integer selected from 1 to 8; in Formula (6) R2 is a group selected from the group consisting of a hydrogen atom (H), halogen atoms, —CN, —NO2, —CF3, —C2F5 and —C3F7; and r is an integer selected from 1 to 8; in Formula (7) R3 is a group selected from the group consisting of a hydrogen atom (H), halogen atoms, —CN, —NO2, —CF3, —C2F5 and —C3F7; and s is an integer selected from 1 to 8. The efficient production methods are also provided.
摘要翻译：具有由通式（1）表示的单体单元组成的聚羟基链烷酸酯：其中A由通式（2）表示，B为选自由通式（3）或（4）表示的单体单元中的至少一种， m的值为0.01以上且小于1：其中n为0〜10，k为3或5，R为选自由通式（1）表示的基团中的至少1种 5）至（7）：在式（5）中，R 1为选自氢原子（H），卤素原子，-CN，-NO 2，-CF 3，-C 2 F 5和-C 3 F 7的基团; q为选自1至8的整数;在式（6）中，R 2为选自氢原子（H），卤素原子，-CN，-NO 2，-CF 3，-C 2 F 5和-C 3 F 7 ; 并且r是选自1至8的整数;在式（7）中，R 3是选自氢原子（H），卤素原子，-CN，-NO 2，-CF 3，-C 2 F 5和-C 3 F 7的基团 ; s是选自1至8的整数。还提供了有效的制备方法。

70. 发明授权

US06479621B2 Polyhydroxyalkanoate containing 3-hydroxythienylalkanoic acid as monomer unit and method for producing the same 失效
标题翻译：含有3-羟基噻吩基链烷酸作为单体单元的聚羟基链烷酸酯及其制备方法
公开(公告)号：US06479621B2
公开(公告)日：2002-11-12
申请号：US09793920
申请日：2001-02-28
申请人： Tsutomu Honma , Tetsuya Yano , Shin Kobayashi , Takeshi Imamura , Takashi Kenmoku , Shinya Kozaki
发明人： Tsutomu Honma , Tetsuya Yano , Shin Kobayashi , Takeshi Imamura , Takashi Kenmoku , Shinya Kozaki
IPC分类号： C08G6306
CPC分类号： C12P7/625 , C08G63/6882 , Y10S435/874 , Y10S435/877
摘要： Microorganisms capable of synthesizing novel polyhydroxyalkanoate having 3-hydroxythienylalkanoic acid as monomer unit, using thienylalkanoic acid as a stock are cultured on a culture medium containing thienylalkanoic acid, and the polyhydroxyalkanoate produced in the cultured cell is extracted and
摘要翻译：使用噻吩烷基酸作为原料合成具有3-羟基噻吩基链烷酸作为单体单元的新型聚羟基链烷酸酯的微生物在含有噻吩基链烷酸的培养基上培养，提取培养细胞中产生的聚羟基链烷酸酯，

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