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61. 发明申请

US20110034707A1 METHOD FOR STARTING A GAS-PHASE OXIDATION REACTOR 有权
标题翻译：启动气相氧化反应器的方法
公开(公告)号：US20110034707A1
公开(公告)日：2011-02-10
申请号：US12936807
申请日：2009-04-07
申请人： Hagen Wilmer , Zürgen Zühike , Thomas Lautensack , Hans-Martin Allmann , Frank Rosowski , Cornelia Katharina Dobner
发明人： Hagen Wilmer , Zürgen Zühike , Thomas Lautensack , Hans-Martin Allmann , Frank Rosowski , Cornelia Katharina Dobner
IPC分类号： C07D307/89
CPC分类号： C07C51/265 , C07D307/89
摘要： What is described is a process for starting up a gas phase oxidation reactor for oxidation of o-xylene to phthalic anhydride, said reactor comprising at least one catalyst layer and being temperature-controllable by means of a heat carrier medium, wherein a) the catalyst layer is interrupted by a moderator layer which is less catalytically active than the catalyst layer or is catalytically inactive, b) a gas stream is passed through the reactor with an initial loading of o-xylene and at an initial temperature of the heat transfer medium, c) the loading of the gas stream is increased to a target loading and, in parallel, the temperature of the heat transfer medium is lowered to an operating temperature. The introduction of the moderator layer allows the loading to be increased more rapidly and the startup time to be shortened.
摘要翻译：描述的是用于启动用于将邻二甲苯氧化成邻苯二甲酸酐的气相氧化反应器的方法，所述反应器包括至少一个催化剂层，并且可通过热载体介质温度控制，其中a）催化剂层被催化剂层催化活性较低或催化无活性的中间体层中断，b）气流以邻二甲苯的初始负荷和传热介质的初始温度通过反应器， c）将气流的负载增加到目标负载，并且并联地将传热介质的温度降低到工作温度。调节器层的引入允许加载更快速并且启动时间被缩短。

62. 发明申请

US20100069659A1 PROCESS FOR PRODUCING GEOMETRIC SHAPED CATALYST BODIES 有权
标题翻译：生产几何形状催化剂体的方法
公开(公告)号：US20100069659A1
公开(公告)日：2010-03-18
申请号：US12546883
申请日：2009-08-25
申请人： Andreas RAICHLE , Catharina Horstmann , Frank Rosowski , Klaus Joachim Muller-Engel , Holger Borchert , Gerhard Cox , Ulrich Cremer
发明人： Andreas RAICHLE , Catharina Horstmann , Frank Rosowski , Klaus Joachim Muller-Engel , Holger Borchert , Gerhard Cox , Ulrich Cremer
IPC分类号： C07C253/18 , B01J21/06 , C07C45/35
CPC分类号： C07C45/28 , B01J23/002 , B01J23/8885 , B01J35/0006 , B01J35/023 , B01J37/0036 , B01J37/0221 , B01J37/04 , B01J2523/00 , C07C45/35 , C07C45/37 , C07C51/252 , C07C253/26 , Y02P20/52 , C07C47/22 , C07C57/04 , B01J2523/13 , B01J2523/41 , B01J2523/54 , B01J2523/68 , B01J2523/69 , B01J2523/842 , B01J2523/845 , C07C255/08
摘要： A process for producing geometric shaped catalyst bodies K whose active material is a multielement oxide of stoichiometry [Bi1WbOx]a[Mo12Z1cZ2dFeeZ3fZ4gZ5nOy]1, in which a finely divided oxide Bi1WbOx with the particle size d50A1 and, formed from element sources, a finely divided intimate mixture of stoichiometry Mo12Z1cZ2dFeeZ3fZ4gZ5h with the particle size d50A2 are mixed in a ratio of a:1, this mixture is used to form shaped bodies and these are treated thermally, where (d50A1)0.7•(d90A1)1.5•(a)−1≧820.
摘要翻译：一种用于生产几何形状的催化剂体K的方法，其活性材料是化学计量[Bi1WbOx] a [Mo12Z1cZ2dFeeZ3fZ4gZ5nOy] 1的多元素氧化物，其中具有粒度d50A1的细分离氧化物Bi1WbOx，并且由元素源形成，化学计量比的混合物Mo12Z1cZ2dFeeZ3fZ4gZ5h以a：1的比例混合，该混合物用于形成成型体，热处理，其中（d50A1）0.7•（d90A1）1.5•（a）-1≧ 820。

63. 发明申请

US20090198073A1 PREPARATION OF PHTHALIC ANHYDRIDE BY GAS PHASE OXIDATION OF O-XYLENE 有权
标题翻译：气相氧化制备邻苯二甲酸二异氰酸酯
公开(公告)号：US20090198073A1
公开(公告)日：2009-08-06
申请号：US12301352
申请日：2007-05-18
申请人： Thomas Mackewitz , Frank Rosowski , Andreas Tenten
发明人： Thomas Mackewitz , Frank Rosowski , Andreas Tenten
IPC分类号： C07D317/46
CPC分类号： C07D307/89 , C07C51/265 , C07C63/16
摘要： A process is described for preparing phthalic anhydride by catalytic gas phase oxidation of o-xylene. In, in a main reactor, a gaseous mixture of o-xylene and an oxygenous gas is passed through at least two reaction zones whose temperature can be controlled independently, and converted to a gaseous intermediate reaction product which comprises unconverted o-xylene, phthalic anhydride underoxidation products and phthalic anhydride, and the intermediate reaction product is introduced into a postreactor, wherein the temperature of the reaction zones in the main reactor is regulated in such a way that the concentration of unconverted o-xylene in the intermediate reaction product is at least 0.5% by weight. The process allows an increase in the overall yield of phthalic anhydride without or without significant deterioration in the product quality.
摘要翻译：描述了通过邻二甲苯的催化气相氧化制备邻苯二甲酸酐的方法。在主反应器中，邻二甲苯和氧气的气态混合物通过至少两个反应区，其温度可独立控制，并转化成气态中间反应产物，其包含未转化的邻二甲苯，邻苯二甲酸酐未反应产物和邻苯二甲酸酐，并将中间反应产物引入后反应器中，其中主反应器中反应区的温度调节为使中间反应产物中未转化的邻二甲苯的浓度至少为 0.5重量％。该方法允许邻苯二甲酸酐的总产率提高，而不会产生质量的显着劣化。

64. 发明授权

US07402288B2 Reactor for testing catalyst systems 失效
标题翻译：用于测试催化剂体系的反应器
公开(公告)号：US07402288B2
公开(公告)日：2008-07-22
申请号：US10478684
申请日：2002-06-05
申请人： Gerhard Olbert , Torsten Mattke , Matthias Kummer , Thomas Ruehl , Frank Rosowski
发明人： Gerhard Olbert , Torsten Mattke , Matthias Kummer , Thomas Ruehl , Frank Rosowski
IPC分类号： B01J19/24 , F27B15/14 , F28D7/16 , G01N31/10
CPC分类号： G01N31/10 , B01J8/067 , B01J2208/00168 , B01J2208/00221 , B01J2208/0023 , B01J2208/00256 , B01J2208/021 , B01J2219/00009 , B01J2219/00745 , B01J2219/00747 , B01J2219/00777 , C40B30/08 , C40B40/18 , F28D7/0066 , F28D7/0091
摘要： A reactor for testing catalyst systems which has a plurality of catalyst tubes (2) which are arranged parallel to one another in the interior space of the reactor and whose ends are welded into tube plates and also has caps (3) at each end of the reactor which each bound a cap space (4), with a fluid reaction medium (5) being fed via one cap space (4) into the catalyst tubes (2), flowing through the catalyst tubes (2) and being discharged via the other cap space (4), and is also provided with a heat exchange medium circuit in which the heat exchange medium (6) is fed in at one end of the reactor, flows through the intermediate space between the catalyst tubes (2) and flows out at the other end of the reactor, wherein the catalyst tubes (2) are arranged in two or more catalyst tube regions (7) which are thermally separate from one another, is proposed.
摘要翻译：一种用于测试催化剂体系的反应器，其具有多个催化剂管（2），所述多个催化剂管（2）在所述反应器的内部空间中彼此平行地布置，并且其端部被焊接到管板中，并且在所述反应器的每一端具有盖（3）反应器，每个反应器结合盖空间（4），流体反应介质（5）经由一个盖空间（4）进入催化剂管（2），流过催化剂管（2）并经由另一个排出盖子空间（4），并且还设置有热交换介质回路，其中热交换介质（6）在反应器的一端进料，流过催化剂管（2）之间的中间空间并流出在反应器的另一端，其中催化剂管（2）布置在彼此热分离的两个或更多个催化剂管区域（7）中。

65. 发明申请

US20070270597A1 Process for preparing maleic anhydride in a microchannel reactor 审中-公开
标题翻译：在微通道反应器中制备马来酸酐的方法
公开(公告)号：US20070270597A1
公开(公告)日：2007-11-22
申请号：US11798707
申请日：2007-05-16
申请人： Hagen Wilmer , Torsten Maurer , Frank Rosowski , Rudolf Schuch
发明人： Hagen Wilmer , Torsten Maurer , Frank Rosowski , Rudolf Schuch
IPC分类号： C07D307/34
CPC分类号： C07D307/34
摘要： The present invention relates to a process for preparing maleic anhydride by heterogeneously catalyzed gas-phase oxidation of a hydrocarbon, which comprises feeding a hydrocarbon-comprising stream and a stream comprising oxygen or an oxygen source into a microchannel reactor and carrying out the reaction to form maleic anhydride in the explosive range in the microchannel reactor comprising the catalyst.
摘要翻译：本发明涉及通过烃的非均相催化气相氧化制备马来酸酐的方法，该方法包括将包含烃的料流和包含氧或氧源的物流进入微通道反应器并进行反应以形成在包含催化剂的微通道反应器的爆炸范围内的马来酸酐。

66. 发明授权

US07176335B2 Method for producing methacrolein from isobutane 失效
标题翻译：从异丁烷生产甲基丙烯醛的方法
公开(公告)号：US07176335B2
公开(公告)日：2007-02-13
申请号：US10482337
申请日：2002-06-28
申请人： Silke Berndt , Klaus Joachim Mueller-Engel , Goetz-Peter Schindler , Frank Rosowski , Jochen Petzoldt
发明人： Silke Berndt , Klaus Joachim Mueller-Engel , Goetz-Peter Schindler , Frank Rosowski , Jochen Petzoldt
IPC分类号： C07C45/29 , C07C51/16 , C07C67/00
CPC分类号： B01J23/002 , B01J27/199 , B01J2523/00 , C07C45/33 , C07C45/35 , C07C47/22 , B01J2523/13 , B01J2523/15 , B01J2523/3706 , B01J2523/43 , B01J2523/828 , B01J2523/41 , B01J2523/54 , B01J2523/68 , B01J2523/69 , B01J2523/842 , B01J2523/845 , B01J2523/17 , B01J2523/51 , B01J2523/53 , B01J2523/55 , B01J2523/62
摘要： A process prepares methacrolein from isobutane by subjecting isobutane to a partial catalytic dehydrogenation in the gas phase and using the isobutenic product gas mixture to charge an oxidation zone in which the isobutene is oxidized to methacrolein in the gas phase with heterogeneous catalysis using molecular oxygen accompanied by molecular nitrogen as the oxygen source.
摘要翻译：一种方法是通过使异丁烷在气相中进行部分催化脱氢，并使用异丁烯产物气体混合物，在气相中将异丁烯氧化成甲基丙烯醛的氧化区，使用分子氧伴随着非均相催化，由异丁烷制备异丁烯醛分子氮作为氧源。

67. 发明授权

US07134848B2 Pump for transporting heat-exchange medium for a multi-tube reactor 有权
标题翻译：用于输送多管反应器的热交换介质的泵
公开(公告)号：US07134848B2
公开(公告)日：2006-11-14
申请号：US10479625
申请日：2002-06-05
申请人： Gerhard Olbert , Torsten Mattke , Matthias Kummer , Thomas Rühl , Frank Rosowski
发明人： Gerhard Olbert , Torsten Mattke , Matthias Kummer , Thomas Rühl , Frank Rosowski
IPC分类号： G21C19/04
CPC分类号： F04D3/00 , F04D29/406
摘要： The invention relates to a pump (1) having a pump guide tube (13) for the transport of a heat-exchange medium (6) for a reactor having a bundle of catalyst tubes (2), where the pump (1) has a casing (14) which surrounds the pump guide tube (13), having an aperture (15) in the lower part of the casing (14) via which the heat-exchange medium (6) discharged from the lower region of the reactor by means of the pump (1) flows into the casing (14), flows upward in the region between the inner wall of the casing (14) and the outer wall of the pump guide tube (13), if desired via a heat exchanger (18), flows into the interior of the pump guide tube (13) via an aperture (16) in the upper region of the pump guide tube (13), flows through the pump guide tube (13) from top to bottom and flows via an aperture (17) in the lower region of the pump guide tube (13) into the reactor, into the upper region of the interspace between the catalyst tubes (2).
摘要翻译：本发明涉及一种具有泵引导管（13）的泵（1），用于输送用于具有一束催化剂管（2）的反应器的热交换介质（6），其中泵（1）具有围绕所述泵引导管（13）的壳体（14），在所述壳体（14）的下部具有孔（15），所述热交换介质（6）经由所述开口（15）从所述反应器的下部区域排出，如果需要，通过热交换器（18）将泵（1）流入壳体（14）中，在壳体（14）的内壁和泵引导管（13）的外壁之间的区域中向上流动）通过泵引导管（13）的上部区域中的孔（16）流入泵引导管（13）的内部，从上到下流过泵引导管（13），并经由在泵引导管（13）的下部区域中的孔（17）进入反应器，进入催化剂管（2）之间的间隙的上部区域。

68. 发明授权

US06933407B2 Method for producing methacrylic acid from isobutane 失效
标题翻译：从异丁烷生产甲基丙烯酸的方法
公开(公告)号：US06933407B2
公开(公告)日：2005-08-23
申请号：US10480651
申请日：2002-06-28
申请人： Silke Berndt , Klaus Joachim Müller-Engel , Götz-Peter Schindler , Frank Rosowski , Jochen Petzoldt
发明人： Silke Berndt , Klaus Joachim Müller-Engel , Götz-Peter Schindler , Frank Rosowski , Jochen Petzoldt
IPC分类号： C07C51/235 , B01J27/199 , C07B61/00 , C07C45/33 , C07C45/35 , C07C51/25 , C07C57/05 , C07C57/055 , C07C51/16
CPC分类号： B01J23/002 , B01J27/199 , B01J2523/00 , C07C45/33 , C07C45/35 , C07C51/252 , C07C47/22 , C07C57/04 , B01J2523/17 , B01J2523/53 , B01J2523/13 , B01J2523/15 , B01J2523/3706 , B01J2523/41 , B01J2523/43 , B01J2523/48 , B01J2523/828 , B01J2523/54 , B01J2523/68 , B01J2523/69 , B01J2523/842 , B01J2523/845 , B01J2523/51 , B01J2523/55 , B01J2523/62
摘要： A process prepares methacrylic acid from isobutane by subjecting isobutane to a partial catalytic dehydrogenation in the gas phase and charging an oxidation zone with the isobutenic product gas mixture after the components other than isobutane and isobutene have been substantially removed from the product gas mixture. The oxygen required to charge the oxidation zone is introduced accompanied by nitrogen.
摘要翻译：通过使异丁烷在气相中进行部分催化脱氢，并且在异丁烷和异丁烯以外的成分从产物气体混合物中除去之后，通过异丁烯产物气体混合物装入氧化区，从异丁烷中制备甲基丙烯酸。伴随着氮气导入氧化区域所需的氧气。

69. 发明授权

US06781017B2 Method for the production of acrolein or acrylic acid or the mixture thereof from propane 有权
标题翻译：从丙烷生产丙烯醛或丙烯酸或其混合物的方法
公开(公告)号：US06781017B2
公开(公告)日：2004-08-24
申请号：US10297602
申请日：2002-12-13
申请人： Otto Machhammer , Goetz-Peter Schindler , Andreas Tenten , Klaus Harth , Peter Zehner , Klaus Joachim Müller-Engel , Frank Rosowski , Frieder Borgmeier
发明人： Otto Machhammer , Goetz-Peter Schindler , Andreas Tenten , Klaus Harth , Peter Zehner , Klaus Joachim Müller-Engel , Frank Rosowski , Frieder Borgmeier
IPC分类号： C07C4500
CPC分类号： C07C51/215 , C07C5/333 , C07C45/33 , C07C45/35 , C07C51/252 , C07C11/06 , C07C47/22 , C07C57/04
摘要： In a process for the preparation of acrolein or acrylic acid or a mixture thereof from propane, the propane is subjected, in a first reaction stage, to a partial dehydrogenation under heterogeneous catalysis to give propene, of the components contained in the product gas mixture formed in the first reaction stage other than propene and propane at least a portion of the molecular hydrogen present is then separated off from said mixture and the product gas mixture is then used for the preparation of acrolein and/or acrylic acid by gas-phase catalytic propylene oxidation, molecular nitrogen being present for diluting the reaction gas mixture during the propylene oxidation.
摘要翻译：在从丙烷制备丙烯醛或丙烯酸或其混合物的方法中，丙烷在第一反应阶段中在非均相催化下进行部分脱氢以形成产物气体混合物中所含组分的丙烯在除丙烯和丙烷之外的第一反应阶段中，存在的分子氢的至少一部分然后从所述混合物中分离出来，然后将产物气体混合物用于通过气相催化丙烯制备丙烯醛和/或丙烯酸存在氧化，分子氮，用于在丙烯氧化期间稀释反应气体混合物。

70. 发明授权

US08580982B2 Use of structured catalyst beds for preparing ethylene oxide 有权
标题翻译：使用结构化催化剂床制备环氧乙烷
公开(公告)号：US08580982B2
公开(公告)日：2013-11-12
申请号：US13376879
申请日：2010-06-09
申请人： Georg Seeber , Torsten Mäurer , Gerhard Theis , Dieter Köffer , Frank Rosowski
发明人： Georg Seeber , Torsten Mäurer , Gerhard Theis , Dieter Köffer , Frank Rosowski
IPC分类号： C07D301/03
CPC分类号： C07D301/10
摘要： The present invention relates to a process for preparing ethylene oxide by reaction of ethylene with oxygen in the presence of at least one silver-comprising catalyst, wherein the reaction takes place in a reactor which has a catalyst packed bed having at least two zones (i) and (ii) and the silver content of the catalyst in zone (i) is lower than the silver content of the catalyst in zone (ii). The catalyst packed bed preferably has a further zone (a) with which the reaction mixture comes into contact before the zones (i) and (ii). According to the invention, the silver content of the catalyst in the zone (a) is higher than the silver content of the catalyst in zone (i).
摘要翻译：本发明涉及通过乙烯与氧在至少一种含银催化剂存在下反应来制备环氧乙烷的方法，其中该反应在具有至少两个区域的催化剂填充床（i ）和（ii），并且（i）区域中的催化剂的银含量低于区域（ii）中的催化剂的银含量。催化剂填充床优选具有另外的区域（a），反应混合物在区域（i）和（ii）之前与其接触。根据本发明，区域（a）中催化剂的银含量高于区域（i）中催化剂的银含量。

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